Suncoal Industries Gmbh

Valmet Technologies Oy

Koehler Innovation & Technology Gmbh

Tobias Wittmann

Klaus Bergemann

Panu Tikka

Henrik Wallmo

Eric Enqvist

Bernhard Schwaiger

Jacob Podschun

Isabella Richter

Gerd Schmaucks

Ulf Lüder

Christian Von Olshausen

Anders Littorin

Bodo Max Wolf

Ville Tarvo

Geertje Dautzenberg

Alexander Stücker

Lenz Aron Mathis KÖHL

Bodo M Wolf

Jakob Podschun

The invention relates to fine particulate carbon material, and to a method of production and the use thereof.

Modified fine particulate carbon materials and method for producing same

The invention relates to a method for producing a crosslinked lignin in particle form using a hydrothermal treatment of a liquid, which is made of black liquor, contains lignin and a crosslinker or a precursor thereof, and has an electrical activity ranging from more than 15 mS/cm, preferably more than 25 mS/cm, to 400 mS/cm, and to the crosslinked lignin produced using the aforementioned method. The invention additionally relates to crosslinked lignin particles which have a glass transition temperature Tg of at least 160° C. or no glass transition temperature and an STSA surface area of at least 10 m/g and to rubber articles, in particular technical rubber articles or tires, which comprise crosslinked lignin particles as a filler.

Method for producing a crosslinked lignin with a highly specified surface area, crosslinked lignin, and technical rubber articles or tires comprising crosslinked lignin

It is provided a method for reducing the odor of particulate carbon materials and to the materials obtained thereby.

Method for odor reduction of particulate carbon materials

The present invention relates to a particulate carbon material that can be produced from renewable raw materials, in particular from biomass containing lignin, comprising: a 14C content that corresponds to that of the renewable raw materials, said content being preferably greater than 0.20 Bq/g carbon, especially preferably greater than 0.23 Bq/g carbon, but preferably less than 0.45 Bq/g carbon in each case; a carbon content in relation to the ash-free dry substance of between 60 ma. % and 80 ma. %; an STSA surface area of the primary particles of at least 5 m2/g and at most 200 m2/g; and an oil absorption value (OAN) of between 50 ml/100 g and 150 ml/100 g. The present invention also relates to a method for producing said carbon material and to the use thereof.

Hydrothermal treatment of renewable raw material

The present invention relates to a particulate carbon material that can be produced from renewable raw materials, in particular from biomass containing lignin, comprising: aC content that corresponds to that of the renewable raw materials, said content being preferably greater than 0.20 Bq/g carbon, especially preferably greater than 0.23 Bq/g carbon, but preferably less than 0.45 Bq/g carbon in each case; a carbon content in relation to the ash-free dry substance of between 60 ma. % and 80 ma. %; an STSA surface area of the primary particles of at least 5 m/g and at most 200 m/g; and an oil absorption value (OAN) of between 50 ml/100 g and 150 ml/100 g. The present invention also relates to a method for producing said carbon material and to the use thereof.

Particulate carbon material producible from renewable raw materials and method for its production

The present invention relates to a particulate carbon material that can be produced from renewable raw materials, in particular from biomass containing lignin, comprising: a MC content that corresponds to that of the renewable raw materials, said content being preferably greater than 0.20 Bq/g carbon, especially preferably greater than 0.23 Bq/g carbon, but preferably less than 0.45 Bq/g carbon in each case; a carbon content in relation to the ash-free dry substance of between 60 ma. % and 80 ma. %; an STSA surface area of the primary particles of at least 5 m/g and at most 200 m/g; and an oil absorption value (OAN) of between 50 ml/100 g and 150 ml/100 g. The present invention also relates to a method for producing said carbon material and to the use thereof.

Products extracted from black liquor include undissolved carbonized lignin and carbonized black liquor. The products further include solid carbon separated from the black liquor. Black liquor from an alkaline fractionation process is subjected to a hydrothermal carbonization process. Undissolved carbonized lignin is separated from the carbonized black liquor. The remaining carbonized black liquor is fed back into the alkaline fractionation process. The undissolved carbonized lignin is separated from the carbonized black liquor and purified.

Products extracted from black liquor

A process for recovering carbonized lignin having a defined grain size distribution from a lignin-containing liquid is provided. The lignin-containing liquid is subjected to a hydrothermal carbonization to convert the lignin into a carbonized lignin and the carbonized lignin is separated from the liquid containing the carbonized lignin. The lignin-containing liquid is subjected to a hydrothermal carbonization at temperatures in the range from about 150&#xb0; C. to about 280&#xb0; C. and by adapting the H+ ion concentration in the lignin-containing liquid before and/or during the hydrothermal carbonization the grain size distribution of the carbonized lignin is adjusted.

Method for obtaining stabilized lignin having a defined particle-size distribution from a lignin-containing liquid

Lignin-rich starting material is suspended in a first medium, which is acidic and aqueous, to form a aqueous acidic suspension, which is heated and allowed to form two continuous phases, a thermoplastic lignin phase and an aqueous phase. The thermoplastic lignin phase is separated from the aqueous phase and passed through a shape giving process into a second medium which is at a temperature lower than that of the thermoplastic lignin phase and in which the thermoplastic lignin phase is essentially insoluble. Solid lignin formed in the second medium is recovered.

Method for producing solid lignin

The invention relates to a method for extracting undissolved carbonized lignin from black liquor and products produced thereby. The invention further relates to the solid carbon thus extracted and the carbonized black liquor separated from said solid carbon. According to the invention black liquor from an alkaline fractionation process is subjected to a hydrothermal carbonization process, an undissolved carbonized lignin is separated from the carbonized black liquor, the remaining carbonized black liquor is fed back into the alkaline fractionation process, and the undissolved carbonized lignin is separated from the carbonized black liquor is purified.

Method for extracting lignin from black liquor and products produced thereby

The invention relates to a method for the treatment of process water which is obtained in a plant for the hydrothermal carbonization of renewable raw materials and organic residual materials by an evaporation of process water, a condensation of the washed process steam, and a biological treatment of the process steam condensate as partial quantity or possibly as total quantity of the amount of waste water discharged from an HTC plant.

Method for treating process water from a plant for the hydrothermal carbonisation of renewable raw materials and organic residues

The present invention relates to a continuous method for the hydrothermal carbonization of renewable raw materials and organic residues, in which, in a first processing stage, a pressure increase essentially to the pressure level of the carbonization occurs, in the second processing stage, the carbonization, which is performed at a pressure of at least 5 bar and at most boiling temperature, the obtained carbonized product is at least partially settled as sediment, and the filling height of the water in the second processing stage is set by removing water, and the temperature of the sediment delivered from the second processing stage is reduced by the vaporization of water and it is supplied to the third processing stage, drying which is heated using steam, in which the drying is performed in steam atmosphere, and subsequently discharged from the process.

Growing community of inventors

Berlin, Germany

Tobias Wittmann