USA As Represented by Secretary of the Navy

Other

Science Applications International Corporation

Geo-centers, Inc.

The Government of the United States of America, As Represented by the

Ronald R Price

Joel M Schnur

Paul E Schoen

Robert F Brady, Jr

Walter J Dressick

Daniel Zabetakis

Jacque H Georger, Jr

Alok Singh

Alan S Rudolph

Bruce P Gaber

Ann E Mera

Dana Leamann

Bor-Sen Chiou

Paul Yager

Mark S Spector

Mary A Testoff

Banahalli R Ratna

Henry F Gray

Jeffrey M Calvert

Douglas A Kirkpatrick

Wallace M Manheimer

Anne W Kusterbeck

Dan Zabetakis

Mariam Monshipouri

Robert David Eden

Michael A Dinderman

Jonathan Selinger

The present invention is directed to a method for making a conformal antenna on a surface by providing a composition comprising a polymer matrix and a plurality of metalized tubules and applying the composition to the surface as two parallel wires connected at their ends to make a closed loop with one of the parallel wires broken in the middle. Also disclosed is an alternate method for making a conformal antenna on a surface by spraying a first material comprising a polymer matrix onto the surface and simultaneously spraying a second material comprising a plurality of metalized tubules and a coagulant onto the surface, wherein the first and second materials mix together during the spraying. A further method for making a conformal antenna includes spraying a first material comprising a polymer matrix and a plurality of metalized tubules onto the surface and simultaneously spraying a second material comprising an aqueous electroless plating bath onto the surface, wherein the first and second materials mix together during the spraying.

Conductive microcylinder-based paints for integrated antennas

The present invention provides microwave attenuating, filled composite materials which contain a polymer or ceramic matrix and metallic tubules and processes for making the same and devices which contain such materials.

Microwave-attenuating composite materials, methods for preparing the same, intermediates for preparing the same, devices containing the same, methods of preparing such a device, and methods of attenuating microwaves

A composition is provided having cylindrically shaped metal or metal-coated particles and a polymer latex dispersion. A coating is provided having cylindrically shaped metal or metal-coated particles and a polymer matrix formed from a latex dispersion. The particles form a continuous, conductive network. A method of electromagnetic shielding is provided having the steps of providing the above composition, applying the composition to a surface, and drying the applied composition.

Waterborn coating containing microcylindrical conductors

The wall thickness of lipid microtubules are controlled by selecting a methanol/water system and determining the required amount of a lipid to form the desired wall thickness. The lipid is dissolved in a small portion of the heated methanol and that clear solution is added to the remaining amount of the heated methanol/water system. By slowly cooling the solution, microtubules are formed which have the desired wall thickness. Preferred microtubules have a wall thickness of just 2 bilayers and they are robust so they can be further coated. They can be made with a large aspect ratio and with lengths of greater than 250 microns. The process permits production of microtubules in very high yields.

Processing methodology for the rational control of bilayer numbers leading to high efficiency production of lipid microtubules

A method for delivering encapsulated materials to a subsurface environment, for the treatment of the subsurface environment, has the steps of: (a) loading the lumen of hollow microtubules with an active agent selected for treating the subsurface environment, where the hollow microtubules are compatible with the subsurface environment; and (b) administering the hollow microtubules to the subsurface environment, permitting the controlled release of the active agent into the subsurface environment. This method may be practiced using a slurry of hollow microtubules, where the lumen of these microtubules is loaded with an agent for the treatment of petroleum well environments, and where these loaded microtubules are dispersed in a liquid phase carrier selected from aqueous carriers, non-aqueous carriers, and emulsions of aqueous and non-aqueous materials. This method may also be practiced using a pill made of a consolidated mass of tubules loaded with one or more active agents, typically bound with a binder.

Efficient method for subsurface treatments, including squeeze treatments

Tubules which contain an active agent in their lumen and compositions containing such microtubules are effective for providing a slow, controlled release of the active agent. Such microtubules are useful in the production of coating compositions for the protection of surfaces coming into contact with water, adhesive resins for the production of laminated wood products, and devices for dispensing pesticides.

Method of controlled release and controlled release microstructures

Lipid microtubules having a controlled bilayer structure and high aspect io are formed in a methanol/ethanol/water solvent system. The lipid microtubules may then be catalyzed (e.g., with a palladium/tin catalyst) in an acidified catalytic bath having no more than about 30 g of catalytic salts. These catalyzed microtubules are then metallized using a diluted plating bath with replenishment of the plating bath as needed to obtain the desired metallization thickness.

Process for the formation of high aspect ratio lipid microtubules

Microspheres, of controllable shape and size, encapsulating active ingredients, are made by the internally controlled gelation of an emulsion including a water-soluble polysaccharide, a salt of a di- or trivalent metal cation, a polymerization inhibitor, water, a water-immiscible solvent (as a non-aqueous phase), and the active ingredient. The components of the aqueous phase, containing the water-soluble polysaccharide, polymerization inhibitor, di- or trivalent metal salt, active substance, and water, are blended together. This aqueous phase is then gradually mixed with the oil phase and agitated to form an emulsion. After sufficient time for solidification, the emulsion is broken and the resulting microspheres are collected. The active ingredient may be various substances, including live microorganisms.

Internal gelation method for forming multilayer microspheres and product

The present invention is a method for releasing an active agent into a use nvironment, by disposing this active agent within the lumen of a population of tubules, and disposing the tubules into a use environment, either directly or in some matrix such as a paint in contact with the use environment. The tubules have a preselected release profile to provide a preselected release rate curve. The preselected release profile may be achieved by controlling the length or length distribution of the tubules, or by placing degradable endcaps over some or all of the tubules in the population, or by combinations of these methods. The invention is also a population of tubules having a preselected release profile to provide a preselected release rate curve.

Sustained delivery of active compounds from tubules, with rational

The present invention is a composition for, and a method of, delivering an active agent at a controlled rate. The composition of the invention is a hollow ceramic or inorganic microtubule, where the active agent is contained within the lumen of the microtubules. Typically, the agent is adsorbed onto an inner surface of the microtubule. The method of the invention is disposing this novel composition in a use environment. In a preferred embodiment of the invention, a microtubule is a tubule having an inner diameter of less than 0.2 .mu.m, and microtubules are tubules having an average inner diameter less than 0.2 .mu.m. In a preferred embodiment, the hollow ceramic or inorganic microtubule is a mineral microtubule, such as halloysite, cylindrite, boulangerite, or imogolite. In a more preferred embodiment of the invention, the mineral microtubule has a biodegradable polymeric carrier disposed in its lumen. In a preferred embodiment of the invention, the inner diameter of the microtubules varies from about 0.20 .mu.m to about 0.35 .mu.m, or averages about 0.40 .mu.m. In another preferred embodiment, of the invention, the inner diameter of the microtubules varies from about 200 .ANG. to about 1000 .ANG..

Controlled release of active agents using inorganic tubules

Controlled release microstructures

A high resolution, cathodoluminescent display screen or device and a method of producing such a display device is disclosed. The display screen includes a plurality of channel structures having longitudinal ends, a transparent medium formed in a plane to which the channel structures are fixed with one longitudinal end thereof oriented toward the plane of the transparent medium, and a cathodoluminescent material deposited on the channel structures whereby incident electrons and light generated by the incident electrons are directed along the channel structures. Preferably, the display screen also includes a mechanism for removing built up charge from the display screen, such as conductive channel structures and/or a conductive transparent medium. The cathodoluminescent material can include phosphors, and for producing a color display, different materials producing different colors would be used. In one preferred embodiment, the channel structures are tubules. Alternately, the channel structures can be channel plates or other structures providing channeling structures. In the preferred embodiment, the transparent medium is glass. However, the transparent medium could be quartz or some other equivalent material. In order to provide a display device the display screen is then mated with an addressable electron source for generating electrons incident on the cathodoluminescent material of selected channel structures. Preferably, the electron source means includes a field emitter array with a reflecting surface.

Method and apparatus for a high resolution, flat panel

A field emitter array comprises an array of aligned metallic, conductive rotubules extending from a conductive base. The array is typically made by cutting a matrix comprising the aligned microtubules into sections, usually normal to the tubule alignment axis. One end surface of a section is etched or otherwise treated to remove the matrix, but not the tubules. That end surface is then provided with a conductive coating and fixed to a contact. The other end surface of that section is then also treated to remove the matrix material and leave the tubules extending from the conductive metal base. Field emitter arrays made according to the present invention provide a greater brightness than conventional field emitter arrays.

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Stevensville, MD, United States of America

Ronald R Price