Lucent Technologies Inc.

Fitel USA Corporation

Furukawa Electric Na

Yoram De Hazan

John Burnette MacChesney

Thomas Edward Stockert

Suhas Dattatreya Bhandarkar

Robert Scott Windeler

Christopher Alan White

Dennis J Trevor

Eric M Monberg

The use of large dense vitreous spherical (LDVS) silica powders for making sol-gel silica bodies has been found to have important advantages. Among these are higher gel strength, higher silica loading, more rapid aging and drying of the gel, a reduction in the amount of organic additives leading to reduced process time required for organic burn-off, and easier removal of contaminant particles due to their larger size. It was also discovered that combining LDVS particles with conventional non-spherical, lower density, aggregate particle mixtures, further improves the process.

Manufacture of silica bodies using sol-gel techniques

The doped silica core region of a core rod for an optical fiber preform is protected against unwanted fluorine doping during fluorine doping of the outer silica layer by selectively consolidating the core region prior to fluorine doping. Due to dopants in the core region, the soot in the core region consolidates before the soot in the outer undoped region. This inherent property allows the entire core rod to be heated prior to fluorine doping resulting in selective partial consolidation and preventing fluorine doping of the doped center core region. The process time required may be reduced by using incremental fluorine doping. In the incremental doping process the doping step is separated into a deposit step, where &ldquo;excess&rdquo; fluorine is deposited on the silica particles, and a drive-in step where atomic fluorine is distributed into the silica particles. The drive-in step is conveniently combined with the sintering or consolidation step to further enhance the efficiency of the doping process.

Controlled collapse of depressed index optical fiber preforms

The process time required for fluorine doping of porous silica bodies to produce fluorine doped preforms for the manufacture of depressed index optical fibers is reduced by separating the doping step into a predeposit step, where &ldquo;excess&rdquo; fluorine is deposited on the silica particles, and a drive-in step where atomic fluorine is distributed into the silica particles. The drive-in step is conveniently combined with the sintering or consolidation step to further enhance the efficiency of the doping process.

Manufacture of depressed index optical fibers

The use of silica powders having large particle sizes in making sol-gel silica bodies has been found to have important advantages. Among these are higher gel strength, higher silica loading, more rapid aging and drying of the gel, a reduction in the amount of organic additives leading to reduced process time required for organic burn-off, and easier removal of contaminant particles due to their larger size. It was also discovered that spherical particle morphology contributes to the improved properties.

The disclosed method of making microstructured optical fiber comprises providing a mold, with a multiplicity of elongate elements extending into the mold and being maintained in a predetermined spatial arrangement with respect to the mold. Silica-containing sol is introduced into the mold and is caused to or permitted to gel, such that a gel body results. After removing the elongate elements from the gel body and removing the gel body from the mold, the gel body is dried, sintered and purified, and the microstructured fiber is drawn from the sintered body.

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Oley, PA, United States of America

Yoram De Hazan