Cabot Corporation

Ricky W Kitchell

Jonathon L Kimmel

James Allen Fife

Sridhar Venigalla

Jeffrey A Kerchner

David M Reed

Dorran L Schultz

Stephen J Krause

Heather L Enman

Heather L Wolbach

Methods to at least partially reduce a niobium oxide are described wherein the process includes mixing the niobium oxide and niobium powder to form a powder mixture that is then heat treated to form heat treated particles which then undergo reacting in an atmosphere which permits the transfer of oxygen atoms from the niobium oxide to the niobium powder, and at a temperature and for a time sufficient to form an oxygen reduced niobium oxide. Oxygen reduced niobium oxides having high porosity are also described as well as capacitors containing anodes made from the oxygen reduced niobium oxides.

Methods of making a niobium metal oxide and oxygen reduced niobium oxides

Methods to at least partially reduce a niobium oxide are described. In one embodiment, a milling process is described wherein the surfaces of the mill in contact with the starting metal oxide, getter material, and/or oxygen reduced metal oxide are the same as the material being milled. Other milling techniques and products are also described.

Methods of making a niobium metal oxide

Methods to at least partially reduce a niobium oxide are described wherein the process includes heat treating the niobium oxide in the presence of a getter material and in an atmosphere which permits the transfer of oxygen atoms from the niobium oxide to the getter material, and for a sufficient time and at a sufficient temperature to form an oxygen reduced niobium oxide. Niobium oxides and/or suboxides are also described as well as capacitors containing anodes made from the niobium oxides and suboxides.

Methods to partially reduce a niobium metal oxide and oxygen reduced niobium oxides

Methods to at least partially reduce a niobium oxide are described wherein the process includes heat treating the niobium oxide in the presence of a getter material and in an atmosphere which permits the transfer of oxygen atoms from the niobium oxide to the getter material, and for a sufficient time and at a sufficient temperature to form an oxygen reduced niobium oxide. Niobium oxides and/or suboxides are also described as well as capacitors containing anodes made from the niobium oxides and suboxides. Anodes formed from niobium oxide powders using binders and/or lubricants are described as well as methods to form the anodes.

Oxygen reduced niobium oxides

The present invention relates to capacitor anodes containing a niobium oxide having an atomic ratio of niobium to oxygen of 1:less than 2.5 and being formed at a formation voltage of about 6 volts or higher. The present invention further relates to a niobium oxide having an atomic ratio of niobium to oxygen of 1:less than 2.5, and having a nitrogen content of from about 31,000 ppm N to about 130,000 ppm N . Capacitors containing the various types of niobium oxide are further described.

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Douglassville, PA, United States of America

Ricky W Kitchell