Invensys Systems, Inc.

Schneider Electric Systems USA, Inc.

Russell Jackson

W Marcus Trygstad

Bruce A Keen

A spectroscopic sample analysis apparatus includes an actively controlled heat exchanger in serial fluid communication with a spectroscopic analyzer, and a controller communicably coupled to the heat exchanger. The heat exchanger is disposed downstream of a fluid handler in the form of a stream selection unit/stream switching unit (SSU), a solvent/standard recirculation unit (SRU), and/or an auto-sampling unit (ASU). The SSU selectively couples individual stream inputs to an output port. The SRU includes a solvent/standard reservoir, and selectively couples output ports to the heat exchanger, and returns the solvent/standard sample to the reservoirs. The ASU includes a sample reservoir having a sample transfer pathway with a plurality of orifices disposed at spaced locations along a length thereof. The controller selectively actuates the fluid handler, enabling sample to flow there through to the heat exchanger, and actuates the heat exchanger to maintain the sample at a predetermined temperature.

Spectroscopic crude oil analysis

A method and apparatus is provided for determining concentration of components in a liquid hydrocarbon mixture including hydrocarbons and water flowing through an alkylation process. A fluid flow path conveys the liquid continuously from the alkylation process through a first instrument configured for measuring a property of the liquid mixture, and having responsivities to concentration of the components, which are independent of the concentration of the water. A temperature detector generates temperature data for the liquid, and a second instrument measures another property of the liquid mixture. The instruments have mutually distinct responsivities to concentrations of the components. A processor captures data from the temperature detector and instruments, using the data with a model of responsivities of various concentrations of the components at various temperatures, to determine a temperature compensated concentration of the components while the liquid mixture flows continuously through the fluid flow path.

System and method for alkylation process analysis

A method and apparatus is provided for off-line concentration determination of components liquid hydrocarbon mixtures such as crude or heavy oil. A sampling unit continuously delivers a sample volume to a fluid flow path while a temperature control module maintains the sample at a predetermined setpoint temperature. A homogenization module helps prevent sample stratification while a flow control module maintain a constant sample flow rate. A spectrometer is communicably coupled to an optical transmission cell to transmit and receive radiation. The transmission cell includes collection optics to capture and aggregate non-collimated radiation emerging from the cell, for transmission to the spectrometer. The spectrometer measures sample spectra at a predetermined rate of flow of the sample volume through the transmission cell. A processor is configured to capture and use the spectra in combination with a model of spectra for the hydrocarbon mixture.

Offline analyzer system and method for multivariate characterization of properties in crude and heavy hydrocarbon oils

A spectroscopic sample analysis apparatus includes an actively controlled heat exchanger in serial fluid communication with a spectroscopic analyzer, and a controller communicably coupled to the heat exchanger. The heat exchanger is disposed downstream of a fluid handler in the form of a stream selection unit (SSU), a solvent/standard recirculation unit (SRU), and/or an auto-sampling unit (ASU). The SSU selectively couples individual stream inputs to an output port. The SRU includes a solvent/standard reservoir, and selectively couples output ports to the heat exchanger, and returns the solvent/standard sample to the reservoirs. The ASU includes a sample reservoir having a sample transfer pathway with a plurality of orifices disposed at spaced locations along a length thereof. The controller selectively actuates the fluid handler, enabling sample to flow therethrough to the heat exchanger, and actuates the heat exchanger to maintain the sample at a predetermined temperature.

Spectroscopic sample analyzer and sample handling system

Closed-loop control of a hydrocarbon process is provided by an analyzer including an instrument configured for measuring a property of the liquid mixture, and having responsivities to concentrations of one of the components, independent of concentrations of others of the components. A temperature detector generates temperature data for the liquid mixture, and a processor captures data generated by the temperature detector and the instrument, and uses the data in combination with a model of responsivities to various concentrations of the components at various temperatures, to determine a temperature compensated concentration of the components while the liquid mixture flows continuously through the analyzer. A process control module including a process model of the hydrocarbon process, is coupled to the analyzer and is couplable to the hydrocarbon process, to receive the temperature compensated concentration and to generate at least one output configured to affect operation of the hydrocarbon process.

System for alkylation process analysis

A spectroscopic sample analysis apparatus includes an actively controlled, direct contact heat exchanger in serial fluid communication with a spectroscopic analyzer, and a controller communicably coupled to the heat exchanger. The heat exchanger is disposed downstream of a fluid handler in the form of a stream selection unit (SSU), a solvent/standard recirculation unit (SRU), and/or an auto-sampling unit (ASU). The SSU selectively couples individual stream inputs to an output port. The SRU includes a solvent/standard reservoir, and selectively couples output ports to the heat exchanger, and returns the solvent/standard sample to the reservoirs. The ASU includes a sample reservoir having a sample transfer pathway with a plurality of orifices disposed at spaced locations along a length thereof. The controller selectively actuates the fluid handler, enabling sample to flow therethrough to the heat exchanger, and actuates the heat exchanger to maintain the sample at a predetermined temperature.

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Sudbury, MA, United States of America

Russell Jackson