Soochow University

Tufts College

Nantong Textile and Silk Industrial Technology Research Institute

Shenzhou Lu

Tieling Xing

Guoqiang Chen

David L Kaplan

Fiorenzo G Omenetto

Xiaoqin Wang

Yirong Wang

Juntao Zhao

Ailing Xie

Xin Ai

Chuchu Lin

Shuqing Lu

The invention provides a silver-plated conductive nylon fiber and a preparation method thereof. The method includes: immersing a nylon fiber in an aqueous solution containing a polyphenolic compound at 60° C. to 70° C., adding a water-soluble oxidant into the solution, continuously reacting at 70° C. to 80° C., and obtaining a polyphenol grafted nylon fiber, where the polyphenolic compound contains a catechol group; immersing the polyphenol grafted nylon fiber into a solution containing silver ions at 15° C. to 25° C. for reaction, and raising the temperature to 70° C. to 80° C. for continuous reaction to obtain a surface-activated nylon fiber; and carrying out chemical silver plating treatment on the surface-activated nylon fiber to obtain the silver-plated conductive nylon fiber. The method does not require a heavy metal sensitizer and therefore is non-toxic and environment-friendly, and the fiber strength is maintained.

Silver-plated conductive nylon fiber and preparation method thereof

The present invention provides a method for preparing a conductive silk fibroin material, comprising the steps of: (1) preparation of a high-molecular-weight silk fibroin solution; (2) preparation of an insoluble silk fibroin material; (3) surface treatment of the silk fibroin material; (4) oxidation of the silk fibroin material; and (5) in-situ oxidative polymerization of 3,4-ethylenedioxythiophene on the surface of the graft-modified silk fibroin material. In the present invention, a conductive composite film grafted with 3,4-ethylenedioxythiophene on the surface is prepared, and the surface resistance is 100 to 5000 ohms. The preparation process is simple and mild, and the obtained conductive silk fibroin material can be used as a flexible electronic device, especially as a device for measuring human blood glucose level and heartbeat.

Conductive silk fibroin material, and preparation method and use thereof

The present invention provides for compositions and methods for preparing aqueous insoluble, ductile, flexible silk fibroin films. The silk films comprise silk fibroin and about 10% to about 50% (w/w) glycerol, and are prepared by entirely aqueous processes. The ductile silk film may be further treated by extracting the glycerol from and re-drying the silk film. Active agents may be embedded in or deposited on the glycerol modified silk film for a variety of medical applications. The films may be shaped into 3-dimensional structures, or placed on support surfaces as labels or coatings. The glycerol modified silk films of the present invention are useful in variety of applications such as tissue engineering, medical devices or implants, drug delivery, and edible pharmaceutical or food labels.

Modified silk films containing glycerol

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Suzhou, China

Shenzhou Lu