Bodenseewerk Perkin-elmer Co.

Bodenseewerk Perkin-elmer Gmbh

Wolfgang Chlosta

Wolfgang Riegger

Rolf G Tamm

Toma Tomoff

Bernhard W Huber

Peter Pospisil

Klaus Joachim Braun

Henry Klemm

Heinz W Henninger

Viktor Lochle

Klaus Grossmann

Franz Eier

In a dosing device for analyzing apparatus, particulary for liquid chromatography, with a dosing loop, a change-over valve and a dosing needle (20) which can be introduced into a sample inlet (56) of the change-over valve (24), through which dosing needle (20) sample liquid can be dosed by means of a sample pump (66) into the sample inlet (56) and the dosing loop (22), the dosing needle (20) has a conical sealing surface (138) at its front end. The sample inlet (56) has a sample inlet passage (128) which forms a conical annular shoulder (136). The dosing needle (20) with its conical sealing surface (138) engages this annular shoulder (136) with a defined pre-stress.

Dosing device for analyzing apparatus

A needle is movable by a servomotor between a position of rest and an operating position in a stationary housing. The needle includes a tip and a first lateral opening close to the tip and a second lateral opening spaced therefrom. A longitudinal passage of the housing through which the needle is guided includes a pair of seals at the lower end and a seal at the upper end. A carrier gas conduit ends in the longitudinal passage axially inwards of the seals. A port communicating with atmosphere ends axially inwards of the upper seal. The arrangement permits a sample extraction from sample vessels closed by a membrane without the sample vessels having to be lifted and pressed against the needle.

Needle assembly for introducing a carrier gas into a sample vessel

A sample vessel container in a sampling device for use in gas chromatography includes a rotatable metal block having a circular array of axial bores for accommodating a plurality of sample vessels. A heating jacket operative as an electric heater is non-rotatably connected to a housing, which jacket tightly surrounds in material contact with, and is adapted to heat, the rotatable metal block.

Electric heater for a rotating sample vessel container in a sampling

A needle assembly for feeding a carrier gas into a sample vessel during the head-space analysis of a sample includes a lateral outlet passage for conveying the gas.

Needle assembly useful in the head-space method of gas chromatography

A plurality of samples subject to the same thermostatting time periods are directed one by one to the inlet section of a gas chromatograph for analysis in accordance with the head space method. To this end, a first heatable sample store adapted to be stepwise advanced is provided, in which thermostatting of the samples is accomplished. A second sample store also adapted to be stepwise advanced is provided, from which sample vessels are transferred one by one into the first sample store.

Sampler for feeding samples in gas chromatography

A sample feeding device includes a turntable driven by a servomotor and mounted on a carrier driven by a separate servomotor. The turntable servomotor and the carrier servomotor, as well as a movable intake tube, are controlled by a control device.

Sample feeding device

A graphite furnace for flameless atomic absorption spectroscopy comprising a graphite sample tube with a sample port at the mid-point of its length. Electrodes supportively contact the tube ends and pass electrical heating current through the tube. The electrodes have hollow cylindrical portions which laterally envelope the tube over substantially its entire length, one of the electrodes being longer than the other and containing a radial bore in registration with the sample port. The cylindrical portions of the electrodes are disposed with complementary-shaped recesses in cooling jackets which encase all but the mid-length regions of the electrode cylindrical portions. The electrodes fit readily in the cooling jackets at room temperature due to differential expansion of these members. The sample tube, electrodes, cooling jackets and associated structure are mounted on a base with provisions for adjustment of the tube about various orthogonal axes.

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Uberlingen, Germany

Wolfgang Chlosta