Zhejiang Huangma Technology Co., Ltd.

Zhejiang Huangma Shangyi New Material Co., Ltd.

Zhejiang Lukean Chemical Co., Ltd.

Shangyu Huangma Surface Activated Reagent Research Institute Co., Ltd.

Qingmei Wan

Yifeng Jin

Weisong Wang

Majishi Wang

Hongjun Gao

Dinglian Ma

Ran Kou

Related are a high-molecular weight allyl alcohol polyoxyethylene polyoxypropylene ether and a preparation method. During preparation, an allyl alcohol raw material and a supported catalyst Rb-NHPA are firstly added into a high-pressure reaction kettle, and it is heated after being replaced with a nitrogen gas; then after the internal temperature of the reaction kettle is raised to a reaction temperature, an ethylene oxide (EO) and propylene oxide (PO) mixture is continuously fed for a reaction; and finally, after the internal temperature of the reaction kettle is reduced, an acetic acid is dropwise added into the reaction kettle so that the crude product of the high-molecular weight allyl alcohol polyoxyethylene polyoxypropylene ether is neutralized to be neutral. The refining process of a polyether is omitted, the process flow is greatly simplified, and the process time is effectively saved. In addition, the supported catalyst Rb-NHP may be recycled.

High-molecular weight allyl alcohol polyoxyethylene polyoxypropylene ether and preparation method

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Zhejiang, China

Qingmei Wan