Exxon Research and Engineering Company

Exxon Production Research Company

Robert E Steele

Eugene R Thomas

Ralph G Wolfe

Constantine Tsonopoulos

Dennis P Maloney

The removal of a glycol contaminant from a mixture of polyalkylene glycol dialkyl ethers is achieved using a dual solvent extraction process. The process is particularly applicable to removing glycols which accumulate in recirculating solutions of polyalkylene glycol dialkyl ethers used for the absorption of acid gases from feedstocks such as natural gas, synthetic natural gas, refinery gas, and ammonia synthesis gas.

Removal of glycols from a polyalkylene glycol dialkyl ether solution

A process is described for removing contaminants from a contaminant-laden solution of dialkyl ethers of polyethylene glycols (polyether solvent) by mixing the solution with an aqueous base solution. The mixture produces at least two liquid phases of different densities, which are then separated from each other. The lighter liquid phase is predominantly the polyether solvent while the heavier liquid phase is predominantly the aqueous base solution and the contaminants. The process is particularly useful in removing triethylene glycol and other glycol-based dehydration solvents.

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Robert E Steele