Heraeus Quarzglas Gmbh & Co Kg

Other

Heraeus Electro-nite International N.v.

Ralph Sattmann

Martin Trommer

Jan Vydra

Manuel Rosenberger

Oliver Ganz

Michael Hünermann

Yasushi Fukui

Bodo Kuehn

Michael Huenermann

Rene Sowa

Kay Schuster

Achim Hofmann

Thomas Bogdahn

Harald Hain

Clemens Schmitt

Steffen Zwarg

Peter Bauer

Enrico Ehrentraut

Norbert Cibis

David Kostka

Yusuf Tansel

Joachim Peekhaus

Joerg Werner

Oliver Humbach

Hidenori Ochiai

Tomomitsu Yaginuma

Toru Ikeda

Benjamin Reis

Michael HÜNERMANN

A high degree of precision and an exact positioning of anti-resonant elements in a sufficiently stable and reproducible manner is achieved in that a step of providing a cladding tube includes a processing measure, in which the cladding tube wall is machined with a longitudinal structure extending in the direction of the cladding tube longitudinal axis in the region of the target positions.

Methods for producing a hollow-core fiber and for producing a preform for a hollow-core fiber

Methods are known for producing an anti-resonant hollow-core fiber which has a hollow core extending along a fiber longitudinal axis and an inner jacket region that surrounds the hollow core, said jacket region comprising multiple anti-resonant elements. The known methods have the steps of: providing a cladding tube that has a cladding tube inner bore and a cladding tube longitudinal axis along which a cladding tube wall extends that is delimited by an interior and an exterior; providing a number of tubular anti-resonant element preforms; arranging the anti-resonant element preforms at target positions of the interior of the cladding tube wall, thereby forming a primary preform which has a hollow core region and an inner jacket region; and elongating the primary preform in order to form the hollow-core fiber or further processing the primary preform in order to form a secondary preform. The aim of the invention is to achieve a high degree of precision and an exact positioning of the anti-resonant elements in a sufficiently stable and reproducible manner on the basis of the aforementioned methods. This is achieved in that the step of providing and/or arranging the anti-resonant element preforms and/or the process of carrying out a hot-forming process includes a fixation measure and/or a sealing measure using an amorphous SiOparticle-containing sealing or joining compound.

Methods are known for producing an anti-resonant hollow-core fiber which has a hollow core extending along a fiber longitudinal axis and an inner jacket region that surrounds the hollow core, said jacket region comprising multiple anti-resonant elements. The known methods have the steps of: providing a cladding tube that has a cladding tube inner bore and a cladding tube longitudinal axis along which a cladding tube wall extends that is delimited by an interior and an exterior; providing a number of tubular anti-resonant element preforms; arranging the anti-resonant element preforms at target positions of the interior of the cladding tube wall, thereby forming a primary preform which has a hollow core region and an inner jacket region; and elongating the primary preform in order to form the hollow-core fiber or further processing the primary preform in order to form a secondary preform. The aim of the invention is to achieve a high degree of precision and an exact positioning of the anti-resonant elements in a sufficiently stable and reproducible manner on the basis of the aforementioned methods. This is achieved in that a positioning template is inserted into the cladding tube inner bore in order to arrange the anti-resonant element preforms, said template having holding elements for positioning the anti-resonant element preforms at the target positions.

Methods for producing an optical fiber by elongating a silica glass blank or a coaxial group of silica glass components, on the basis of which a fiber is obtained that comprises a core zone, an inner jacket zone enclosing the core zone and a ring zone surrounding the inner jacket zone, are known. In order to provide, proceeding from this, a method, a tubular semi-finished product and a group of coaxial components for the cost-effective production of an optical fiber, which is characterized by a high quality of the boundary between the core and jacket and by low bending sensitivity, according to the invention, the silica glass of the ring zone is provided in the form of a ring zone tube made of silica glass having a mean fluorine content of at least 6000 weight ppm and the tube has an inner tube surface and an outer tube surface, wherein via the wall of the ring zone tube, a radial fluorine concentration profile is adjusted which has an inner fluorine depletion layer with a layer thickness of at least 1 &#x3bc;m and no more than 10 &#x3bc;m, in which the fluorine content decreases toward the inner tube surface and is no more than 3000 weight ppm in a region close to the surface which has a thickness of 1 &#x3bc;m.

Tubular semifinished product for producing an optical fiber

Method and tubular semifinished product for producing an optical fiber

The present invention refers to a drawing method for producing cylindrical components of quartz glass in that a quartz glass strand is drawn off in the direction of a drawing axis from a shaping zone of soft quartz glass mass and sections having a cutting length are separated from the quartz glass strand, and the cylindrical components are produced from the sections.

Drawing method for producing cylindrical-shaped components from quartz glass

In a conventional method for the production of an optical component made from quartz glass, a coaxial arrangement with a core rod, surrounded by a quartz glass envelope tube comprising an evacuable inner drilling, is introduced in the vertical direction into a heating zone, softened therein by sections and, with formation of a drawing bulb, elongated to give the quartz glass component. According to the invention, a simple and cheap method based on the above, permitting the production of high-grade optical components by elongation of a coaxial arrangement of core rod and an enveloping tube with great economy, may be achieved, whereby a core rod is used, comprising at least two separate core rods arranged one above the other in the inner drilling and the weight of an upper core rod section is taken by a mounting or support region of the enveloping tube, provided above the drawing bulb.

Method for the production of an optical component made from quartz glass

This method for drawing a quartz glass optical component shortens the pulling process and minimizes loss of material. An end face of a quartz glass hollow cylinder forms a tapered end portion to an attachment piece of quartz glass having a bore. The inner bore of the hollow cylinder and the bore of the attachment piece are at least temporarily interconnected fluidically as a passage bore. A cleaning fluid is passed through the inner bore of the hollow cylinder and the passage bore. A core rod of quartz glass, which rests on a contact surface of the attachment piece, is inserted into the inner bore of the hollow cylinder, and the hollow cylinder is continuously supplied to a heating zone, heated therein so as to form a drawing bulb, and the component is continuously drawn therefrom.

Elongation method for producing an optical component of quartz glass and preliminary product suited for performing the method

The production of an optical component from quartz glass by elongation of a coaxial arrangement of a core rod and a hollow cylinder is known. The arrangement is thus introduced into a heating zone, such that the lower end begins to partly soften and the component drawn from the softened part. According to the invention, a pseudo-continuous method for the formation of the restriction in the inner passage of the hollow cylinder on which the core rod is supported, is disclosed, whereby an upper hollow cylinder is fused end on with a lower hollow cylinder to form an axial composite cylinder, a core rod is introduced into the lower hollow cylinder and the axial cylinder composite partly softened and elongated to form the optical component. A drawing bulb extending to the upper hollow cylinder forms, within which the inner passage at least partly collapses with formation of the restriction and the upper cylinder is then separated off from the drawn optical component at a separating plane and then elongated together with a core rod to form an optical component.

Method for production of an optical component from quartz glass

An immersion sensor for analysis of liquids or melts includes an immersion carrier, a detector and a radiation-guiding unit, and a sample chamber arranged in the immersion carrier. The sample chamber has an inlet opening for liquid or melt, and the sensing components for measurement of the liquid or melt act inside the sample chamber.

Immersion lance for analysis of melts and liquids

The production of an optical component from quartz glass, by elongation of a coaxial arrangement of a core rod and a hollow cylinder of a given length, is known. The arrangement is thus introduced into a heating zone with a vertical orientation, such that the lower end begins to partly soften and the component is drawn downwards from the softened part. The hollow cylinder has an inner passage, provided with a restriction in the region of the lower end thereof, on which the core rod is supported. Several methods are disclosed for formation of the restriction in which the inner passage () is mechanically machined to a final dimension and, in one version of the method, the restriction in the inner passage () is generated by means of softening the lower end face of the hollow cylinder, swaged against a tool and thus folded inwards with formation of a peripheral bead ring.

Method for production of an optical component made from quartz glass

A method for measuring trace quantities of OH groups in quartz glass comprises preparing a set of test pieces comprising a reference test piece from a blank of a quartz glass body whose OH group content is known and a sample test piece from a quartz glass body whose OH group content is to be measured, having two planar planes faced to each other, setting the sample test piece and the reference test piece in an infrared spectrophotometer; successively irradiating perpendicular to one of the two planar planes an incident infrared radiation in a wavelength region of approximately 2500 nm to approximately 2950 nm, while simultaneously detecting the outgoing radiation spectrum from the other plane; obtaining the difference of the outgoing radiation spectrum of each of the test pieces; selecting the absorbance peak assigned to OH groups at a wavelength of 2720 nm to obtain the peak height thereof; and calculating the concentration of OH groups from the peak height in the sample test piece.

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Aschaffenburg, Germany

Ralph Sattmann