E.i. Dupont De Nemours and Company

Thomas A J Schweiger

Hyunkook Shin

Chien-Ping Chai Kao

An azeotropic mixture of perfluorobutylethylene and at least one of the group consisting of bromochloromethane, cyclopentane, cis-1,2 dichloroethylene, trans-1,2 dichloroethylene and dichloromethane useful for cleaning agents, blowing agents and certain of which are suitable for flash spinning of polyolefins to make plexifilamentary fibers.

Azeotrope mixtures with perfluorobutylethylene

A process for flash-spinning a web of plexifilamentary film-fibril strands of synthetic fiber-forming polymer and laying down the web to form a nonwoven batt material therefrom is provided. The process includes the the step of generating a spin fluid consisting essentially of synthetic fiber-forming polymer and a spin agent, wherein the spin agent is comprised of at least 80% by weight, based on the total weight of the spin agent, of hydrocarbons comprised substantially exclusively of carbon and hydrogen atoms. The hydrocarbons are comprised of at least 25% by weight of unsaturated hydrocarbons having 4-8 carbon atoms. The process further includes the steps of flash-spinning the spin fluid at a pressure that is greater than the autogenous pressure of the spin fluid into a spin cell maintained at lower pressure to form a web of plexifilamentary film-fibril strands of said synthetic fiber-forming polymer, applying an electrostatic charge to the web by passing the web through an electric corona, and laying the web onto a grounded surface to form a batt of plexifilamentary film-fibril strands that is suitable for being consolidated into a sheet.

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Fayetteville, AR, United States of America

Thomas A J Schweiger