Standard Oil Company (indiana)

Dresser Engineering Company

Ralph G Ruth

John W Palm

Robert L Reed

An energy efficient process for the separation of two close boiling point components contained in a multi-component feed stream. The feed stream is distilled in a first column to produce a relatively light fraction containing substantially all the more volatile close boiling point component, along with part of the less volatile close boiling point component and a bottoms product. The relatively light overhead fraction from the first column is fed to a second column to produce an overhead product, consisting substantially of the more volatile close boiling point component and a bottoms product consisting substantially of the less volatile boiling point component. The bottoms product from the first column is fed to a third column to produce an overhead vapor consisting substantially of the less volatile close boiling point component, which overhead vapor is passed to the second column to supply part of the reboiling energy requirements for said column. A portion of the bottoms product from the second column is recycled to the top of the third column for use as reflux.

Energy efficient distillation process

Claus-type processes used in the past to recover sulfur from low H.sub.2 S acid gas, in the presence of hydrocarbon or other impurities which are harmful to the Claus catalyst, have required the use of straight-through operation with the burning of supplemental fuel gas to maintain the required combustion temperature in the furnace. A method for conserving the amount of additional fuel gas required involving utilization of the excess heat of combustion to preheat the acid gas and oxygen-containing streams to a temperature in excess of 600.degree. F prior to combustion is described. Additional energy savings are achieved by preheating the Claus tail gas effluent prior to incineration.

Growing community of inventors

Tulsa, OK, United States of America

Ralph G Ruth