Varian Australia Pty Ltd

Varian, Inc.

Philip V Wilson

Michael Ron Hammer

Christopher Webb

Martin Keith Masters

Dower Cameron Bricker

Peter G Layton

Stewart R Campbell

Mark R Williams

A calibrated spectroscopy instrument and a method for calibrating a spectroscopy instrument are disclosed. The spectroscopy instrument includes a monochromator having a drive mechanism comprising a pair of spur gears for rotating a diffraction grating of the monochromator for selecting a desired wavelength. The drive mechanism is calibrated to account for eccentricities in the spur gears to provide an accurate conversion between selected angular settings for the drive mechanism and the wavelength of the diffracted light from the monochromator. The drive mechanism comprises a pinion spur gear and a main spur gear which each have an AGMA (American Gear Manufacturers' Association) rating of at least 10, which allows errors due to random tooth to tooth variations to be neglected. A calibration algorithm is derived which is based on the error due to eccentricities in the spur gears following a precise geometric cyclic pattern.

Calibrated spectroscopy instrument and method

A method and apparatus for the spectrochemical analysis of a sample in which a solid state array detector ( ) is used to detect radiation ( ) of spectrochemical interest. The invention involves the use of a shutter ( ) adjacent the entrance aperture ( ) of a polychromator ( ) to expose the detector ( ) to the radiation ( ) for varying lengths of time whereby for short duration exposure times charge accumulation in elements (i.e. pixels) of the detector ( ) due to high intensity components of the radiation is limited and for longer exposure times charge accumulation in elements (pixels) of the detector ( ) due to feeble intesity components of radiation ( ) is increased. This ensures that each reading of the detector ( ) includes at least one exposure in which the amount of charge accumulated at each wavelength of interest is neither too little or too great. The problems of feeble radiation components not being accurately measurable and of high intensity radiation components exceeding the charge carrying capacity of elements (pixels) of the detector ( ) are thereby able to be avoided. An attenuator ( ) may be placed between the radiation source ( ) and the detector ( ) to permit longer exposure times to be used for very high intensity radiation.

Method and apparatus for spectrochemical analysis

A spectral interval excited by ICP-ES containing expected lines is modeled from wavelength calibration information and from spectra of model components. A sample is then excited and fit to the data with concurrent observation of wavelength calibration and a linear least squares fit obtained with analysis of residuals to determine presence of unexpected spectral features which, if present, provide additional model components for an iterative fitting.

Fast automated spectral fitting method

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Mount Waverley, Australia

Philip V Wilson