United Technologies Corporation

Thomas T Field

Richard W Salkeld

Earle A Ault

Nicholas E Ulion

Otis Y Chen

Roger B Sines

Thomas A Murrin

Patrick F Papineau

Arthur R Geary

Unwanted recrystallization during heat treatment of a directionally solidified nickel alloy single crystal casting is prevented by chemical milling the part before heat treatment. Removal of a layer of as little as 0.013-0.050 mm thick, less than two percent of the part thickness, has been found effective.

Preparation of single crystal superalloys for post-casting heat treatment

A heat treatment is described for producing a desired microstructure in Hastelloy Alloy X components which have small diameter, closely spaced, laser pierced holes therein. The heat treatment produces a small grain size and discontinuous carbide morphology in the component prior to the hole piercing operation, which reduces the propensity for cracking which has been found to be associated with the hole piercing operation. After the piercing operation, the component is heat treated again to increase the grain size and produce a microstructure which provides the optimum balance of creep strength and fatigue strength.

Thermal treatment of wrought, nickel base superalloys in conjunction

Concepts relating to the heat treatment of single crystal superalloy articles are disclosed. A first concept is the use of a heat treatment sequence which includes incipient melting of the article being heat treated followed by one or more steps which essentially heal the incipient melting damage. A second concept relates to the treatment of previously heat treated single crystal articles which have incipient melting. Methods are disclosed for healing this damage and for recovering the mechanical properties of such articles. A third concept disclosed is a particular cycle which permits effective heat treatment of a specific single crystal alloy composition.

Heat treatment of single crystals

The weld zone in Hastelloy X nickel superalloy is thermal mechanically worked by cold working the weld zone to reduce its thickness by about 5-40%, and by annealing at 1120.degree.-1175.degree. C. for one hour to cause recrystallization. Low cycle fatigue properties of laser and gas tungsten arc weld zones are substantially increased.

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Killingly, CT, United States of America

Thomas T Field