Pacific Consolidated Industries, LLC

Air Products and Chemicals, Inc.

Tarik Naheiri

Jason M Burns

William K Goshay

Ravi Kumar

Charles F Watson

Charles Franklin Watson

Javier Lopez

Rakesh Agrawal

Mark Parral

Sören Schmitz

Jochen Rainer Fischer

Dave Scheierl

Robert Wimmer

Dave White

Gary Swiniarski

Mark Baker

Shivaji Sircar

William T Kleinberg

James Yang

Paul Joseph Helterline

Steven Wilson Schellhase

Thomas J Saari

Steve Schellhase

The adsorber vessel is configured for radial flow between a center column and a perimeter manifold. Space between the center column and the perimeter manifold contains adsorption media. End caps close off ends of the vessel. An inlet and an outlet are configured within one of the end caps to feed starting gas into the center column or perimeter manifold, and to draw off product gas from the perimeter manifold or center column. An end cap can be removed to provide access for media loading between the center column and the perimeter manifold. Media is preferably provided within cartridges which can slide into this media space. Cartridges can be concentric with one cartridge inboard of the other, or can be stacked vertically. A spring plate can be provided on an open end to hold the media in position, while sealing the open end of the adsorber vessel.

Radial flow adsorber vessel for gas separation

The adsorption based air separation unit includes an adsorber vessel containing media which selectively adsorbs water vapor and nitrogen preferentially over oxygen. The vessel includes an air entry spaced from an oxygen discharge. At least one dry air tap from the adsorber vessel is located between the entry and the discharge. When the adsorption media is fresh, air entering the adsorber vessel passes through enough of the adsorber vessel to have much of its water vapor removed and only some of its nitrogen removed. The vessel can include multiple taps sequentially further from the entry which can be selectively opened as the adsorption media becomes saturated with water vapor and nitrogen, so that dry air with much of its nitrogen still present can be further tapped from the adsorber vessel. The adsorber vessel thus facilitates production of both oxygen and dry air, such as for use as medical grade air.

Adsorption air separator with dry air tap

An air separation unit includes an air inlet with a reversible blower downstream therefrom and an adsorption bed filled with adsorption media downstream of the reversible blower. The adsorption bed contains an adsorption media which preferentially adsorbs nitrogen over oxygen. An oxygen and argon output is located downstream of the absorption bed. At least a portion of the mixed gas of oxygen and argon is routed to a modular argon separator which separates out at least a portion of the argon to provide high purity oxygen to a high purity oxygen outlet. The argon separator can be configured as a molecular sieve filter to separate the argon from the oxygen or the argon separator can be in the form of a gas cooler and condenser which condenses liquid oxygen for storage and discharge as substantially pure oxygen.

High purity adsorption air separation unit

A driving system for a reversing blower adsorption based air separation unit is configured to not only drive the reversing blower cyclically in a forward and in a reverse direction, but also to allow the reversing blower to coast during a portion of its operating cycle. While coasting, a pressure differential across the blower acts alone to switch the reversing blower between a forward and a reverse direction of operation. Less power is thus required. When coasting, the blower can also be configured to output power such as the drive motor functioning as an electric generator or by having a mechanical power input be driven by the blower for power generation and/or energy storage. Such a system beneficially utilizes the energy associated with the pressure differential across the blower for energy harvesting and to further accelerate cycle times for the reversing blower adsorption based air separation unit.

Reversing blower adsorption utilizing coasting

An exemplary single bed reversing blower adsorption based air separation unit is configured to follow the Oload placed thereon by adjusting flow rates therethrough and power consumption. At least one and preferably multiple pressure sensors sense Opressure within an Ostorage region downstream of an adsorber vessel. These sensed pressures are utilized to generate control signals controlling flow rates at locations upstream of the compressor, such as at a reversible blower and an output compressor. Control loops for the blower and the compressor are independent of each other and have different time constants. Effective following of the Oload is thus achieved without driving the air separation unit into operational conditions outside of design and also maintaining optimal power consumption for the Oproduced, such that efficiency is maintained over a large turndown ratio.

Load following single bed reversing blower adsorption air separation system

The air separation unit includes a single adsorption bed downstream of a reversing blower and configured to operate on the principle of vacuum swing adsorption. An optimal ambient air pressure to vacuum pressure ratio within an adsorber vessel downstream of the reversible blower is identified. When the air separation unit is operated at ambient conditions where ambient air pressure is different, such as at higher altitude (or lower altitude) a pressure ratio across the blower when drawing a vacuum on the adsorption bed is maintained for optimal blower power to oxygen production performance. Time for recovery of the adsorption bed can also be modified due to the lower absolute pressure achieved within the adsorption bed when the pressure ratio across the blower is maintained. An ASU is thus provided which is optimized for performance at various different altitudes without requiring modification of equipment within the ASU.

Ambient pressure optimizing of SBRB VSA ASU

A multi-unit system combines multiple single bed reversing blower vacuum swing adsorption air separation units together. The units feed a common Osupply such as a system buffer tank. Demand is monitored and a number of individual units are brought online sufficient to meet demand. If demand exceeds supply, a further unit is brought online. If demand drops below supply by an amount greater than output of a single unit, then a longest operating unit is taken offline. The multi-unit system thus meets demand through utilization of multiple separate units in a highly redundant and highly reliable and scalable fashion.

Method and system for high reliability oxygen supply from multiple units

A mixed gas is separated with collection of at least one constituent gas. An inlet leads to a blower or other gas compression element through a valve. This blower feeds a chamber which contains media which selectively adsorbs the constituent gas to be collected, such as nitrogen from air. An exhaust from the chamber leads to an exhaust through a check valve. The blower can be reversed after nitrogen has been adsorbed within the chamber to desorb nitrogen and deliver nitrogen back through the blower. The inlet valve is closed after blower reversing and a separate diversion pathway is opened so that nitrogen is delivered from the blower to a nitrogen collection region. A variant system also includes an oxygen collection region on a side of the chamber opposite the blower for collection of both nitrogen and oxygen separated from air simultaneously, or collection of other constituent gases.

Nitrogen and oxygen separation using vacuum swing adsorption

The flow of gas between two vessels, each of which undergoes cyclic changes in gas pressure, is controlled by two check valves installed in parallel between the vessels. The first check valve allows gas to flow from the first vessel to the second vessel when the differential pressure between the vessels exceeds a first value, and the second check valve allows gas to flow from the second vessel to the first vessel when the differential pressure between the vessels exceeds a second value. The gas flow control method is particularly useful in pressure swing adsorption processes.

Pressure swing adsorption gas flow control method and system

A PSA process and system utilizes a combination of cyclic feed, evacuation, purge, and repressurization steps to provide a final gas product enriched in one of the feed components. The process is carried out in a simple system which utilizes a single two-way four-port valve for controlling gas flow between an adsorber vessel and a blower, and the blower is used for the introduction of feed gas into the adsorber and the evacuation of gas from the adsorber. The control of gas flow in either direction between the adsorber vessel and a product gas storage tank is accomplished by two check valves installed in parallel between the vessel and the tank.

Single bed pressure swing adsorption process and system

Process and single-bed pressure swing adsorption system for separating gas mixtures, especially air. The process includes a simultaneous countercurrent product purge and partial product repressurization step which shortens cycle time and improves overall system operation.

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Dana Point, CA, United States of America

Tarik Naheiri