Kerr-mcgee Chemical, LLC

Kerr-mcgee Corporation

Wilbert J Robertson

Robert E Davis

Michael F Lucid

Paul D Bowerman

Roger C Shaw

Sodium metaborate is recovered from a boron-containing first feed solution by extraction of the first feed solution with a 1,3-diol, followed by re-extraction with a solution of an alkali metal hydroxide. Boric acid is recovered from a boron-containing second feed solution by extraction of the second feed solution with a water-insoluble aromatic polyol, followed by re-extraction with mineral acid. The boric acid and sodium metaborate are reacted to form sodium tetraborate. By exchanging sodium ions in the polyol extract with potassium ions, the potassium salts of the mineral acid may be recovered from the polyol as a by-product.

Borax recovery using sodium metaborate and boric acid intermediates

A process for preparing manganese sulfate solutions having reduced concentrations of potassium impurity is disclosed wherein a digestion mixture of a reduced manganese ore, a source of water soluble aluminum ions, a source of water soluble ferric ions and an aqueous acid solution is prepared, having a solution pH ranging from about 0.5 to about 3.5. The mixture is then digested at a temperature sufficient to produce a mixed digestion product comprising a liquid phase of a manganese sulfate solution and a solid phase of digested ore residue and a particulate complex salt by-product. The liquid phase of manganese sulfate solution is then recovered from the mixed digestion product. An additional feature of this process involves conducting the digestion of the digestion mixture in the presence of at least one complex salt of the general formula:

Process of producing manganese sulfate solutions

A process for the simultaneous coextraction of uranium and vanadium from an aqueous acidic solution containing the same comprising contacting said aqueous acidic solution with an organic phase comprising a mixture of (a) an alkyl substituted diaryl phosphoric acid, (b) a trialkylphosphine oxide compound, and (c) an organic diluent whereby the uranium and vanadium are coextracted into the organic phase and thereafter recovering the uranium and vanadium from the organic phase.

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Oklahoma City, OK, United States of America

Wilbert J Robertson