Kolene Corporation

Other

Kilene Corp.

William G Wood

John F Pilznienski

John M Cole

James Christopher Malloy

Robert H Shoemaker

Thomas M Jakubowski

James C Malloy

A composition and apparatus and method for aqueous spray conditioning of scale on metal surfaces. An aqueous solution having a base composition of an alkali metal hydroxide is used. The aqueous solution may contain additives to improve the performance of the salt. In one embodiment, the solution is used to condition the scale on a strip of stainless steel. The strip of steel is at a temperature between the melting point of the alkali metal hydroxide in anhydrous form and a temperature at which the Leidenfrost effect appears. One or more nozzles is provided to spray the solution, and the heated strip is passed by the nozzle or nozzles where the solution is sprayed on the surface or surfaces of the strip that have the scale or oxide. The invention also includes the apparatus and control thereof for the spraying of the solution.

Composition, apparatus, and method of conditioning scale on a metal surface

A composition and apparatus and method of using the composition for aqueous spray descaling or conditioning of scale or oxide on metal surfaces, especially stainless steel strip or the like, in one embodiment, although it can be used to descale or condition oxide or scale on other work pieces such as metal bar, or even discrete objects. An aqueous solution having a base composition of an alkali metal hydroxide, such as sodium hydroxide, potassium hydroxide, or a mixture of alkali metal hydroxides such as sodium hydroxide and potassium hydroxide is used. The aqueous solution may contain certain additives to improve the descaling performance of the salt. In one embodiment, the solution is used to condition the scale or surface oxide on a strip of stainless steel. The strip of steel is at a temperature between the melting point of the alkali metal hydroxide in anhydrous form and a temperature at which the Leidenfrost effect appears. One or more nozzles is provided to spray the solution, and the heated strip is passed by the nozzle or nozzles where the solution is sprayed on the surface or surfaces of the strip that have the scale or oxide. The invention also includes the apparatus and control thereof for the spraying of the solution.

According to the present invention a saturated aqueous solution comprising at least one alkali metal hydroxide and at least one alkali metal nitrate is provided which can be spray added to a fused anhydrous bath which contains alkali metal materials.

Aqueous solution of alkali metal compositions

A method and apparatus is disclosed for prevention of clogging of exhaust systems, especially the exhaust hoods and ducts above fused salt baths onto which salts splatter as they are being added by spraying from aqueous solutions. A fluid tight jacket surrounds a portion of the exhaust pipe and hood and a cooling fluid, preferably the aqueous solution of the salt being added is flowed through the jacket. This will condense the water of the solvent onto the inside of the hood and duct dissolving and washing away any splattered salt.

Method and apparatus for prevention of clogging of exhaust systems

A process for case hardening steel is described. A fused bath of inert salt is maintained which bath is comprised of alkali or alkali earth halides, and alkali, or alkaline earth oxides or carbonates. To this fused bath is added urea, dicyanodiamide or pyrolysis/condensation products of urea or dicyanodiamide. This will form active ions containing carbon and/or nitrogen, and either the nitrogen and/or carbon will diffuse into the surface of a steel piece suspended in the bath to form either a nitride, carbonitride or carburized case depending upon the temperature of the bath, which is maintained between above 540.degree. C. and about 950.degree. C.

Process for case hardening steel

A method and composition is disclosed for removing oxide film from metals and alloys and for detersification of objects. The composition is at least a 1% aqueous solution of gluconic acid or its alkali metal including ammonium salts, citric acid or its alkali metal including ammonium salts, and tartaric acid or its alkali metal including ammonium salts, at least one of these materials being acid in sufficient strength to provide a pH of 4 or less. Also, preferably a non-ionic surfactant is included.

Method for detersifying and oxide coating removal

A method and apparatus is disclosed where aqueous solutions of chemicals are added to fused non-aqueous baths. This is done by spraying the aqueous solution of the chemicals onto the surface of the fused bath in a fine spray, causing the evaporation of the water.

Liquid additions to fused chemical baths

A ferrous metal product to be cleaned is immersed in an oxidizing molten salt bath forming a conditioned scale on the surface of the metal. The conditioned scale is subsequently removed from the metal surface by immersing the metal product in an aqueous caustic bath containing alkali metal hydroxide with alkali gluconate and triethanolamine serving as sequestering agents. The caustic bath may optionally include a brightening catalyst or ethylenediamine-tetracetic acid.

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Grosse Pointe Farms, MI, United States of America

William G Wood