H.c. Starck Gmbh

Wyman Gordon Corporation

Materion Newton Inc.

Peter R Jepson

Dincer Bozkaya

Prabhat Kumar

Steven Alfred Miller

Paul R Aimone

Gary Alan Rozak

Richard Wu

Joseph Hirt

David Meendering

Jerome O'Grady

Timothy Welling

James G Daily, Iii

Hugo E Delgado

Timothy E Howson

Martin M Morra

Paul D Antaya

Thomas F Doherty

Paul J Gargolinski

Howard V Goldberg

Rong-Chein Richard Wu

Brad Lemon

Jack M Hyzak

James E Shannon, Iii

Henning Uhlenhut

David G Schwarz

Davd G Schwarz

James G Iii Daily

Jerone O´Grady

A refractory metal plate is provided. The plate has a center, a thickness, an edge, a top surface and a bottom surface, and has a crystallographic texture (as characterized by through thickness gradient, banding severity; and variation across the plate, for each of the texture components 100//ND and 111//ND, which is substantially uniform throughout the plate.

Refractory metal plates

A refractory metal plate is provided. The plate has a center, a thickness, an edge, a top surface and a bottom surface, and has a crystallographic texture (as characterized by through, thickness gradient, banding severity; and variation across the plate, for each of the texture components 100//ND and 111//ND, which is substantially uniform throughout the plate.

Refractory metal plates with improved uniformity of texture

In accordance with various embodiments, plates are formed via a plurality of upset-forging and forging-back cycles followed by a plurality of rolling passes.

Refractory metal pots

In various embodiments, tubular sputtering targets are produced by forming a tubular billet at least by pressing molybdenum powder in a mold and sintering the pressed molybdenum powder, working the tubular billet to form a worked billet, and heat treating the worked billet.

Methods of forming molybdenum sputtering targets

Methods and apparatus for rolling metal sheet or plate are provided. The method comprises the step of feeding the metal plate or sheet into a rolling mill at an angle. The apparatus comprises a rolling mill having a tilted feed table, or an apron upon which a transfer table and tilted feed table can rest. Through-thickness gradient and shear texture can be improved using the methods and apparatus of the invention.

Methods and apparatus for controlling texture of plates and sheets by tilt rolling

Molybdenum, sputtering targets and sintering characterized as having no or minimal texture banding or through thickness gradient. The molybdenum sputtering targets having a fine, uniform grain size as well as uniform texture, are high purity and can be micro-alloyed to improved performance. The sputtering targets can be round discs, square, rectangular or tubular and can be sputtered to form thin films on substrates. By using a segment-forming method, the size of the sputtering target can be up to 6 m&#xd7;5.5 m. The thin films can be used in electronic components such as Thin Film Transistor-Liquid Crystal Displays, Plasma Display Panels, Organic Light Emitting Diodes, Inorganic Light Emitting Diode Displays, Field Emitting Displays, solar cells, sensors, semiconductor devices, and gate device for CMOS (complementary metal oxide semiconductor) with tunable work functions.

Molybdenum tubular sputtering targets with uniform grain size and texture

Computer-implemented processes for making refractory metal pots, including: cutting an a refractory metal ingot into a first workpiece; subjecting the first workpiece to multiple upset forgings, annealings in a vacuum or inert gas to a temperature sufficiently high to cause at least partial recrystallization, forging-backs, and rollings to form a plate; wherein the forged, annealed workpiece undergoes a reduction in thickness after at least one rolling pass and is turned between at least one pass, to form the plate; and deep drawing the plate to form a pot; wherein dimensions of at least one workpiece or plate suitable for processing into a pot are pre-determined with a computer-implemented finite element modeling assessment method.

Refractory metal products, such as tantalum, can be rejuvenated after metal consumption in selected zones by filling the zones with powder and simultaneously applying focused radiant energy to the powder.

Rejuvenation of refractory metal products

A process to chemically refine and consolidate tantalum, niobium and their alloys to a fabricated product of net shape or near-net shape with higher throughput, more consistency, and lower manufacturing costs compared to prior art routes or rejuvenate damaged and deteriorated refractory metal parts. Powder metal is loaded into hoppers to be fed into laser forming/melting equipment. A suitable substrate is loaded into a laser forming/melting chamber onto which the powder will be deposited and consolidated in a point-scan process. As the powder is fed onto successive points of the surface of the substrate in linear traces, the laser is used to heat and partially melt the substrate and completely melt the powder. A combined deposition and melt beam traces the substrate surface repeatedly over a selected area to build up a dense coating of controlled microstructure in multiple layers. A fully dense deposit is built up that becomes the desired shape.

Refractory metal and alloy refining by laser forming and melting

A forging press includes a die set having a stationary die, a movable die in facing-but-spaced-apart relation to the stationary die along a press axis and defining a workpiece volume therebetween, and an exterior constraint extending circumferentially around the workpiece volume. The movable die has a base level region lying generally in a workpiece plane perpendicular to the press axis, and three rotationally symmetric segments raised above the base level region. Each of the segments forms an angular segment of a disk having an included segment angle and that is angularly separated from the other segments. A press mechanism includes a axial drive operable to move the movable die in a direction parallel to the press axis, and an indexing drive operable to rotate the movable die about the press axis by an indexing rotational angle. In operation, the axial drive performs a press stroke and retracts, the indexing drive rotates the movable die by the indexing rotational angle of less than the included segment angle, and the axial drive performs another press stroke. By repeating these steps, the entire workpiece is forged incrementally.

Closed-die forging process and rotationally incremental forging press

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Newbury, MA, United States of America

Peter R Jepson