Peroxid-chemie Gmbh

Kali-chemie Aktiengesellschaft

Rudolf Siegel

Werner Doetsch

Richard Roesler

Werner Zeiss

Helmut Honig

Helmut Dillenburg

A process is described for preparing peroxyborate agglomerates having an active oxygen content of at least 14% by weight in which amorphous primary particles composed of peroxyborate prepared by a spray drying process are subjected to compacting pressing-agglomeration. Briquettes, compressed strips and tablets can be obtained which can be comminuted, if desired, to peroxyborate granules of desired particle size and bulk density. Advantageous, optionally colored, peroxyborate agglomerates, particularly peroxyborate granules are prepared. Preferred agglomerates and granules are composed of sodium peroxyborates.

Process for preparing peroxyborate agglomerates

A process for preparing microcrystalline perborate hydrate products and highly concentrated, storage stable aqueous solutions used for this purpose which have a stable active oxygen content and a boron content of 3 to 8% by wt. based on the total weight of the solution. The products of the invention are suitable for numerous uses in the field of bleaching agent, disinfectant and liquid detergent formulations, and other fields of use.

Process for preparing microcrystalline perborate products

A process for producing a solid, cold-water soluble, sulfate containing aluminum chloride composition suitable for use as a waste water clarifying agent comprising introducing alkali aluminate, sulfuric acid, hydrochloric acid and hydrated aluminum oxide into a spray drier and recovering the resulting solid product.

Process for producing solid aluminum chloride compositions

Superoxidized sodium perborate with an active oxygen content of more than 16 wt. % and a specially adapted process for its preparation.

Superoxidized sodium perborate

Disclosed is potassium perborate-hydrate of the formula KBO.sub.3.nH.sub.2 O where n is 0 to 1 and a process for its preparation by the reaction of H.sub.2 O.sub.2 with potassium metaborate in the presence of an excess of potassium ions.

Potassium perborate-hydrate and process for its preparation

Disclosed is an adduct of the formula 4Na.sub.2 SO.sub.4.2H.sub.2 O.sub.2.KCl and a process for the preparation of this adduct by crystallizing the adduct out of a suspension containing from about 100 to 900 g of hydrogen peroxide per liter of solution and a quantity of sodium sulphate and potassium chloride which exceeds the saturation concentration of the adduct at the crystallization temperature, whereby the weight ratio of sodium sulphate to potassium chloride is in the range of from about 2:1 to 12:1. A continuous process is also disclosed for producing the adduct.

Hydrogen peroxide adduct and process for preparation and use thereof

A process for improving the storage behavior of alkali persalts in particularly alkali percarbonates, by preparing a granulate composition therefore is disclosed. The process comprises the steps of:

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Neuwied, Germany

Rudolf Siegel