Degussa Aktiengesellschaft

Evonik Degussa Gmbh

Ralf Jantke

Steffen Hasenzahl

A process for the production of a titanium silicalite shaped article by: a) preparation of a synthesis gel containing a Sisource, a Tisource, a template compound and water, b) crystallization of the synthesis gel under hydrothermal conditions, c) drying of the titanium silicalite from step b) at a temperature below the decomposition temperature of the template compound, d) preparation of a formable mass containing the product from step c), a binder and a paste-forming agent, e) forming of the mass from step d) into a green shaped article, f) optionally drying, and g) calcinations of the green shaped article, as well as a titanium silicalite shaped article obtainable according to this process, and the use of this shaped article as a catalyst in epoxidation or ammoximation reactions.

Process for the production of a titanium silicalite shaped article

The present invention relates to a process for the production of a titanium silicalite shaped body by: (a) forming a formable composition containing titanium silicalite, a binder and a pasting agent, so that the Curd curve of the formable composition has a plateau value in the range from 20 to 90 mm; (b) shaping the composition of step (a) to form a green body; (c) optionally drying and (d) calcining the green body, to a titanium silicalite shaped body obtainable by that process, and to the use of such titanium silicalite shaped bodies in the epoxidation of olefins or the ammoximation of ketones.

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Mömbris, Germany

Ralf Jantke