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Gneuss Kunststofftechnik Gmbh

Ulrich Thiele

Donald R Kelsey

Robert Lawrence Blackbourn

Detlef Gneuss

Eckhard Seidel

Fritz Wilhelm

Hans Reitz

Robert Stephen Tomaskovic

Klaus Mackensen

Process of producing polytrimethylene terephthalate (PTT) by esterification of terephthalic acid (TPA) with trimethylene glycol (TMG) in the presence of a catalytic, titanium compound, precondensation and polycondensation. The esterification is effected in at least two stages, where in the first stage a molar ratio of TMG to TPA of 1.25 to 2.5, a content of titanium of 0 to 40 ppm, a temperature of 245 to 260&deg; C. as well as a pressure of 1 to 3.5 bar are adjusted. In the at least one subsequent stage a content of titanium is adjusted which is higher than in the initial stage by 35 to 110 ppm. For generating the vacuum in the polycondensation and in the precondensation, there are used vapor jet pumps operated with TMG vapor.

Process for producing polytrimethylene terephthalate (PTT)

A multipath valve for distributing and/or dividing at least one flow of polymer melt during the manufacture and processing thereof, wherein melt flows through all internal chambers of the valve during all conditions of operation. At least one rotary disc is rotatably mounted on an axle bolt between a front plate and a rear plate which are each provided with openings serving as inlets and outlets for the polymer melt. The rotary disc is provided with circular segment-shaped ducts having a width and end radii corresponding to an inner width of the openings, wherein the ducts have center lines which are located on a reference circle extending through the centers of the openings, and wherein the positions of the ducts are adjustable in accordance with a desired flow direction of the polymer melt.

Multipath rotary disc valve for distributing polymer plastics melts

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Bruchköbel, Germany

Ulrich Thiele