Ifp Energies Nouvelles

Eramet

Nanomakers

Yohan Florent Oudart

Malika Boualleg

Vincent Lecocq

Fabien Burdet

Alexandre Chambard

Fabien André Pierre Burdet

Jean-François Perrin

Guillaume Patrick André Maillet

The present invention relates to the field of solid materials for the adsorption of lithium. In particular, the present invention relates to a new method for the preparation of a crystallized and shaped solid material, preferably in extruded form, of the formula (LiCl).2Al(OH),nHO, wherein n is between 0.01 and 10, x is between 0.4 and 1, wherein it comprises a step a) of precipitation of boehmite under specific temperature and pH conditions, a step of bringing into contact the precipitate obtained with LiCl, at least one acid extrusion-kneading shaping step, wherein the method also comprises a final hydrothermal treatment step, all of which makes it possible to increase the lithium adsorption capacity, the adsorption kinetics, as well as the lithium/boron selectivity of the materials obtained with respect to the materials of the prior art, when it is used in a lithium extraction method of saline solutions.

Method for producing an adsorbent material and method for extracting lithium from saline solutions using the material

The present invention relates to the field of solid materials for the adsorption of lithium. In particular, the present invention relates to a novel process for preparing a solid crystalline material formed preferably in extrudate form, of formula (LiCl).2Al(OH),nHO with n being between 0.01 and 10, x being between 0.4 and 1, comprising a step a) to precipitate boehmite under specific conditions of temperature and pH, a step to place the precipitate obtained in contact with a specific quantity of LiCl, at least one forming step preferably via extrusion, said process also comprising a final hydrothermal treatment step, all allowing an increase in lithium adsorption capacity and in the adsorption kinetics of the materials obtained compared to prior art materials, when used in a process to extract lithium from saline solutions.

Process for preparing an adsorbent material and process for extracting lithium using said material

A production method is provided in which submicronic particles containing silicon are incorporated into a matrix, wherein, during the incorporation of the particles, the particles are in a compacted state with a bulk density of more than 0.10 grams per cubic centimeter, and the compacted particles have a specific surface area at least 70% of that of the particles considered separately without contact between each other.

Production method incorporating particles containing silicon

For preparing a reforming catalyst comprising a support, a group VIIIB metal and a group VIIB metal, comprises the following steps in the order a) then b) or b) then a):

Process for preparing a reforming catalyst comprising a support, a group VIIIB metal and a group VIIB metal

The invention relates to a method of preparing a dehydrogenation catalyst comprising a group VIII metal, a group IVA metal and a refractory oxide support. The method comprises stages of preparing the dry impregnation aqueous solution containing said group VIII metal, ammonia, either in solution or in gas form, and a complexing agent. It then comprises stages of aging the aqueous solution, of dry impregnation of the support, of maturing the impregnated support, of drying the impregnated support and of calcining the dried support.

Dehydrogenation catalyst preparation by dry impregnation

The invention relates to a method of preparing a reforming catalyst comprising a group VIII metal, a halogen, at least one metal selected from the group made up of the group VIIB metals and group IVA metals, a refractory oxide support. The method comprises stages of preparing a dry impregnation aqueous solution containing ammonia, either in solution or in gas form and a complexing agent, of aging the aqueous solution, of dry impregnation of the support, of maturing the impregnated support, of drying and of calcination.

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Versailles, France

Yohan Florent Oudart