China University of Petroleum

Xianbin Huang

Jingping Liu

Kaihe Lv

Jinsheng Sun

Jintang Wang

Yingrui Bai

Jiafeng Jin

Guancheng Jiang

Jian Li

Yinbo He

Shenglong Shi

Lili Yang

Zhengqiang Deng

Meichun Li

Li Li Zhao

Fan Liu

Yang Xuan

Tengfei Dong

Xuwu Luo

Kun Zhang

Shuanglei Peng

Kai Wang

Yang Bai

Xi Wang

Chunlei Wang

Chong Liu

Chunyao Peng

Guangchang Ma

Xiaohui Sun

Wei Wan

Xinliang Li

Rongchao Cheng

Xiaoxiao Ni

Ren Wang

Yawei Shi

Haiyang Liu

Jingen Deng

Wuquan Li

Xiaoqing Li

Weian Huang

Zepu Cheng

He Li

Jiaqi Xu

Bo Liao

Mei-Chun Li

Ziyan Li

Xiaosen Shang

A phase change microcapsule for drilling fluid cooling and its preparation method and application, belonging to the field of oilfield chemistry technology; the preparation method of the phase change microcapsule of the invention includes the steps as follows: the core materials of NaNOand KNOare dried, heated, melted, cooled and ground to obtain a phase change material mixture; added emulsifier into the linseed oil, then heated and stirred to obtain the oil phase; the phase change material mixture were added into the suspension of cellulose nanofibers (CNFs), then stirred followed by adding ammonium hydroxide to obtain the water phase; mixed the water phase with the oil phase, heated and stirred to form water-in-oil (W/O) emulsion; then added shell prepolymer material (tetraethyl silicate) into the emulsion, after centrifugation, washing and drying, the phase change microcapsule for cooling drilling fluid was obtained.

Phase change microcapsule for drilling fluid cooling and its preparation method and application

A high-temperature and high-salt resistant hyperbranched lubricant for a water-based drilling fluid, and preparation and application thereof are provided, belonging to the technical field of oilfield chemistry. The preparation method includes the steps of: mixing tetraethyl orthosilicate (TEOS), diethanolamine (DEA), and triethanolamine (TEA) for a transesterification and polycondensation reaction to obtain highly reactive hyperbranched polysiloxane; adding an acrylamide (AM) monomer, an anionic monomer, and a polar ester monomer into deionized water to obtain a monomer solution; adjusting the pH of the monomer solution to 5-9, and then adding highly reactive hyperbranched polysiloxane; introducing nitrogen to remove oxygen, adding an initiator, and thermally initiating a polymerization reaction; and after the reaction is completed, vacuum-drying and crushing an obtained product to obtain the high-temperature and high-salt resistant hyperbranched lubricant for a water-based drilling fluid.

High-temperature and high-salt resistant hyperbranched lubricant for water-based drilling fluid, and preparation and application thereof

Disclosed is a bio-enzyme degradable temporary plugging material and a preparation method and application thereof in the technical field of natural gas hydrate drilling and production; the preparation method of the bio-enzyme degradable temporary plugging material includes the following steps: mixing the ceramsite with an aqueous solution of 3-aminopropyl trimethoxysilane before a stirring reaction and drying to obtain modified ceramsite; and fully dispersing the modified ceramsite, ethyl cellulose, and epoxy resin in dichloromethane to obtain an oil phase; adding the oil phase into a gelatin aqueous solution and mixing uniformly; after a stirring reaction, evaporating an organic solvent, filtering, washing, and drying, to obtain the bio-enzyme degradable temporary plugging material.

Bio-enzyme degradable temporary plugging material and preparation method and application thereof

An oil-soluble thermosensitive resin lost circulation material for protecting a reservoir includes the following raw materials in parts by weight: 40-60 parts of resin matrix, 15-40 parts of modified asphalt, 5-12 parts of viscosity modifier, 2-5 parts of cross-linking agent, 6-15 parts of softening point modifier, and 1-3 parts of dispersant; it further provides a method for preparing the resin lost circulation material; the resin lost circulation material can melt and adhere in different temperature ranges, rapid plugging is realized, and the plugging time is long; the oil-soluble thermosensitive resin lost circulation material can be dissolved by oil flow during oil well production, so that the reservoir permeability is recovered, so as to achieve the purpose of protecting the hydrocarbon reservoir.

Oil-soluble thermosensitive resin lost circulation material for protecting a reservoir as well as preparation method and application thereof

A high temperature and high salinity-resistant complementarily rigid-flexible plugging agent, a method for preparing the same, and a water-based drilling fluid and a use thereof.

High temperature and high salinity-resistant complementarily rigid-flexible plugging agent and method for preparing the same and water-based drilling fluid and use thereof

A nano-organosilicon film-forming and hydrophobic shale surface hydration inhibitor is obtained by performing hydrophobic modification for nano-particles through long-chain organosilicon together with a surface-active agent. A preparation method of the said hydrophobic shale surface hydration inhibitor comprises steps as follows: nano-particles are added to the solvent under stirring conditions, and then an ultrasonic dispersion is performed; upon the end of the ultrasonic dispersion, the reaction system is adjusted to a pH of 9-11 to obtain mixed solution A; a long-chain organosilicon solution is then dropwise added to the mixed solution A for reaction under stirring conditions to obtain mixed solution B; a surface-active agent is added to the mixed solution B for reaction under stirring conditions; upon the reaction is finished, part of the solvent is removed to obtain the inhibitor.

Nano-organosilicon film-forming and hydrophobic shale surface hydration inhibitor and its preparation method and application

The present disclosure to a cementitious plugging wall solidifier for water-based drilling fluid and a preparation method thereof and a water-based drilling fluid.

Cementitious plugging wall solidifer for water-based drilling fluid, and a preparation method thereof and a water-based drilling fluid

The present discloses a water-based gel-consolidation type lost circulation material system suitable for fractured lost circulation formation, preparation method and use thereof.

Water-based gel-consolidation type lost circulation material system suitable for fractured lost circulation formation, preparation method and use thereof

A high-temperature resistant, high-strength, and thixotropic gel plugging agent is composed of 8-20% of acrylamide monomer, 0.05-0.5% of reactive polymer, 0.1-1.0% of organic polymer cross-linker, 3.0-8.0% of resin toughening agent, 1.0-5.0% of flow pattern regulator, 0.01-0.5% of cross-linking regulator by the weight in the water. The gel solution shows a low apparent viscosity during the shear flow and is easy to be pumped into the wellbore and then into the formation leakage layer; after the pumping stops, the gel solution shows rapidly increased viscosity and strong adhesive force, and form a high-strength barrier between the wellbore and the formation, preventing the drilling fluid from further leaking.

High-temperature resistant, high-strength, and thixotropic gel plugging agent and its preparation method and application

A high temperature-resistant and high oil-absorption resin particle plugging agent suitable for oil-based drilling fluid and its preparation method is prepared from raw materials in parts by mass as follows: 15-30 parts of reaction monomers, 5-12 parts of linear high polymers, 0.1-1.5 parts of cross-linking agents, 0.1-0.5 parts of initiators, 1-3 parts of modified starches, 1-5 parts of filler particles and 1-5 parts of dispersing agents; it has high oil absorption capacity under a high-temperature condition and high toughness after oil-absorbing expansion.

High temperature-resistant and high oil-absorption resin particle plugging agent suitable for oil-based drilling fluid and its preparation method

The present disclosure provides a preparation method of an environment-friendly high-temperature resistant water-based drilling fluid plugging anti-sloughing agent, the preparation method comprises the following steps: mixing and emulsifying a styrene monomer, an acrylic monomer and an emulsifier MS-1 aqueous solution to prepare a pre-polymerization emulsion; dispersing hydrophilic monomer, cationic monomer and an emulsifier MS-1 in water, adjusting the pH to be within a range of 6.5-8.5, then adding mixed monomers of the styrene monomer and acrylic monomer to blend and emulsify to prepare a post-polymerization emulsion; adding a first cross-linking agent and a first initiator into the pre-polymerization emulsion, uniformly dispersing the mixture and carrying out reaction; subsequently dropwise adding the post-polymerization emulsion, adding a second cross-linking agent and a second initiator, uniformly dispersing the mixture and then continuously carrying out reaction, drying and crushing the reaction product to prepare the plugging anti-sloughing agent.

Environment-friendly high-temperature resistant water-based drilling fluid plugging anti-sloughing agent, preparation method thereof and the water-based drilling fluid

The invention discloses a calcium-resistant zwitterionic polymer, a preparation method and an application thereof, and a water-based drilling fluid containing the polymer as a dispersing agent, wherein the polymer contains a structural unit A, a structural unit B and a structural unit C, and the structural unit A is at least one selected from the group consisting of structural units with a structure shown in a formula (11), a structure shown in a formula (12) and a structure shown in a formula (13); the structural unit B is a structural unit with a structure shown in a formula (2); the structural unit C is at least one selected from the group consisting of structural units having a structure represented by formula (31) and a structure represented by formula (32); the weight-average molecular weight of the polymer is 350,000 to 600,000. 

Calcium-resistant zwitterionic polymer, preparation method and application thereof, and water-based drilling fluid containing polymer as dispersant

The present disclosure relates to the technical field of oil and gas drilling, and particularly relates to a modified silicon dioxide material of a fluorocarbon active agent type super-amphiphobic cutting-carrying agent suitable for a water-based drilling fluid, and a preparation method thereof. The preparation method of the modified silicon dioxide material comprises the following steps: subjecting silicon dioxide and a silane coupling agent represented by Formula (1) to a first contact reaction in a mixed solvent containing alcohol and water; subjecting the product of the first contact reaction, the compound represented by Formula (2) and the compound represented by Formula (3) to a second contact reaction; subjecting the product of the second contact reaction and the compound represented by Formula (4) to a third contact reaction. The modified silicon dioxide material can be used as a cutting-carrying agent in a water-based drilling fluid and produce an excellent cutting-carrying effect. 

Modified silicon dioxide material of fluorocarbon active agent type super-amphiphobic cutting-carrying agent suitable for water-based drilling fluid and preparation method thereof

The present invention relates to the field of petrochemical drilling and discloses a drilling fluid additive composition. The composition contains an emulsifier and a rheological modifier. The emulsifier is one or more of the compounds represented by Formula (1); the rheological modifier is dimer acid-organic amine copolymer, comprising structural units from the dimer acid, structural units from the alkylamine and structural units from the arylamine. The present invention further provides a drilling fluid containing the foregoing composition. When a clay-free oil-in-water drilling fluid contains the drilling fluid additive composition of the present invention containing the emulsifier and rheological modifier, it may have high temperature resistance and high density; 

Drilling fluid additive composition and super high temperature super high density clay-free oil-in-water drilling fluid

The present invention relates to the field of petrochemical drilling and discloses a drilling fluid additive composition. The composition contains rheological modifier, emulsifier and tackifier. Among them, the rheological modifier is dimer acid-organic amine copolymer comprising structural units from dimer acid, structural units from alkylamine and structural units from arylamine; the tackifier is modified polysiloxane nano-particles, and the modifying group Z on the polysiloxane nano-particles is the emulsifier is one or more of the compounds represented by the following Formula (1). The present invention further provides a high temperature resistant clay-free whole-oil-based drilling fluid containing the foregoing composition. Through synergistic effect of the rheological modifier, the emulsifier and the tackifier in the composition, the present invention obtains a clay-free whole-oil-based drilling fluid with desirable suspending power and temperature resistance. 

Drilling fluid additive composition and high temperature resistant clay-free whole-oil-based drilling fluid

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Beijing, China

Xianbin Huang