Jiangsu Hengli Chemical Fibre Co., Ltd.

Shanshui Wang

Lili Wang

Hongwei Fan

Fangming Tang

Lixin Yin

Damao Yang

Zangzang Niu

Xiaoyu Wang

Yanli Zhao

Chaoming Yang

Jiangen Shen

Zhujun Ding

Huirong Zhao

Ye Zhang

Yiwei Shao

Xiaohua Sun

Wengang Li

Xiaobing Fan

Qianhan Liu

Guangkun Song

Yumei Zhang

Cunhong Wei

A recycled polyester filament and preparation method therefor are disclosed. In the process of preparing a fiber from a recycled polyester according to the FDY process, the ring-blowing is used for cooling, and the distribution of spinneret holes on the spinneret is controlled to meet certain conditions, then the recycled polyester filament is obtained by relaxation heat treatment after a fully drawn yarn is produced. The spinneret holes are C-shaped spinneret holes and circular spinneret holes, the cross-section of the C-shaped spinneret hole is composed of an outer arc, an inner arc, and two line segments, and two endpoints of the outer arc are A and B respectively; wherein the certain conditions include: all the spinneret holes are distributed in concentric circles, and the C-shaped spinneret holes are located on the outermost circle, rotating at different angles and randomly distributed.

Recycled polyester filament and preparation method therefor

A high-strength creep-resistant polyester industrial yarn and preparation method thereof are provided. The high-strength creep-resistant polyester industrial yarn is prepared by spinning, winding and coordination treatment of a modified polyester after solid-state polycondensation to increase viscosity. The condition of coordination treatment is 60-72 hours at 80-100° C. The coordination agent is AgNO, FeCl, CuCl, or NiCl. The polyester segments of the prepared high-strength creep-resistant polyester industrial yarn includes a terephthalic acid segment, an ethylene glycol segment and a 2-(4-pyridine) terephthalic acid segment, and 2-(4-pyridine) terephthalic acid segments of different polyester segments are coordinated by metal ions (Ag, Fe, Cuor Ni). The molar ratio of the terephthalic acid segment to the 2-(4-pyridine) terephthalic acid segment is 1:(0.03-0.05). The N atom on the pyridine of the 2-(4-pyridine) terephthalic acid segment is involved in coordination. Metal ions are coordinated with 2-(4-pyridine) terephthalic acid to greatly reduce the creep degree of the polyester fiber.

High-strength creep-resistant polyester industrial yarn and preparation method thereof

A high-strength thermal-stability polyester industrial yarn is prepared by spinning, winding and coordination treatment of a modified polyester after a solid-state polycondensation; wherein the method of coordination treatment comprises: soaking the wound fiber in an aqueous solution of a coordination agent, and the concentration of the aqueous solution of the coordination agent is 0.1-0.2 mol/L; wherein the condition of coordination treatment is 48-72 hours at 80-100° C., and the concentration of the aqueous solution of the coordination agent is 0.1-0.2 mol/L; wherein the polyester segments of the prepared high-strength thermal-stability polyester industrial yarn comprises a terephthalic acid segment, an ethylene glycol segment and a 2,6-pyridinedicarboxylic acid segment, and 2,6-pyridinedicarboxylic acid segments of different polyester segments are coordinated by Fe, the molar ratio of the terephthalic acid segment to the 2,6-pyridinedicarboxylic acid segment is 1:(0.03-0.05).

High-strength thermal-stability polyester industrial yarn and preparation method thereof

A preparation method of self-crimping elastic combined filament yarns for knitting is disclosed, wherein the combined filament yarns are extruded from the same spinneret; a first fiber-forming polymer melt is divided into two ways, one is directly extruded after distribution; and the other is extruded after distribution by side-by-side composite spinning together with a second fiber-forming polymer melt; the first fiber-forming polymer and the second fiber-forming polymer are compatible or partially compatible; on the same spinneret, a ratio of the number of spinneret holes m for direct extrusion to the number of spinneret holes n for extrusion after distribution by side-by-side composite spinning is 1:(5-10); the self-crimping elastic combined filament yarns for knitting are prepared according to specific spinning processes, wherein the combined filament yarn mainly comprises a first fiber-forming polymer monofilament and a first/second fiber-forming polymer side-by-side composite monofilament; wherein the monofilament crimping directions are randomly distributed.

Preparation method of self-crimping elastic combined filament yarn for knitting

A degradable polyester fiber and its preparation method are disclosed. The preparation method is to cool a PET melt dispersing with doped ZrOpowder by ring-blowing after extruded from a trilobal spinneret hole on a spinneret, and manufacture a fully drawn yarn (FDY) according to an FDY process with the PET melt, then the degradable polyester fiber is prepared after a relaxation heat treatment. The trilobal spinneret hole on the spinneret has three leaves with unequal lengths and angles, and all the trilobal spinneret holes are distributed in concentric circles, with a center line of the leaf opposite to the smallest angle in each trilobal spinneret hole passing through the center of the circle, and pointing away from the center of the circle. The process is simple, and the obtain fiber has good performances in degradation and elasticity.

Degradable polyester fiber and its preparation method

A thermal-moisture comfortable polyester FDY for summer use and a preparation method thereof are provided. The FDY is made of matting agents dispersed polyester via the steps of spinning melt metering, extruding via the compositional spinneret, cooling, oiling, drawing, heat setting and winding. The woven fabrics manufactured with the FDY possess a wicking height and an evaporation rate of larger than or equal to 135 mm and 0.22 g/h, respectively. The compositional spinneret is simultaneously provided with cruciform orifices and circular orifices, and the length ratio of cruciform orifice to circular orifice is equal to the product of their equivalent diameter ratio and a coefficient K, here equivalent diameter is the ratio of orifice cross-section area to its circumference and K ranges from 0.97 to 1.03, and the oiling involves the oiling agent containing 67.30-85.58 wt % of crown ether.

Method for preparing thermal-moisture comfortable polyester FDY

A lightweight heat-preserving fiber and a preparation method thereof are provided, wherein the fiber is prepared by measuring, composite spinneret's extruding, cooling, oiling, drawing, heat setting and winding a polyester melt. The composite spinneret has a hollow spinning hole and a circular spinning hole. The ratio of the micropore length of hollow spinning hole to circular spinning hole equals to the ratio of the equivalent diameter of hollow spinning hole to circular spinning hole multiplies the coefficient K, and the equivalent diameter is the ratio of the cross-sectional area to the circumference of the cross-section, the coefficient K ranges from 0.97 to 1.03. The oil agent contains a crown ether, and the content of the crown ether ranges from 67.30 to 85.58 wt %. The thermal conductivity of a knitted fabric having a basis weight of 100 g/mprepared by lightweight heat-preserving fiber is no larger than 0.150 W/m&#xb7;K.

Light weight heat-preserving fiber and preparation method thereof

A type of polyester yarn for an industrial sewing thread and preparing method thereof are provided. The preparing method is composed of a viscosity enhancing by a solid state polycondensation and a melt spinning for a modified polyester, and the modified polyester is a product of esterification and polycondensation of evenly mixed terephthalic acid, ethylene glycol, tert-butyl branched dicarboxylic acid, trimethylsilyl branched diol and a doped SbOpowder, wherein the tert-butyl branched dicarboxylic acid is selected from the group consisting of 5-tert-butyl-1,3-benzoic acid, 2-tert-butyl-1,6-hexanedioic acid, 3-tert-butyl-1,6-hexanedioic acid and 2,5-di-tert-butyl-1,6-hexanedioic acid. Moreover, the modified polyester is dispersed with a doped ZrOpowder. An obtained fiber has an intrinsic viscosity drop of 23-28% when stored at 25&#xb0; C. and R.H. 65% for 60 months.

Polyester yarn for industrial sewing thread and preparing method thereof

A type of easy-to-dye degradable polyester FDY and preparing method thereof are disclosed. The method for preparing an easy-to-dye degradable polyester FDY is to prepare a modified polyester FDY from a modified polyester melt with FDY process; wherein the material is a modified polyester; wherein the modified polyester has a molecular chain structure composed of terephthalic acid segments, ethylene glycol segments, 2,2,3,4,5,5-hexamethyl-3,4-hexanediol segments and tert-butyl branched heptanediol segments; wherein the modified polyester is dispersed by solid heteropolyacid powder calcined at a 400&#x2dc;700&#xb0; C. temperature. The preparing method has a simple process, modifying the polyester through solid heteropolyacid, tert-butyl branched heptanediol and 2,2,3,4,5,5-hexamethyl-3,4-hexanediol, which increases the hydrolysis rate of the polyester, improves the dyeing performance and prepares products with excellent mechanical properties.

Easy-to-dye degradable polyester FDY and preparing method thereof

A type of high-modulus-low-shrinkage activated PET industrial yarn and preparing method thereof are disclosed. The preparing method is to manufacture filament from a modified polyester, which is the product of the esterification and the successive polycondensation reactions of evenly mixed terephthalic acid, ethylene glycol and tert-butyl branched heptanediol, through a series of processes composed of viscosity enhancing by solid state polycondensation, melting, metering, extruding, cooling, oiling, stretching, heat setting, relaxation heat-treating, oiling with activation oil, winding and pre-activation treatment. The relaxation heat-treating indicates passing the modified polyester yarns through a space with a certain temperature within 200-220&#xb0; C. under a proper relaxation state; and the proper relaxation state means a 3.0-5.0% of overfeed for the winding. The improvement of activator efficiency by importing the tert-butyl branched diol into the polyester, together with the synergistic effect of heat setting temperature and high winding overfeed rate, will reduce the fiber thermal shrinkage.

Preparing method of high-modulus-low-shrinkage activated PET industrial yarn

A type of wool-like polyester filament and preparing method thereof are disclosed. The preparing method is manufacturing filament from a modified polyester through a POY process and a successive DTY processes, wherein the modified polyester is the product of the esterification and the successive polycondensation reactions of evenly mixed terephthalic acid, 1,4-butanediol, fluorinated dicarboxylic acid, tert-butyl branched hexanediol and 2,5,6,6-tetramethyl-2,5-heptanediol. The obtained fiber has a dye uptake of 90.32-93.27% and a K/S value of 22.15-23.42 when dyed at 100&#xb0; C., and has an intrinsic viscosity drop of 17-20% when stored at 25&#xb0; C. and R.H. 65% for 60 months. This invention features a method with ease of application and a product with good dyeing and degradation performance.

Wool-like polyester filament and preparing method thereof

A bi-profiled fiber and preparing method thereof are provided. The bi-profiled fiber is manufactured through the steps of spinning melt metering, extruding via the composite spinneret, cooling, oiling, drawing, heat setting and winding, finally containing both double-cross monofilaments and circular monofilaments simultaneously. The bi-profiled fiber is made of the modified polyester, and the modified polyester is dispersed by matte agent and is composed of terephthalic acid segments, ethylene glycol segments and branched diol segments, and the branched diol segment has a structural formula of 

Bi-profiled fiber and preparing method thereof

A high uniformity coloured polyester industrial yarn and preparation method. The raw material of the high-uniformity coloured polyester industrial yard is the modified polyester composed of terephthalic acid segment, an ethylene glycol segment and a branched diol. The high-uniformity coloured polyester industrial yarn is prepared by esterification reaction of terephthalic acid with a branched diol using concentrated sulfuric acid as catalyst to obtain terephthalic acid glycol ester. Terephthalic acid and ethylene glycol are formulated to carry out esterification reaction to obtain ethylene terephthalate. Finally, stir and mix the two materials and carry out the polycondensation reaction in the low vacuum stage and the high vacuum stage under the action of the catalyst and the stabilizer to obtain modified polyester. Measure the modified polyester and add black masterbatch. After porous spinneret extrusion, cooling, oiling, drawing, heat setting and winding the modified polyester, high uniformity coloured polyester industry yarn is obtained.

High-uniformity coloured polyester industrial yarn

A porous ultra-soft ultra-fine denier polyester fiber and preparation method. The modified polyester is spun with a porous spinneret to produce the porous ultra-soft ultra-fine denier polyester fiber, and the spinneret holes on the porous spinneret are arranged in an elliptical arrangement. The porous ultra-soft ultra-fine denier polyester fiber is obtained by metering, extruding, cooling, oiling and high-speed winding the modified polyester chips. The preparation method of modified polyester is as follows: terephthalic acid reacts with ethylene glycol to produce ethylene terephthalate. The modified polyester is obtained by the reaction of terephthalic acid with branched diol. The fiber of the invention has good properties and the deviation rate of fiber density. The deviation rate of fiber density is &#x2264;0.5%, the CV value of breaking strength is &#x2264;4.0%, the CV value of elongation at break is &#x2264;8.0%, the CV value of yarn unevenness is &#x2264;2.0%.

Porous ultra-soft ultra-fine denier polyester fiber and its preparation method

A polyester obtained by the esterification of terephthalic acid and ethylene glycol and the polycondensation catalysed by a mixture of magnesium ethylene glycol and antimony ethylene glycol followed by granulation. In the polyester sections, the carboxyl end group is less than 15 mol/t, the mass percentage of oligomer is lower than 0.5%, and weight percentage of diethylene glycol is lower than 0.5%.

Growing community of inventors

Wujiang, China

Shanshui Wang