Monsanto Company

Samuel Steingiser

Morris Salame

James M McKelvey

In forming containers by distending preforms of nitrile thermoplastic material at molding temperature, the improvement comprising exposing such preforms to low dosage radiation to reduce residual nitrile monomer in the thermoplastic material and then distending the irradiated preforms to cause HCN generated during irradiation to flash off in forming the container. The containers formed have unusually low concentrations of residual nitrile monomer as well as extractable HCN making them especially suitable for packaging foods, beverages, pharmaceuticals and the like. The irradiated preforms from which such containers are made have similarly low residual nitrile monomer levels.

Nitrile preforms and containers and process improvements for forming same

In plastics extrusion apparatus including a rotating screw in a cylinder forming a channel receiving solid material and eventually expressing it through a die, the channel comprising a feed zone, a melting and compression zone and a melt pumping zone, the improvement wherein a solids decompression zone is between the feed and the melting and compression zones which has increased unit volume relative to that of the feed zone, with the channel of the melting and compression zone communicating with the feed inlet through the decompression and feed zones such that solids are initially metered producing a starved condition so as to melt at substantially atmospheric pressure without filling the channel of the melting and compression zone until close to its end.

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Bloomfield, CT, United States of America

Samuel Steingiser