American Superconductor Corporation

Other

Puritan-bennett Corporation

William L Carter

Gilbert N Riley, Jr

Alexander Otto

Qi Li

Martin W Rupich

Eric R Podtburg

Elliott D Thompson

Patrick John Walsh

Lawrence J Masur

Mark D Teplitsky

Donald R Parker

William J Michels

William J Rosati

Michael A Tanner

Gregory L Snitchler

Craig J Christopherson

Ronald D Parrella

Peter D Antaya

Henry C Valcour, Iii

John Gannon

Subramaniam Anandakugan

Hong Cai

David Crotzer

Ronald D Parella

Theodore S Greene

David A Meadows

Dana Krause

Jay L Hayes

John S Voege

Henry C Valcour Iii

A sterile glove dispensing assembly includes a container for storing a plurality of sterile gloves. The container has a dispensing opening and the plurality of sterile gloves is strategically oriented that a cuff of each of the sterile gloves extends outwardly through the dispensing opening. In this way a user can draw the sterile gloves outwardly from the container without touching fingers of the sterile gloves for retaining sterility of the fingers. A box is included for insertably receiving the container and a dispensing slot is integrated into the box. The dispensing opening in the container is aligned with the dispensing slot when the container is positioned inside of the box thereby facilitating the sterile gloves to be drawn outwardly from the dispensing slot.

Sterile glove dispensing assembly

A rotating machine includes a stator and a rotor configured to rotate within the stator. Rotor windings are supported in the rotor and are formed of a laminated electrical conductor in a single-layer saddle coil configuration. The conductor includes a first support lamina, a second support lamina, an insert including a high temperature superconductor disposed between the first and second support lamina, and a filler material surrounding the insert that bonds the insert to each of the first and second support lamina. At the location between the first support lamina and second support lamina corresponding to the location of the insert, the width dimension of the filler material on each side of the insert is at least 10 percent of a width of the conductor. The conductor is configured to carry at least 600 Amperes per turn and have a C-axis tensile strength of at least 21 MPa.

Wide electrical conductor having high C-axis strength

A method includes locating a defect in a first segment of high temperature superconducting wire. A second segment of high temperature superconducting wire is then positioned onto the first segment of high temperature superconducting wire such that the second segment of high temperature superconducting wire overlaps the defect. A path is then created such that current flows through the second segment of high temperature superconducting wire. The first segment of high temperature superconducting wire and second segment of high temperature superconducting wire are then laminated together.

Mitigating the effects of defects in high temperature semiconductor wires

A method is described to prepare a highly textured oxide superconductor article in a single deformation-sinter process. A precursor article including a plurality of filaments comprising a precursor oxide having a dominant amount of a tetragonal BSCCO 2212 phase and a constraining member substantially surrounding each of the filaments is provided. Each of the filaments extends along the length of the article. The oxide article is subjected to a heat treatment at an oxygen partial pressure and temperature selected to convert a tetragonal BSCCO 2212 oxide into an orthorhombic BSCCO 2212 oxide and, thereafter, roll worked in a high reduction draft in a range of about 40% to 95% in thickness so that the filaments have a constraining dimension is substantially equivalent to a longest dimension of the oxide superconductor grains. The rolled article is sintered to obtain a BSCCO 2223 oxide superconductor.

Simplified deformation-sintering process for oxide superconducting articles

A novel process of the production and processing of high quality, high T (Bi,Pb)SCCO superconductors starts with fabrication of a precursor article including selected intermediate phases with desired chemical and structural properties. The precursor fabrication includes mixing raw powders with a desired ratio of Bi:Pb:Sr:Ca:Cu elements and reacting the mixture under different selected reaction conditions that form a precursor powder with a dominant (Bi, Pb)SCCO 2212 phase and without Ca&mdash;Pb&mdash;O phase, wherein the 2212 phase may be the orthorhombic 2212 phase. The precursor article is then subjected to optimized reaction and mechanical deformation processes that lead to a reaction induced texturing and deformation induced texturing, respectively. A heating process is used to convert the precursor powder to the 2223 phase and subsequent deformation and annealing processes may be used to form a substantially single phase, highly textured (Bi, Pb)SCCO 2223 superconductor with high Jc.

Production and processing of (Bi, Pb)SCCO superconductors

A novel process of the production and processing of high quality, high T BSCCO or (Bi,Pb)SCCO superconductors starts with fabrication of a forming a bundle including a plurality of billets, each billet containing at least one filament comprising a dominant amount of an tetragonal BSCCO phase with selected intermediate phases, and substantially surrounded by a constraining metal. The bundle is thermomechanically consolidated to form a multifilamentary precursor article by applying pressure and heat to the bundle under conditions cooperatively selected to cause interdiffusion of said constraining metal at the interfaces between said metal and said filaments and substantially complete elimination of voids in said bundle, and the consolidation step is completed before any high strain longitudinal deformation is performed on the bundle. The precursor article is then heated at a second selected processing temperature in an inert atmosphere with a second selected oxygen partial pressure for a second selected time period, the second processing temperature, the second time period and the second oxygen partial pressure being cooperatively selected to form a dominant amount of an orthorhombic BSCCO phase in the reacted mixture. It may then be deformed to form an elongated precursor article of a desired texture; and thereafter heated at a third selected processing temperature in an inert atmosphere with a third selected oxygen partial pressure for a third selected time period, all cooperatively selected to convert at least a portion of the orthorhombic BSCCO phase to the final superconducting BSCCO material.

Method of forming superconducting composite article

A method for preparing a BSCCO-2223 oxide superconducting article includes annealing an oxide superconductor article comprised of BSCCO-2223 oxide superconductor at a temperature selected from the range of about 500&deg; C.&lE;T&lE;787&deg; C. and an annealing atmosphere having an oxygen pressure selected from within the region having a lower bound defined by the equation, P (lower)&gE;3.5&times;10 exp(&minus;32,000/T&plus;273) and an upper bound defined by the equation, P (upper)&lE;1.1&times;10 exp(&minus;32,000/T&plus;273). The article is annealed for a time sufficient to provide at least a 10% increase in critical current density as compared to the critical current density of the pre-anneal oxide superconductor article. An oxide superconductor having the formula Bi Pb Sr Ca Cu O , where 0&lE;x&lE;1.5 and where 0&lE;y&lE;0.6 is obtained, the oxide superconductor characterized by a critical transition temperature of greater than 111.0 K, as determined by four point probe method.

Processing of oxide superconductors

A reduced coefficient of friction, preferably created by ideal lubrication conditions, may advantageously be employed in the breakdown deformation of a precursor to a multifilamentary superconducting composite, particularly in combination with one or more high reduction breakdown drafts, to improve composite homogeneity and significantly increase the range of deformation conditions over which dimensional tolerances and J may be optimized. Precursor composites made by this method exhibit reduced microhardness variability and fewer and less serious transverse filament defects than composites made by prior art methods. The method comprises the steps of: first, providing a precursor article comprising a metal matrix surrounding a plurality of filaments extending along the length of the article and comprising precursors to a desired superconducting ceramic; next, roll working the precursor article during a breakdown stage at a predetermined pressure and a coefficient of friction less than about 0.2, preferably less than 0.01, and preferably less than about 0.001 during each roll working draft, and, then, sintering the rolled article to obtain the desired superconducting ceramic. The coefficient of friction is preferably obtained by interposing a lubricant between the precursor article and one or more rolls, most preferably under conditions which create ideal lubrication conditions.

Method of making a multifilamentary super-conducting article

An aspected multifilamentary oxide article is provided having a plurality of aspected filaments including a metal oxide and extending continuously for the length of the article. A constraining member substantially surrounds each filament, wherein each of the filaments has an average transverse cross-sectional thickness less than about 35 &mgr;m and an average variation in cross-section along its length of less than about 10%. The article exhibits superior filament uniformity, hardness, and oxide density and texture.

High texture factor

A novel process of the production and processing of high quality, high T,(Bi,Pb)SCCO superconductors starts with fabrication of a precursor article including selected intermediate phases with desired chemical and structural properties. The precursor fabrication includes introducing the reacted mixture having a dominant amount of the tetragonal BSCCO phase into a metal sheath, and sealing the reacted mixture within said sheath, heating the mixture at a second selected processing temperature in an inert atmosphere with a second selected oxygen partial pressure for a second selected time period, the second processing temperature and the second oxygen partial pressure being cooperatively selected to form a dominant amount of an orthorhombic BSCCO phase in the reacted mixture. The sealed sheath is deformed to form an elongated precursor article of a desired texture; and thereafter heated at a third selected processing temperature in an inert atmosphere with a third selected oxygen partial pressure for a third selected time period. The third processing temperature and third oxygen partial pressure are cooperatively selected to convert at least a portion of the orthorhombic BSCCO phase to the final superconducting BSCCO material.

Processing of (Bi,Pb)SCCO superconductor in wires and tapes

A multicomponent powder useful in the formation of BSCCO-2223 is provided comprised of orthorhombic BSCCO-2212 and alkaline earth cuprate, without formation of undesirable secondary phases such as alkaline earth bismuthates and alkaline earth plumbates. A method for the production of the multicomponent powder includes providing a mixture of raw materials comprising constituent metallic elements in a ratio corresponding to a superconducting BSCCO-2223 material and heating the mixture under conditions which form a dominant amount of the orthorhombic BSCCO phase and the alkaline earth cuprate phase while preventing formation of an undesirable secondary phase selected from the group of alkaline earth plumbates and alkaline earth bismuthates. A subsequent heating step converts the multicomponent powder into the BSCCO-2223 and subsequent deformation and annealing processes may be used to form a substantially single phase, highly textured (Bi,Pb)SCCO-2223 superconductor article.

Production and processing of (Bi,Pb) SCCO superconductors

A method for preparing a BSCCO-2223 oxide superconducting article includes annealing an oxide superconductor article comprised of BSCCO-2223 oxide superconductor at a temperature selected from the range of about 500&deg; C.&lE;T&lE;787&deg; C. and an annealing atmosphere having an oxygen pressure selected from within the region having a lower bound defined by the equation, P,(lower)&gE;3.5&times;10,exp(&minus;32,000/T&plus;273) and an upper bound defined by the equation, P,(upper)&lE;1.1&times;10,exp(&minus;32,000/T&plus;273). The article is annealed for a time sufficient to provide at least a 10% increase in critical current density as compared to the critical current density of the pre-anneal oxide superconductor article. An oxide superconductor having the formula Bi,Pb,Sr,Ca,Cu,O,, where 0&lE;x&lE;1.5 and where 0&lE;y&lE;0.6 is obtained, the oxide superconductor characterized by a critical transition temperature of greater than 111.0 K, as determined by four point probe method.

The combination of one or more high reduction drafts with controlled, low back tensions increases the range of deformation conditions over which dimensional tolerances and J,may be optimized. The method comprises the steps of: first, providing a precursor article comprising a metal matrix surrounding a plurality of filaments extending along the length of the article and comprising precursors to a desired superconducting ceramic; next, roll working the precursor article during a breakdown stage at a back tension less than the elastic to plastic transition threshold of the composite during at least one high reduction roll working draft, and, then, sintering the rolled article to obtain the desired superconducting ceramic. In a preferred embodiment, the rolling step further comprises rolling the article at a front tension less than the elastic to plastic transition threshold of the rolled, unsintered article.

Tensioning process for manufacture of superconducting ceramic composite conductors

A novel process of the production and processing of high quality, high T.sub.c BSCCO or (Bi,Pb)SCCO superconductors starts with fabrication of a forming a bundle including a plurality of billets, each billet containing at least one filament comprising a dominant amount of an tetragonal BSCCO phase with selected intermediate phases, and substantially surrounded by a constraining metal. The bundle is thermomechanically consolidated to form a multifilamentary precursor article by applying pressure and heat to the bundle under conditions cooperatively selected to cause interdiffusion of said constraining metal at the interfaces between said metal and said filaments and substantially complete elimination of voids in said bundle, and the consolidation step is completed before any high strain longitudinal deformation is performed on the bundle. The precursor article is then heated at a second selected processing temperature in an inert atmosphere with a second selected oxygen partial pressure for a second selected time period, the second processing temperature, the second time period and the second oxygen partial pressure being cooperatively selected to form a dominant amount of an orthorhombic BSCCO phase in the reacted mixture. It may then be deformed to form an elongated precursor article of a desired texture; and thereafter heated at a third selected processing temperature in an inert atmosphere with a third selected oxygen partial pressure for a third selected time period, all cooperatively selected to convert at least a portion of the orthorhombic BSCCO phase to the final superconducting BSCCO material.

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Chelmsford, MA, United States of America

William L Carter