Chinese Academy of Sciences

Changchun Institute of Applied Chemistry

Xuguang Li

Tianhong Lu

Wei Xing

A method of preparing non-platinum composite electrocatalyst for a fuel cell cathode, comprising: (1) preparing a carbon supporting titanium dioxide; (2) compounding the carbon supporting titanium dioxide with a transition metal macrocyclic compound in an organic solvent to produce a carbon supporting titanium dioxide-transition metal macrocyclic compound comprising 0.1&#x2013;5 g/L of macrocyclic compound; and (3) thermal treating the resulting compound in step (2) at 100&#x2013;1000&#xb0; C. to produce a composite catalyst. The composite catalyst prepared with the method according to the present invention also has the advantages of better resistance to methanol and lower cost over the Pt/C catalyst. The said composite catalyst would have better prospects in application.

Method of preparation of non-platinum composite electrocatalyst for cathode of fuel cell

The present invention relates to a method for preparing nano-level Pt/C electrocatalyst for cathode of fuel cell. By employing ammonium chloride, potassium chloride, ammonium bromide, potassium bromide, ammonium iodide or potassium iodide as anchoring agent for the chloroplatinic acid, the present invention realizes the preparation of Pt/C electrocatalyst with platinum micro-particles homogeneously distributed in the interstices as well as on the surfaces of the active carbon. The sizes of the platinum particles in the catalyst are homogeneous and their average diameter is in the range of 2.5 to 4.5 mm. The present method is a novel one for preparing nanometer level Pt/C electrocatalyst. Said electrocatalyst possesses high specific activity per unit mass for the catalytic reduction of oxygen.

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Changchun, China

Xuguang Li