Nippon Petrochemicals Company, Limited

Jx Nippon Oil Energy Corporation

Nippon Oil Corporation

Shozo Hayashi

Atsushi Sato

Shigenobu Kawakami

Keiji Endo

Hitoshi Yanagishita

Hideyuki Dohi

Akira Takagi

Kunio Sugisawa

Yasuo Togami

Hiroyuki Hoshino

Toshikatsu Shoko

Satoru Inoue

Tadanori Kawamata

Shoji Tai

A method for controlling a particle diameter and a particle diameter distribution of emulsion particles during manufacturing of an emulsion dispersion is provided. The method includes causing two or more types of liquids substantially immiscible with each other to continuously and sequentially pass through net bodies. The net bodies are disposed in a cylindrical flow passage at intervals of 5 to 200 mm, and the number of the net bodies is more than 50 and 200 or less. Each of the net bodies is equivalent to a gauze having a mesh number of 35 mesh to 4000 mesh in accordance with an ASTM standard and has a surface that intersects the direction of the flow passage. An emulsification apparatus used for the method includes a feed pump for feeding two or more types of liquids substantially immiscible with each other; and a cylindrical flow passage to which the two or more types of liquids fed by the feed pump are delivered. A predetermined number of net bodies are disposed in the cylindrical flow passage at predetermined intervals, and each net body has a surface intersecting the direction of the flow passage.

Method and apparatus for controlling particle diameter and particle diameter distribution of emulsion particles in emulsion

The present invention relates to an emulsification method and an emulsification apparatus, capable of attaining easy control of particle size and particle size distribution, and simple scale-up and maintenance, and providing an emulsifying amount sufficient for industrial production. Namely, the method comprises continuously and successively passing two or more types of liquids which are substantially immiscible with each other through two or more mesh members disposed at certain intervals in the presence of an emulsifier to thereby perform emulsification, and the emulsification apparatus as an apparatus for carrying out the method comprises liquid feed pumps for feeding two or more types of liquids which are substantially immiscible with each other, and a cylindrical flow passage to which the two or more types of liquids are fed by the liquid feed pumps, the cylindrical flow passage including a predetermined number of wire gauzes disposed therein at a predetermined interval.

Continuous emulsification method and emulsification apparatus therefor

A method for producing an aromatic compound styrenic compound adduct comprising the steps of: (1) reacting an aromatic compound and a styrenic compound in a first reactor of fixed-bed flow type in a liquid phase in the presence of a solid acid catalyst, (2) circulating a part of the reaction mixture from the above step to the first reactor (3) feeding a reaction mixture flowing out from the first reactor to a second reactor thereby reducing the content of unsaturated components with the aid of a solid acid catalyst, and (4) distilling the resultant reaction mixture, to thereby obtain a fraction having a reduced content of unsaturated components. The method can be used for producing an aromatic compound/styrenic compound adduct having a reduced content of unsaturated components in high yield and at a low cost.

Method for producing aromatic compound

A fraction of low bromine number mainly containing a styrenic compound/aromatic compound adduct can be attained, by feeding reaction materials of a styrenic compound and an aromatic compound to a fixed-bed flow reactor packed with a solid acid catalyst in a liquid phase at a temperature in the range of 40 to 350&deg; C. to form a styrenic compound/aromatic compound adduct, in which (1) the feed of reaction materials is stopped when the bromine number of the above fraction is increased up to a predetermined value, (2) a saturated aromatic hydrocarbon having a mean value of the proportion of aromatic ring carbons in a molecule of 55% or more is fed to the reactor in a liquid phase at a temperature higher by 5 to 150&deg; C. than that of the reaction mixture just before the above stopping, and (3) the feed of reaction materials is then restarted to obtain the fraction.

Method for producing low bromine number fraction

A method to produce diarylmethane or its derivatives by condensation reaction can be carried out without difficulty and without the deterioration of catalyst, and the intended product can be produced inexpensively by recovering and recycling used alcohol. In the method, dimethoxymethane and an aromatic compound are reacted at a temperature of 80 to 400&deg; C. with an acid catalyst. Further, the method comprises the steps of (1) reacting alcohol with formaldehyde using an acid catalyst to obtain acetal; (2) reacting the acetal and an aromatic compound using an acid catalyst to obtain a reaction mixture containing diarylmethane or its derivatives and alcohol; (3) separating and recovering diarylmethane or its derivatives and alcohol from the reaction mixture, and (4) recycling at least a portion of the recovered alcohol to the step (1).

Method for producing diarylmethane or its derivatives

Metallized plastic film capacitor

A plurality of capacitors of the type each including capacitor elements with a very small gap between adjacent electrodes are filled and impregnated with a capacitor oil with the aid of a capacitor oil filling/impregnating apparatus. The apparatus comprises an impregnating chamber including a capacitor oil supplying portion, a charging/discharging platform having a plurality of capacitors placed thereon, and distributing/supplying means arranged above the charging/discharging platform so as to allow the capacitor oil to be supplied to the respective capacitors from above by its free falling-down induced by a dead weight of the capacitor oil itself. A capacitor oil filling/impregnating method is practiced with the aid of the foregoing apparatus by way of the steps of heating the interior of the impregnating chamber under a high level of vacuum to dry the respective capacitors on the charging/discharging platform, cooling the capacitors after completion of the drying operation, supplying the capacitor oil to each capacitor from a capacitor oil refining/supplying system via the capacitor oil supplying portion, keeping the capacitors still for a predetermined period of time after completion of the capacitor oil supplying operation, and allowing the capacitors to be impregnated with the capacitor oil.

Apparatus and method for filling and impregnating capacitors with a

An electrical insulating oil which is suitable for use in impregnating electrical appliances such as capacitors, cables and transformers, especially those in which plastic materials are used partially or totally as dielectrics or insulating materials, and electrical appliances that are impregnated with the above electrical insulating oil. The electrical insulating oil of the invention contains at least one monoolefin and/or diolefin having three condensed or non-condensed aromatic rings.

Electrical insulating oil and electrical appliances impregnated with the

A novel method for improving electrical insulating hydrocarbon. The electrical insulating substance is obtained by dehydrogenating aromatic hydrocarbons having two aromatic nuclei. The electrical insulating substance itself or a mixture of it with other electrical insulating oils is suitable for use in impregnation of electrical appliances.

Method for improving an electrical insulating hydrocarbon

An improved electrical insulating oil which is stable in refining treatment and good electrical properties are maintained under high temperature conditions, and oil-filled electrical appliances impregnated therewith. The electrical insulating oil comprises 1,1,-diarylalkenes which are represented by the following general formula (I): ##STR1## wherein R.sub.1 to R.sub.4 's are the same or different and each of them is a hydrogen atom or an alkyl group having 1 to 5 carbon atoms, and m and n are integers from 0 to 3, inclusive.

Electrical insulating oil and oil-filled electrical appliances

A refined electrical insulating oil and oil-filled electrical appliances impregnated therewith. The electrical insulating oil is quite suitable for use in oil-filled electrical appliances in which insulating materials or dielectric materials made of plastics are employed. The electrical insulating oil is prepared by refining a mixture of unsaturated dimers of styrenes and alkylbiphenyls and/or alkylnaphthalenes, using a solid acidic substance.

Refined electrical insulating oil and oil-filled electrical appliances

An improved electrical insulating oil and oil-filled electrical appliances impregnated therewith. The electrical insulating oil is quite suitable for use in oil-filled electrical appliances in which insulating materials or dielectric materials made of plastics are employed. The electrical insulating oil comprises (a) an electrical insulating oil except polyaromatic hydrocarbons and (b) an aromatic monoolefin and/or diolefin having two condensed or noncondensed aromatic nuclei.

A novel electrical insulating oil and oil-filled electrical appliances that are impregnated with the novel insulating oil. The electrical insulating oil is quite suitable for use in oil-filled electrical appliances in which insulating materials or dielectric materials made of plastics are employed. The electrical insulating oil comprises (a) at least one member of alkylbiphenyls and alkylnaphthalenes and (b) at least one member of monoolefins and diolefins each having two condensed or noncondensed aromatic nuclei.

An improved electrical insulating oil and oil-filled electrical appliances impregnated therewith. The electrical insulating oil is quite suitable for use in oil-filled electrical appliances in which insulating materials or dielectric materials made of plastics are employed. The electrical insulating oil comprises (a) at least one member of diarylalkanes and (b) at least one member selected from the group of mono- and/or diolefins having two condensed or noncondensed aromatic nuclei.

Growing community of inventors

Yokohama, Japan

Shozo Hayashi