Exxon Production Research Company

Ronald P Steiger

Peter K Leung

Rudolf J Stankovich

John M Longo

Kenneth R Kunze

Michael K Kroeger

Russell T Ewy

An end-cap-to-piston coupling, with or without an integral load cell has been developed for triaxial test apparatus. One triaxial test apparatus shown has a housing, sample mounting apparatus in the housing, a load piston opening through the housing through which projects a load piston, and a load transfer coupling, with or without an integral load cell, interposed between the end cap and the load piston. In one aspect the coupling has a coupling body and a channel on one end into which the load piston is inserted to contact a shoulder of the coupling body. Another end of the coupling has a channel which receives a top end cap of a sample mounting arrangement. This channel may be sized and configured to receive a load transfer ball interposed between the coupling and the end cap or between the coupling and the piston. In one aspect a series of interchangeable top and bottom members are provided, each with a different diameter recess, to accommodate load pistons and sample end caps of different diameters.

End-cap-to-piston coupling for triaxial test apparatus

Load cell having a body with a ball recess therein and a ball removably disposed in the recess above a strain gauge means disposed in the body centrally below the ball recess, the load cell useful in measuring samples of geologic materials, e.g., core samples and for methods and apparatuses for measuring ultrasonic velocities in materials, particularly in the triaxial testing of low permeability rock samples.

Load cell

A method for determining drilling fluid density for stabilizing a wellbore including obtaining shale cuttings from a wellbore. In one embodiment of a method according to this invention, shale cuttings are obtained from a wellbore and their index properties, including but not limited to surface area, is measured; mean effective stress around the wellbore is calculated using the geostatic overburden in situ stress, the field pore pressure, and the total stress around the wellbore; the in situ shale strength is determined using a correlation between surface area, mean effective stress and shale strength; and drilling fluid density is determined using the shale strength. Methods for determining in situ shale strengths, elastic properties, pore pressures, and formation stresses of low permeability rocks.

Methods for measuring physical parameters of a low permeability rock

Methods and apparatuses for testing the effects of one or more fluids on geologic materials; in one aspect a method for quantitatively determining the hydration and swelling behavior of shale core samples in response to one or to different fluids circulated around a core sample confined under pressure in a test cell; apparatuses for circulating such fluids and for conducting such tests; and an adjustable LVDT holder.

Measurement of hydration behavior of geologic materials

Methods and apparatuses for measuring ultrasonic velocities in materials are disclosed which, in one embodiment, include such methods and apparatuses for triaxial tests of low permeability rock samples, the apparatus including top and bottom end caps for mounting to a sample to be tested, each end cap having an ultrasonic transducer mounted therein for disposition in contact with the material to be tested for measuring the velocities of ultrasonic waves through the material. In another embodiment, at least one end cap having channels and a sensor for sensing changes in sample pore pressure is disclosed. In another aspect, a pressure generator or microaccumulator for changing the amount of a pore pressure fluid in the channels, thereby changing sample water content and making possible an efficient multistage test is disclosed. In another embodiment an end cap for such measurements is disclosed.

Apparatuses and methods for measuring ultrasonic velocities in materials

Methods are disclosed for multi-stage tests of material samples, including but not limited to rock and shale samples, the methods, in one aspect, including the steps of placing a load on the sample, while under a constant confining pressure the sample mounted in a triaxial test apparatus; measuring and recording sample pore pressure continuously during the test; removing the load on the sample; changing confining pressure on the sample; permitting the sample's pore pressure to equilibrate at a new pore pressure with the new confining pressure; permitting the sample to drain fluid to an equilibrium value and placing a new load on the sample measuring and recording resulting pressure and load. In one embodiment these steps are repeated a plurality of times and a plurality of pore pressure, confining pressure, and load readings are obtained.

Apparatuses and methods for adjusting a material's fluid content and

Methods and apparatuses for quantitatively measuring the strengths, pore pressures, and mechanical properties of low permeability geologic materials, such as shales, including test specimen preparation apparatus for adjusting test specimen water content and test apparatus with an end cap having a pore pressure transducer channel disposed adjacent a test specimen filled with an immiscible, inert fluid which does not wet the test specimen, and controlling the deviatoric load on the test specimen during the test to prevent premature failure.

Methods and apparatuses for measurement of the strengths, pore

Methods for determining in situ shale strengths, elastic properties,

A nontoxic, nonchloride, water-base drilling fluid which stabilizes water sensitive shales is disclosed. This drilling fluid is comprised of the potassium or ammonium salt of an organic acid in combination with a polar organic liquid, so as to reduce shale swelling with mineral adverse impact on the environment.

Nontoxic, nonchloride, water-base, inhibitive fluid to stabilize water

A microaccumulator for receiving and holding fluid under pressure, and for measuring fluid volume changes in one aspect in very small amounts, and for indicating the amount, the microaccumulator having a body with an interior cavity for receiving the fluid and a piston movably disposed therein which moves in response to a change in fluid amount, the piston having a sensor interconnectible with a monitor and/or system control (e.g. a computer) which can control monitor and/or record changes in the amount of fluid. A triaxial test apparatus for low permeability rock (e.g. shales) using such a microaccumulator. Methods for triaxial tests and for the use of such devices.

Microaccumulator for measurement of fluid volume changes under pressure

A method for determining at wellsites the swelling-clay content of cement mixtures by high-frequency dielectric measurements including: grinding a cement mix sample to a size suitable for testing; washing the cement mix sample with a fluid having a water activity substantially less than water, which may contain a soluble cation; packing the washed cement mix sample into a sample cell suitable for dielectric measurement; measuring the dielectric constant at a preselected frequency; and comparing the measured dielectric constant of the cement mix sample to calibration curves.

Method for determining the swelling clay content of cement mixtures by

A method for determining at wellsites the solids content of drilling fluids by high-frequency dielectric measurements including: preparing samples of the drilling fluid, of the drill cuttings from the formation, and of each solids-additives type added to the drilling fluid for uniform dielectric constant measurements at preselected frequencies and obtaining the solids content in accordance with the relationship between the dielectric constant measurements of the drilling fluid-solids, drill cuttings, and each of the solids-additives type. In accordance with the method of the invention two levels of determination are possible. These levels of determination depend upon whether the quantities of solids-additives type added to the drilling fluid are known.

Process for rapidly determining the solids content in drilling fluids

A method for determining at wellsites the swelling-clay content of shales and shaly sandstones earth formations whereby a sample of the formation is washed with a fluid having a water activity substantially less than that of water, which fluid may contain a soluble cation, and measurements of the sample's dielectric constant are made at a preselected frequency for subsequent comparison to calibration curves, thereby obtaining a measurement of the welling-clay content of the formation. The determinations of the swelling-clay content may be performed at different levels depending on the nature of the samples.

Method for rapidly determining the swelling-clay content in shales and

A removable porous layer is placed on the outside of various well implements. The layer allows movement of liquid toward sites of localized low pressure and therefore prevents differential pressure stickage of the well implements on the borehole wall.

Detachable apparatus for preventing differential pressure sticking in

A porous layer is placed on the outside of various well implements. The layer allows movement of liquid toward sites of localized low pressure and therefore prevents differential pressure stickage of the well implements on the borehole wall.

Growing community of inventors

Houston, TX, United States of America

Ronald P Steiger