Cabot Corporation

Viren M Pathare

James Allen Fife

Roger W Steele

Hongju Chang

Bhamidipaty K Rao

Lee M Ruch

Prabhat Kumar

David A Knudson

A capacitor having a central electrode body having sintered metal anode with an electrode lead, the anode having a sintered product produced from a tantalum powder having deagglomerated particles such that the product of the volume mean diameter in microns multiplied by the specific surface area measured in m.sup.2 /g is a number in the range of below about 25. Capacitors having a central electrode with the anode produced from a sintered product produced from a heat treated and oxidized tantalum powder wherein the oxidized particle size is greater than about 0.7 m.sup.2 /g. Capacitors are defined in terms of anodes produced from powders having specified ratios of Scott Bulk Density to surface area or ratio of die fill rate to surface area.

Tantalum metal power with controlled size distribution and products made

A process for sizing (i.e., comminuting) a tantalum powder including agglomerates of smaller particles, which process yields a tantalum powder having an as-comminuted agglomerate size distribution with the product of the Volume Mean Diameter, MV (in microns as measured by light scattering techniques such as Microtrac analysis), times specific surface area, BET (m.sup.2 /g), being less than about 25. These powders after sizing typically have ratios of Scott Bulk Density : BET Surface Area in the range from about 20 to about 35. Also provided are powders having a substantially unimodal and narrow agglomerate size distribution in all stages of production, namely after sizing (i.e., deagglomeration by comminution), thermal agglomeration (i.e., heat treatment), and deoxidation. These resultant powders have high surface area and good flowability properties and, upon sintering, exhibit controlled shrinkage with high porosity. Further provided are sized heat treated tantalum powders having agglomerate particle sizes wherein the product of the Volume Mean Diameter, MV, times the specific surface area, BET, is in the range from about 90 to about 250. Sized and agglomerated powders which are deoxidized are also provided wherein the product of the Volume Mean Diameter, MV, times the specific surface area, BET, is in the range from about 90 to about 250.

Method of making tantalum metal powder with controlled size distribution

Tantalum electrode material is produced which has extremely low tortuosity, exceptionally low ESL and ESR, potentially extended high frequency performance, very high volumetric efficiency, and reduced tantalum consumption per electrode. The electrode material is characterized by having a cross-section composed of plates of tantalum separated by spaced gaps resulting in a highly dense (volumetric efficiency) electrode. The plates are electrically interconnected which also adds to the structural stability of the article. This is made possible by being able to carefully control the geometry of the tantalum material during processing. A method for producing such material includes extruding a billet filled with a (preferentially geometrically uniform) mixture of rods of tantalum and an extrudable metal. When the billet has been sufficiently reduced in size and severed, the extrudable metal is removed by selectively dissolving with acid. In addition to the above advantages, the resulting article is particularly adapted for use in super-miniaturization applications.

Extruded capacitor electrode and method of making the same

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Viren M Pathare