Rolls-royce High Temperature Composites Inc.

Rolls-royce Corporation

Richard W Kidd

Robert J Shinavski

Chong M Cha

David Liliedahl

Ross Galligher

Nicholas Doan

Sungbo Shim

Kang N Lee

Stephen Isaiah Harris

A method of making a ceramic matrix composite (CMC) that may show improved resistance to chemical attack from molten silicon along with excellent mechanical strength is described. The method includes forming an interphase coating on one or more silicon carbide fibers, depositing a matrix layer comprising silicon carbide on the interphase coating, oxidizing the matrix layer to form an oxidized film comprising silicon oxide, depositing a wetting layer comprising silicon carbide on the oxidized film. After depositing the wetting layer, a fiber preform containing the silicon carbide fibers is heat treated. After the heat treatment, the fiber preform is infiltrated with a slurry. After infiltration with the slurry, the fiber preform is infiltrated with a melt containing silicon, and then the melt is cooled to form a ceramic matrix composite.

Method of fabricating a ceramic matrix composite for resistance against silicon attack

A system may include a reactor vessel comprising an outer wall, a heat source thermally coupled to the reactor vessel, at least one reactor inlet in the outer wall, and at least one reactor outlet. The reactor vessel may be configured to house a porous preform in a radially central core region. The at least one reactor inlet may be configured to introduce a precursor gas to the reactor vessel to produce swirling flow of the precursor gas around the radially central core region of the reactor vessel. The at least one reactor outlet may be configured to remove exhaust gas from the reactor vessel and assist in maintaining a dynamic pressure of the reactor vessel greater than a pressure in the porous preform.

Swirled flow chemical vapor deposition

A method of forming a moisture-tolerant coating on a silicon carbide fiber includes exposing a silicon carbide fiber to a gaseous N precursor comprising nitrogen at an elevated temperature, thereby introducing nitrogen into a surface region of the silicon carbide fiber, and exposing the silicon carbide fiber to a gaseous B precursor comprising boron at an elevated temperature, thereby introducing boron into the surface region of the silicon carbide fiber. Silicon-doped boron nitride is formed at the surface region of the silicon carbide fiber without exposing the silicon carbide fiber to a gaseous Si precursor comprising Si. Thus, a moisture-tolerant coating comprising the silicon-doped boron nitride is grown in-situ on the silicon carbide fiber.

Method of forming a moisture-tolerant coating on a silicon carbide fiber

A ceramic matrix composite component for use in a gas turbine engine and method for making the same are described herein. The component includes a body and an outer region. The body includes a silicon containing ceramic composite. The outer region is on an outer surface of the body.

Modified atmosphere melt infiltration

A method includes heating, using a heat source, a reactor vessel including a substrate in a radially central core region of the reactor vessel and introducing, using at least one reactor inlet in an outer wall of the reactor vessel, a precursor gas to the reactor vessel. The at least one reactor inlet is configured to swirling flow of the precursor gas around the radially central core region of the reactor vessel. The material deposits on the substrate from the precursor gas. The method includes removing, using at least one reactor outlet, an exhaust gas from the reactor vessel.

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Rancho Palos Verdes, CA, United States of America

Richard W Kidd