Bridgestone Tire Company Limited

Suminobu Kurahashi

Toru Okuyama

Kinji Masuda

Shigetake Sato

Tsuneharu Akiyama

Sakae Inoue

Toshiyuki Osaki

Motokazu Kikuchi

Noboru Hamada

Sakae Inouye

Susumu Muta

Norio Wada

Method for the preparation of a foam polyamide in which the lactam together with a basic catalyst at a temperature above the melting point of the lactam is mixed with the promoter and foaming agent in a mixing vessel at ambient temperature while subjecting the mix to violent agitation to initiate polymerization, and the mix is discharged into a container for completion of the reaction before polymerization is more than 10% complete.

Process for continuous preparation of a foam polyamide

Methods of preparing polyamide foam comprising polymerizing and foaming a mixture of one or more specified lactams, a basic alkali metal lactam catalyst, an alkyl isocyanate activator and a foaming agent at a temperature above the melting point of the lactam, and below the melting point of the polyamide foam thus produced.

Process for producing polyamide foam

A vulcanizable rubber composition suitable for the production of rubber materials having improved scorching stability and heat aging resistance can be obtained by compounding raw material rubber with a sulfenamide compound having the following general formula ##EQU1## wherein X represents a residue selected from the group consisting of residues of hydrocarbon, alkyl ether and secondary alcohol having 2-20 carbon atoms, and residues represented by the general formulae ##EQU2## (wherein R' represents a residue of hydrocarbon or alkyl ether having 0-20 carbon atoms, and R' represents a hydrocarbon residue having 1-10 carbon atoms), and R.sub.1, R.sub.2, R.sub.3 and R.sub.4 are same or different and are selected from hydrocarbon residues having 2-10 carbon atoms, and hydrogen atom, or R.sub.1 is ringed with R.sub.2 and/or R.sub.3 is ringed with R.sub.4, through the nitrogen atom of the general formula (1), to form heterocyclic rings of 5-7 members.

Sulfenamides in vulcanizable rubber composition

This invention relates to an improvement of the adhesion of a metallic material such as copper, copper alloys and other metals coated therewith with a vulcanizable rubber composition. It is realized by previously adding orthoboric acid or a metal borate to the rubber composition in order to proceed with metal-rubber bonding reaction and vulcanization reaction in good balance, and vulcanizing an assembly of the metallic material and the boric compound containing rubber composition closely contacted therewith.

Method for improving adhesion of metallic material with vulcanizable

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Yokohama, Japan

Suminobu Kurahashi