General Electric Company

Diamond Innovations. Inc.

Momentive Performance Materials Gmbh

Bellataire International, LLC

Other

Suresh Shankarappa Vagarali

Thomas R Anthony

Mark Philip D'Evelyn

John William Lucek

Steven William Webb

William Edwin Jackson

Alan Cameron Smith

William Frank Banholzer

John Kieran Casey

Lionel M Levinson

Stephen Daley Arthur

Dong-Sil Park

Robert Arthur Giddings

Kristi Jean Narang

Larry Burton Rowland

Steven Alfred Tysoe

George Rene Kaplan

Robert Vincent Leonelli, Jr

Yavuz Kadioglu

Joel Rice Dysart

Robert C DeVries

Abhijit Prabhakar Suryavanshi

Biju Varghese

Stephen Lee Dole

Zheng Chen

David Charles Pender

Christian James Truemner

Bobby G Hoyle

Adamos Dalis

Mark Philip D'evelyn

A superabrasive compact and a method of making the superabrasive compact are disclosed. A method of making a superabrasive compact includes the steps of providing a plurality of superabrasive particles; subjecting the plurality of superabrasive particles to conditions of a first elevated temperature and pressure; and crushing the plurality of superabrasive particles into a pill under the first elevated high pressure and high temperature.

High-density polycrystalline diamond

Cutting elements having a substrate and a layer of superhard material sintered to the substrate are disclosed. The layer includes a working surface at a first surface. From the interface of the layer with the substrate, a reaction zone extends into the layer toward the working surface and a binder metal depletion zone extends into the substrate toward a base surface. The layer of superhard material has a composition including chromium or an alloy thereof. Also disclosed is an abrasive compact having a body with a composition including (i) a superhard material, (ii) a metal from a grain growth inhibitor or a metal from a metallic carbide other than WC, and (iii) an iron group binder metal. Cutting elements incorporating the abrasive compact, and drill bits incorporating abrasive compacts and cutting elements are also disclosed as well as methods of manufacture and methods of cutting material.

Abrasive compact of superhard material and chromium and cutting element including same

A method for removing defects at high pressure and high temperature (HP/HT) or for relieving strain in a non-diamond crystal commences by providing a crystal, which contains defects, and a pressure medium. The crystal and the pressure medium are disposed in a high pressure cell and placed in a high pressure apparatus, for processing under reaction conditions of sufficiently high pressure and high temperature for a time adequate for one or more of removing defects or relieving strain in the single crystal.

Method for reducing defect concentration in crystals

A capsule for containing at least one reactant and a supercritical fluid in a substantially air-free environment under high pressure, high temperature processing conditions. The capsule includes a closed end, at least one wall adjoining the closed end and extending from the closed end; and a sealed end adjoining the at least one wall opposite the closed end. The at least one wall, closed end, and sealed end define a chamber therein for containing the reactant and a solvent that becomes a supercritical fluid at high temperatures and high pressures. The capsule is formed from a deformable material and is fluid impermeable and chemically inert with respect to the reactant and the supercritical fluid under processing conditions, which are generally above 5 kbar and 550&#xb0; C. and, preferably, at pressures between 5 kbar and 80 kbar and temperatures between 550 &#xb0; C. and about 1500&#xb0; C. The invention also includes methods of filling the capsule with the solvent and sealing the capsule, as well as an apparatus for sealing the capsule.

High temperature high pressure capsule for processing materials in supercritical fluids

The present invention is directed to a method for changing the color of colored natural diamonds. The method includes placing a discolored natural diamond in a pressure-transmitting medium which is consolidated into a pill. Next, the pill is placed into a high pressure/high temperature (HP/HT) press at elevated pressure and elevated temperature for a time sufficient to improve the color of the diamond. The diamond may be exposed at elevated-pressure and elevated-temperature conditions within the graphite-stable region of the carbon-phase diagram&#x2014;without significant graphitization of the diamond, or above the diamond-graphite equilibrium and within the diamond-stable region of the carbon-phase diagram. Finally, the diamond is recovered from said press. Colorless Type Ia and Type II diamonds may be made by this method.

High pressure/high temperature production of colorless and fancy-colored diamonds

The present invention is directed to a method for treating discolored natural diamond, especially Type IIa diamond and Type IaA/B diamond with nitrogen as predominantly B centers, for improving its color. The method includes preblocking and preshaping a discolored natural diamond to prevent its breakage in a high pressure/high temperature (HP/HT) press, placing said discolored natural diamond in a pressure transmitting medium which is consolidated into a pill. Next, the pill is placed into a HP/HT press at elevated pressure and elevated temperature within the graphite-stable or diamond-stable range of the carbon phase diagram for a time sufficient to improve the color of said diamond. Finally, the diamond is recovered from said press. Colorless and fancy colored diamonds can be made by this method.

High pressure and high temperature production of diamonds

Method for reducing defect concentrations in crystals

A capsule for containing at least one reactant and a supercritical fluid in a substantially air-free environment under high pressure, high temperature processing conditions. The capsule includes a closed end, at least one wall adjoining the closed end and extending from the closed end; and a sealed end adjoining the at least one wall opposite the closed end. The at least one wall, closed end, and sealed end define a chamber therein for containing the reactant and a solvent that becomes a supercritical fluid at high temperatures and high pressures. The capsule is formed from a deformable material and is fluid impermeable and chemically inert with respect to the reactant and the supercritical fluid under processing conditions, which are generally above 5 kbar and 550&#xb0; C. and, preferably, at pressures between 5 kbar and 80 kbar and temperatures between 550&#xb0; C. and about 1500&#xb0; C. The invention also includes methods of filling the capsule with the solvent and sealing the capsule, as well as an apparatus for sealing the capsule.

A method of forming at least one single crystal of a Group III metal nitride. The method includes the steps of: providing a flux material and a source material comprising at least one Group III metal selected from the group consisting of aluminum, indium, and gallium, to a reaction vessel; sealing the reaction vessel; heating the reaction vessel to a predetermined temperature and applying a predetermined pressure to the vessel. The pressure is sufficient to suppress decomposition of the Group III metal nitride at the temperature. Group III metal nitrides, as well as electronic devices having a Group III metal nitride substrate formed by the method are also disclosed.

High pressure high temperature growth of crystalline group III metal nitrides

A jadeite material has a thickness in excess of about 1.0 mm and CIELAB indices of L*&#x3e;42, a*&#x3c;&#x2212;6, and b*&#x3e;+6. The grain size of the jadeite material is less than about 30 microns and is an equiaxed grain structure. The jadeite material has an optical transmission peak between 500 and 565 nm with an I/Ioptical transmission ratio of over 40%. The first step in making the jadeite material is to wrap a glass block, convertible by HP/HT into jadeite and having a nominal composition of NaAlSiO, with a graphite or refractive metal sheet. The wrapped glass block is placed in an HP/HT apparatus, rapidly heated, and subjected therein to a pressure in excess of about 3 GPa and a temperature in excess of about 1000&#xb0; C. for a time adequate to convert the glass block into jadeite. The jadeite material then is cooled and the pressure subsequently released.

Jadeite and its production

Polycrystalline gallium nitride (GaN) characterized by having the atomic fraction of gallium ranging from between about 49% to 55%, an apparent density of between about 5.5 and 6.1 g/cm, and a Vickers hardness of above about 1 GPa. Polycrystalline GaN can be made by hot isostatic pressing (HIPing) at a temperature ranging from about 1150&#xb0; C. to 1300&#xb0; C. and a pressure ranging from between about 1 and 10 Kbar. Alternatively, polycrystalline GaN can be made by high pressure/high temperature (HP/HT) sintering at a temperature ranging from about 1200&#xb0; to 1800&#xb0; C. and a pressure ranging from about 5 to 80 Kbar.

Sintered polycrystalline gallium nitride and its production

A perovskite feedstock (powder or preform) is placed in a high-pressure cell of a high pressure/high temperature (HP/HT) apparatus and subjected to pressures in excess of about 2 kbar and temperatures above about 800&deg; C. for a time adequate to increase the density of the preform.

High pressure production of perovskites and resulting products

The present invention is directed to a method for changing the color of colored natural diamonds. The method includes placing a discolored natural diamond in a pressure-transmitting medium which is consolidated into a pill. Next, the pill is placed into a high pressure/high temperature (HP/HT) press at elevated pressure and elevated temperature for a time sufficient to improve the color of the diamond. The diamond may be exposed at elevated-pressure and elevated-temperature conditions within the graphite-stable region of the carbon-phase diagram&mdash;without significant graphitization of the diamond, or above the diamond-graphite equilibrium and within the diamond-stable region of the carbon-phase diagram. Finally, the diamond is recovered from said press. Colorless Type Ia and Type II diamonds may be made by this method.

A method for detecting whether a natural diamond has been processed at high pressure and high temperature (HPHT) conditions comprises steps of disposing the diamond in a cyrostat that is provided at temperatures equal to or less than liquid nitrogen; illuminating the diamond with a laser beam; recording an optical spectrum of the diamond with a photoluminescence spectrometer; and examining the optical spectrum of the diamond to detect an absence of selected photoluminescent spectral lines. The invention also sets forth a method for predicting whether a natural diamond has been treated under HPHT conditions

Method of detection of natural diamonds that have been processed at high pressure and high temperatures

An improved process for converting hexagonal boron nitride (HBN) particles into cubic boron nitride (CBN) in a high pressure/high temperature apparatus (HP/HT) is disclosed. More specifically, by using melamine as a catalyst, operating pressures and temperatures as well as catalyst costs, may all be reduced.

Growing community of inventors

Columbus, OH, United States of America

Suresh Shankarappa Vagarali