Baker Hughes, a Ge Compnay, LLC

Baker Hughes Holdings LLC

Georgia Tech Research Corporation

Qusai Darugar

Valery Khabashesku

Sankaran Murugesan

Radhika Suresh

Oleg Antonovych Mazyar

Oleksandr V Kuznetsov

Darryl Ventura

Devesh Kumar Agrawal

Rostyslav Dolog

Bradley G Harrell

D V Satyanarayana Gupta

Dennis K Clapper

Jianzhong Yang

Mostafa A El-Sayed

Joseph J Arensdorf

Wei Qian

Stephen Mark Heath

Billy M Dye

Ibraheem T Hussain

Melissa V McCray

Alyssa Renee Garcia

Valery N Khabashesku

Darryl N Ventura

A method of fracturing multiple productive zones of a subterranean formation penetrated by a wellbore is disclosed. The method comprises injecting a fracturing fluid into each of the multiple production zones at a pressure sufficient to enlarge or create fractures in the multiple productive zones, wherein the fracturing fluid comprises an upconverting nanoparticle that has a host material, a dopant, and a surface modification such that the upconverting nanoparticle is soluble or dispersible in water, a hydrocarbon oil, or a combination thereof; recovering a fluid from one or more of the multiple production zones; detecting the upconverting nanoparticle in the recovered fluid by exposing the recovered fluid to an excitation radiation having a monochromatic wavelength; and identifying the zone that produces the recovered fluid or monitoring an amount of water or oil in the produced fluid by measuring an optical property of the upconverting nanoparticle in the recovered fluid.

Upconverting nanoparticles as tracers for production and well monitoring

A method of reducing water saturation onto surfaces exposed to hydrocarbons during the production of hydrocarbons from subterranean formations by altering the wettability of the surface of the formation with surface modified nanoparticles.

Methods of altering the wettability of surfaces to enhance hydrocarbon production

A composition of matter includes a liquid and nanoparticles suspended in the liquid. The nanoparticles each include silica, alumina, and an organosilicon functional group having a molecular weight of at least 200. A method includes functionalizing a surface of nanoparticles with an organosilicon functional group and dispersing the nanoparticles in a liquid to form a suspension. The functional group has a molecular weight of at least 200. The nanoparticles each include silica and alumina at a surface thereof.

Methods including functionalizing nanoparticles and forming suspensions

A method of recovering hydrocarbons comprises introducing a suspension comprising nanoparticles to a material and contacting surfaces of the material with the suspension. After introducing the suspension comprising the nanoparticles to the material, the method further includes introducing at least one charged surfactant to the material and removing hydrocarbons from the material. Accordingly, in some embodiments, the nanoparticles may be introduced to the material prior to introduction of the surfactant to the material. Related methods of recovering hydrocarbons from a material are also disclosed.

Methods of recovering a hydrocarbon material

A method of making a thin film substrate involves exposing carbon nanostructures to a crosslinker to crosslink the carbon nanostructures. The crosslinked carbon nanostructures are recovered and disposed on a support substrate. A thin film substrate includes crosslinked carbon nanostructures on a support substrate. The crosslinked carbon nanostructures have a crosslinker between the carbon nanostructures. A method of performing surface enhanced Raman spectroscopy (SERS) on a SERS-active analyte involves providing a SERS-active analyte on such a thin film substrate, exposing the thin film substrate to Raman scattering, and detecting the SERS-active analyte.

Thin film substrates including crosslinked carbon nanostructures and related methods

A cyanide-functionalized gold nanoparticle. A method of making cyanide-functionalized gold nanoparticles includes forming an aqueous reaction mixture comprising a gold precursor and glycine, keeping the reaction mixture at about 18&#xb0; C. to about 50&#xb0; C. for at least 6 days to provide formation of the cyanide-functionalized gold nanoparticles, and isolating the cyanide-functionalized gold nanoparticles from the reaction mixture. A method of analyzing a sample, comprising contacting cyanide-functionalized gold nanoparticles with the sample and performing an analytical method on the sample. A sensor comprises cyanide-functionalized gold nanoparticles.

Process for making cyano functionalized gold nanoparticles

A method of analyzing a well sample for a well treatment additive includes contacting the sample with functionalized metallic nanoparticles that contain metallic nanoparticles functionalized with a functional group including a cyano group, a thiol group, a carboxyl group, an amino group, a boronic acid group, an aza group, an ether group, a hydroxyl group, or a combination including at least one of the foregoing; irradiating the sample contacted with the functionalized metallic nanoparticles with electromagnetic radiation at a selected energy level; measuring a Raman spectrum emitted from the sample; and determining presence, type or concentration of the well treatment additive in the sample from the Raman spectrum.

Detection of trace chemicals in oil and gas applications

Compositions of matter comprising suspended nanoparticles and related methods

A method of determining a property within a subterranean formation comprises introducing silica nanoparticles into a well; obtaining a sample of a fluid produced from the well; and analyzing the sample for presence of the silica nanoparticles, wherein the silica nanoparticles comprise a core, a donor chromophore, an acceptor chromophore, and an outer silica shell; the donor chromophore and the acceptor chromophore being selected such that an emission spectrum of the donor chromophore overlaps with an absorption spectrum of the acceptor chromophore.

Multicolor fluorescent silica nanoparticles as tracers for production and well monitoring

Base oil can be recovered from contaminated O/SBF by combining a chemical process with a mechanical process. The chemical treatment includes adding a demulsifier, an anionic surfactant, a non-ionic surfactant and/or a mutual solvent to the contaminated O/SBF in an amount effective to separate the base oil from the contaminated O/SBF fluid followed by mechanical separation of oil from water, and optionally from any solids present. The recovered base oil (i.e. conventional drilling fluid, conductive drilling fluid and constant rheology drilling fluid, etc.) may then be reformulated to make a new OBM of the same type from which the base oil was recovered, or as a fuel for engines.

Recovering base oil from contaminated invert emulsion fluid for making new oil-/synthetic-based fluids

A method of treating a fluid in a subterranean formation comprises injecting a fluid into the subterranean formation, the fluid containing dissolved oxygen; contacting the fluid with an oxygen removal device, the oxygen removal device comprising an anode, a cathode comprising metallic nanoparticles loaded on a support, an ion exchange membrane disposed between, and electrically separating the anode and the cathode, and a power source electrically coupled to the anode and the cathode; and reducing the amount of the dissolved oxygen in the fluid.

Electrochemical methods of removing dissolved oxygen from drilling or completion fluids

Capped nanoparticles may be added to an oil-based fluid to improve the electrical conductivity of the oil-based fluid. The oil-based fluid may be a drilling fluid, a completion fluid, a drill-in fluid, a stimulation fluid, a servicing fluid, and combinations thereof. In a non-limiting embodiment, the oil-based fluid composition may be circulated in a subterranean reservoir wellbore.

Electrically conductive oil-based fluids

A system and method for estimating a concentration of monoethanolamine (MEA) in a fluid. A substrate for supporting a sample of the fluid during testing includes a carbon nanotube mat layer, a silver nanowire layer disposed on the carbon nanotube mat layer, and a chemical enhancer layer disposed on the silver nanowire layer. A sample of the fluid is placed on the substrate, and the fluid sample is radiated with electromagnetic radiation at a selected energy level. A detector measures a Raman spectrum emitted from the sample in response to the electromagnetic radiation. A processor estimates the concentration of MEA in the sample from the Raman spectrum and adds a corrosion inhibitor to the fluid in an amount based on the estimated concentration of MEA to reduce the concentration of MEA in the fluid.

Growing community of inventors

Houston, TX, United States of America

Qusai Darugar