Qianjiang Yongan Pharmaceutical Co., Ltd.

Other

Qiangjiang Yongan Pharmaceutical Co., Ltd.

Xiquan Fang

Yong Chen

Shaobo Li

Feng Liu

Xiaojun Jiang

Wei Zhou

The present disclosure relates to a method for recycling a taurine mother liquor, which includes: adding a base to the taurine mother liquor, heating to a first temperature, carrying out a hydrolysis reaction, removing ammonia produced, and evaporating and concentrating the ammonia-removed solution to obtain an alkali metal hydroxyethyl sulfonate solution. When applying the method provided by the present disclosure for the recycling of the taurine mother liquor, the taurine mother liquor can be further converted into the alkali metal hydroxyethyl sulfonate solution, impurities are removed from the obtained alkali metal hydroxyethyl sulfonate solution, the impurity-removed alkali metal hydroxyethyl sulfonate solution is concentrated and crystallized, and the alkali metal hydroxyethyl sulfonate is separated out. The method provided by the present disclosure is an efficient and simple method for recycling the taurine mother liquor, which is very easy to implement industrially and can effectively recycle the taurine mother liquor.

Method for recycling taurine mother liquor

The present invention discloses a method for preparing taurine. According to the method, ethylene oxide reacts with hydrogen sulfite to generate isethionate, after the isethionate and ammonia are subjected to an ammonolysis reaction under a microwave condition, ammonia removal is conducted to obtain a taurine salt solution, the taurine salt solution is converted into a taurine solution through acidification or ion exchange or ion membrane or heating, and taurine is extracted through concentration and crystallization. According to the present invention, the reaction time can be shortened, and the reaction temperature and pressure can be reduced, thereby achieving high yield and reducing energy consumption.

Method for preparing taurine

A method for preparing high-purity taurine and salt by reacting ethylene oxide with bisulfite to generate isethionate, performing an ammonolysis reaction on the isethionate in combination with ammonia and a metal salt, evaporating the reaction solution and subjecting the concentrated solution to ion exchange to obtain an adsorption solution, extracting taurine from the adsorption solution, eluting adsorbed metal cations from the ion exchange system by an acid, and separately collecting the eluate containing a salt.

Method and system for preparing high-purity taurine and salt

A method for removing impurities from a taurine mother liquor and recovering the taurine mother liquor. The method is used in an ethylene oxide production process for taurine. The last mother liquor of taurine is ion-exchanged through an anion exchange resin; then the anion exchange resin is eluted and regenerated with alkaline solution, and the eluate is collected. The eluate is subjected to ammonia mixing treatment, and the treated mother liquor is generated after the impunity is removed from the eluate by solid-liquid separation. The treated mother liquor can then be returned to the ammonolysis step of taurine production.

Method and system for removing impurities out of taurine mother liquor and taurine mother liquor recovery

A method and a production system for recovering and treating taurine mother liquor, which is used for the process of ethylene oxide taurine production process. As for the treatment of the last mother liquor of taurine, add alkali firstly to the last mother liquor of taurine and then acid to form salt, or add salt directly; then concentrate and crystallize and filter, to remove lots of impurities in taurine mother liquor. This solves the problem of separating impurities, greatly shortening the time of removing impurities. The last mother liquor can also be decolorizes and additional impurities removes by activated carbon, and the removal of salt by mixing ammonia into the mother liquor to obtain the pure taurine mother liquor, thereby recovering the mother liquor and increasing the product yield.

Method and production system for fully recovering and treating taurine mother liquor

The high-yield circular production method of taurine includes the following steps: S1, ethylene oxide reacts with sodium bisulfite solution to generate sodium hydroxyethyl sulfonate; S2, sodium hydroxyethyl sulfonate obtained in S1 is subjected to ammonolysis reaction in ammonia, and ammonia gas is recycled through flash evaporation upon completion of the reaction; S3, a reaction solution obtained after flash evaporation in S2 is sent to pass through an acidic cation exchange resin column, a material liquid containing taurine is collected, the inactivated resin column is subjected to regeneration with sulfur dioxide or carbon dioxide aqueous solution, and an eluent acquired during regeneration can be recycled directly or recycled after treated by sulfur dioxide; S4, the material liquid collected in S3 is subjected to post treatment to acquire taurine.

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Qianjiang, China

Xiquan Fang