United States of America, As Represented by the Secretary of Agriculture

Other

The United States of America As Represented by the Secretary of

Wisconsin Alumni Research Foundation

Director, Bureau of Engraving and Printing, Department of the Treasury

Roland L Gleisner

Junyong Zhu

Dennis E Gunderson

Liheng Chen

Freya Tan

Xuejun Pan

Jun Yong Zhu

Steven G Hankel

Gaosheng Wang

C Timothy Scott

Methods of fractionating lignocellulosic biomass using maleic acids are provided. Also provided are methods of forming lignin particles, furans, sugars, and/or lignocellulosic micro- and nanofibrils from the liquid and solid fractions produced by fractionation process. The fractionation can be carried out at low temperatures with short reaction times to carboxylate and dissolve lignin with a low degree of condensation.

Fractionation of lignocellulosic biomass using maleic acid at low temperature

Methods of fractionating lignocellulosic biomass using hydrotropic solid organic acids are provided. Also provided are methods of forming lignin particles, furans, sugars, and/or lignocellulosic micro- and nanofibrils from the liquid and solid fractions produced by fractionation process. The fractionation can be carried out at low temperatures with short reaction times.

Low temperature and efficient fractionation of lignocellulosic biomass using recyclable organic solid acids

Methods of fractionating lignocellulosic biomass using hydrotropic sulfonic acids are provided. Also provided are methods of forming lignin particles, furans, sugars, and/or lignocellulosic micro- and nanofibrils from the liquid and solid fractions produced by fractionation process. The fractionation can be carried out at low temperatures with short reaction times.

Methods of pretreating lignocellulosic biomass in preparation for enzymatic saccharification and fermentation are provided. Also provided are methods of producing ethanol from lignocellulosic biomass via enzymatic saccharification and fermentation that utilize the pretreatment method. In the methods, pretreatment is conducted in two stages. In the first stage, the lignocellulosic biomass is treated in a mildly acidic or near pH-neutral solution to promote delignification and lignin sulfonation, while minimizing the formation of degradation products that inhibit subsequent enzymatic saccharification and/or fermentation. In the second stage, the pH of the solution is decreased in order to promote the depolymerization and dissolution of hemicelluloses in the lignocellulosic biomass.

Methods of pretreating lignocellulosic biomass with reduced formation of fermentation inhibitors

The present invention relates to a method using sulfite pretreatment to overcome recalcitrance of lignocellulose (SPORL). More specifically, it relates to a sulfite-based chemical process for pretreating biomass in solutions to reduce access barriers of enzymes to the lignocellulose, resulting in efficient conversion through enzymatic saccharification.

Sulfite pretreatment for biorefining biomass

A method and apparatus are presented for determining the quantity of liquid and solid content in a removal stream of a froth created from a suspension that is generated during a froth flotation operation. Specifically, electrodes are immersed in the froth generated from a suspension having a known quantity of fiber particles, and the conductance of the froth is measured to establish a relationship between the measured conductance and the quantity of fiber particles. The electrodes are then submerged in a froth generated from a suspension having an unknown quantity of fiber particles, and the froth conductance is measured. The quantity of fiber particles in the froth can then be determined from the pre-established relationship between conductance and solid particle content.

Method and apparatus for monitoring liquid and solid contents in a froth

An apparatus and method uses vacuum restraint, or other pressure differenl, to hold the ends of a sheet specimen to two opposing surfaces, thereby creating a fold in the specimen. As the opposing surfaces cycle along a parallel axis in opposite directions, the fold repeatedly rolls through a specific region of the specimen. The spacing between the opposing surfaces can be adjusted to increase or to decrease the radius of the fold. The velocity of the fold and the number cycles also can be controlled precisely. After repeated movement of the fold, the adhesion of surface treatments, coatings or printing on the specimen substrate begins to break down. Additionally, the integrity of the substrate itself may begin to deteriorate, if it is susceptible to deterioration and to varying degrees depending upon the susceptibility. The extent to which the specimen coating is degraded and substrate integrity reduced is a function of spacing, fold velocity and number of cycles.

Method and apparatus for evaluating fold endurance and surface adhesion

An improved method and apparatus for dry forming adhesive coated wood fibers in an airstream in a particular mold apparatus. The invention includes a particular sequence of steps and related apparatus, and permits the manufacturer of a mat of differing cross-sectional shapes but of uniform density. The invention includes the advantageous steps of final curing of the mat off of the main molding apparatus, thus achieving efficiencies in use.

Method for forming structural components from dry wood fiber furnish

An improved apparatus for dry forming adhesive coated wood fibers in an airstream in a particular mold apparatus. The invention permits the manufacture of a mat of differing cross-sectional shapes but of uniform density. The invention includes the advantageous steps of final curing of the mat off of the main molding apparatus, thus achieving efficiencies in use.

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Jefferson, WI, United States of America

Roland L Gleisner