Owens-Illinois Plastic Products Inc.

Prakash R Ajmera

Saleh A Jabarin

A method for making a partially crystalline, biaxially oriented heat set hollow polyethylene terephthalate free standing container from a hollow parison having an open end and a closed end including engaging the open end of a plastic parison which is at a temperature within its molecular orientation temperature range, positioning a mold base in axial alignment with said engaged hot parison, enclosing a hot mold about the mold base, the mold being at heat setting temperature and the mold base being at a temperature preferably significantly lower than the mold, expanding the plastic parison within the hot mold and mold base by internal pressurization to induce biaxial orientation of the plastic parison and force the plastic parison into intimate contact and conformance with the hot mold and to maintain contact by such internal pressurization between the mold and mold base and the biaxially oriented container for a time sufficient to induce partial crystallization in the side wall and base of the biaxially oriented container, reducing the internal pressure in the blown container, opening the hot mold while maintaining engagement of the open end of the blown hollow container, disengaging the hot mold base from the blown container, maintaining a lower internal pressurization of the container to prevent significant shrinkage, and engaging a cold mold base with the base of the container, and enclosing a cold mold about the container and the mold base to cool the container while maintaining engagement of the open end with the container and maintaining pressure in the container at least sufficient to prevent shrinkage, and opening the cold mold and releasing the container.

Method of making partially crystalline biaxially oriented hollow plastic

A method and apparatus for making a partially crystalline, biaxially oriented heat set hollow plastic container from a hollow parison having an open end and a closed end including engaging the open end of a plastic parison which is at a temperature within its molecular orientation temperature range, enclosing the hot parison in a hot mold, which is at heat setting temperature, expanding the plastic parison within the hot mold by internal pressurization to induce biaxial orientation of the plastic parison and to induce partial crystallization in the biaxially oriented container, exhausting the blow molding fluid while continuously introducing a cooling fluid such as liquid carbon dioxide into the biaxially oriented container and continuously removing the cooling fluid while the hot mold is closed for a period of time, opening the hot mold while continuing to introduce, circulate and remove coolant fluid for a predetermined period of time until the container is cooled sufficiently to prevent significant shrinkage and finally releasing the container.

Heat set method for oval containers

A method including engaging the open end of a first plastic parison which is at a temperature within its molecular orientation temperature range, enclosing a hot mold which is at heat setting temperature about the parison at a first position, simultaneously enclosing a cold mold at a second position about a container previously blown in the hot mold to cool the previously blown container, expanding the plastic parison within the hot mold by internal pressurization through the open end to induce biaxial orientation of the plastic parison and force the plastic parison into intimate contact and conformance with the hot mold and to maintain contact by such internal pressurization between the mold and biaxially oriented container for a time sufficient to induce partial crystallization in the biaxially oriented container, moving the hot mold and the cold mold in unison to bring the hot mold to the second position and the cold mold to a third position during the expanding of the parison within the hot mold and during the cooling of the previously blown container in the cold mold, maintaining a lower internal pressurization of the container in the hot mold and exhausting the pressurization to atmospheric pressure in the cold mold, substantially simultaneously opening the hot mold and cold mold, moving the open hot mold to the first position and open cold mold to the second position.

Method for making partially crystalline biaxially oriented heat set

A method and apparatus of forming a hollow partially crystalline heat set biaxially oriented polyethylene terephthalate container having a hemispherical base comprising blowing a heated parison at orientation temperature outwardly against the confines of a mold which is at heat setting temperature wherein the side wall and the major portion of the base of the container are subjected to a heat setting temperature and the center of the base of the container is subjected to a temperature not greater than 150.degree. C. so that the central portion is crystallized a substantially lesser amount than the side wall and the major portion of the base. The container is then quenched. The resultant container can be formed at a rapid cycle and has good drop impact properties and obviates the problems of sticking to the hot mold or blow out when the hot mold is opened.

Method for forming hollow partially crystalline biaxially oriented heat

A method for making a partially crystalline, biaxially oriented heat set hollow plastic container from a hollow poly(ethylene) terephthalate parison having an open end and a closed end comprising engaging the open end of a plastic parison which is at a temperature within its molecular orientation temperature range, enclosing a hot mold about the hot parison, the mold being at heat setting temperature, expanding the plastic parison within the hot mold by internal pressurization to induce biaxial orientation of the plastic parison and force the plastic parison into intimate contact and conformance with the hot mold and to maintain contact by such internal pressurization between the mold and the biaxially oriented container for a time sufficient to induce partial crystallization in the biaxially oriented container, maintaining a lower internal pressurization of the container to prevent significant shrinkage, opening the hot mold while maintaining engagement of the open end of the blown hollow container, enclosing the blown hollow container in a cold mold having substantially the same volume as the hot mold, or smaller, increasing the pressurization to force the container into intimate contact with the cold mold to cool the container while maintaining internal pressurization and then exhausting the pressure and opening the cold mold. The method results in a thermally stable container.

Method of making partially crystalline biazially oriented heat set

A method for making a partially crystalline, biaxially oriented heat set hollow plastic container from a hollow parison having an open end and a closed end comprising engaging the open end of a plastic parison which is at a temperature within its molecular orientation temperature range, positioning a mold base in axial alignment with said engaged hot parison, enclosing a hot mold about the mold base, the mold being at heat setting temperature, expanding the plastic parison within the hot mold and mold base by internal pressurization to induce biaxial orientation of the plastic parison and force the plastic parison into intimate contact and conformance with the hot mold and to maintain contact by such internal pressurization between the mold and the biaxially oriented container for a time sufficient to induce partial crystallization in the biaxially oriented container, lowering the internal pressure in the container, opening the hot mold while maintaining engagement of the open end and engagement of the mold base with the blown hollow container, maintaining a lower internal pressurization of the container to prevent significant shrinkage, and cooling the container while maintaining engagement of the open end and engagement of the mold base with the container and maintaining pressure in the container at least sufficient to prevent shrinkage.

A multilayer biaxially oriented heatset article and method of making forming a preform comprising an outer layer and an inner layer of poly(ethylene terephthalate) (PET), an intermediate layer of olefin-vinyl alcohol copolymer, a layer of adhesive laminating the olefin-vinyl alcohol copolymer layer and the outer layer and a layer of adhesive laminating the inner olefin-vinyl alcohol copolymer layer and the inner layer. The preform is then heated to orientation temperature and blown against a heatset hot mold to produce an article such as a container that has high barrier properties, improved thermal stability, i.e., capable of being hot filled at elevated temperatures, have layer uniformity, good interlayer adhesion., good transparency and is light in weight.

Multilayer biaxially oriented heat set articles

A high barrier heatset intimate fusion blend article is disclosed where the article includes a blend of a high barrier copolyester, formed from terephthalic acid, ethylene glycol and 1,3 bis(2-hydroxyethoxy) benzene, and poly(ethylene terephthalate) (PET). The PET/copolyester blend articles are formed using a blowmolding and heatsetting process to rapidly achieve a high percentage of crystallinity of the PET in the article. The articles have excellent gas barrier and mechanical strength properties, high thermal stability and remain optically clear after heatsetting.

Heatset high barrier container

A hollow transparent delamination resistant heatset multilayer article is disclosed where the article includes at least one barrier layer containing a copolyester formed from terephthalic acid, ethylene glycol and 1,3 bis(2-hydroxyethoxy) benzene directly adhered to at least one layer containing poly(ethylene) terephthalate (PET). The multilayer articles are blowmolded using a heatsetting process. The heatset multilayer articles retain high gas barrier properties, uniform thickness in layers, and desirable mechanical strength properties even after the heatsetting process. Also, the multilayer heatset articles have excellent interlayer adhesion without the need for an adhesive layer, high thermal stability, and remain optically clear after the heatsetting process.

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Toledo, OH, United States of America

Prakash R Ajmera