Ashland Oil, Inc.

Paul W Walters

Lloyd E Busch

Oliver J Zandona

Roger M Benslay

H Anthony Raiche

George D Myers

Dwight F Barger

William P Hettinger, Jr

Billy T Fritz

Ronald L Harness

Genaro M Quodala

Steven W Murray

Ricky L Adkins

Robert L Cottage

James R Riggs

A V Peppard

William M Rice

A vented cup ballistic separation device and method of use for achieving rapid separation of a suspension of fluidized solid particulate and gasiform material. The vented cup ballistic separation apparatus is useful in a wide variety of vapor-solid contacting devices where rapid separation of solids from vapor is desired e.g. in fluidized catalytic cracking systems. The vented cup ballistic separation apparatus particularly comprises annular chamber about the outer periphery of an open ended riser conduit. The annular chamber is open in the upper end and one or more open end conduits extend outwardly from the annular chamber to provide means for discharging vapors and also for attachment of cyclone separation means if desired. The riser with vented cup or annular chamber preferably terminates within a larger diameter chamber.

Carbometallic oil conversion with ballistic separation

A process for upgrading topped crude oils and residual portions comprising material boiling above 552.degree. C. (1025.degree. F.) by the combination of partial demetallizing and decarbonizing of the residual oil before effecting zeolite catalytic cracking thereof is described in conjunction with a product separation process, a combined hydrocarbon gas product concentration section and the use of parallel arranged CO boilers to produce sulfur free flue gas and steam. Steam generated by the combination operation effectively reduces the energy requirement of the combustion process.

Combination process for upgrading residual oils

An apparatus for separating solids and vapors from a suspension of the two materials is disclosed. The solids are directed through a conoid element to enhance directional flow and to prevent return of solids to the separation apparatus.

Apparatus for the separation of solid particulates from a gaseous

A process for upgrading residual portions of crude oils comprising metal contaminants and Conradson Carbon contributing components by the combination of thermal visbreaking with fluid inert solids and catalytic upgrading of naphtha and higher boiling components of thermal visbreaking in separate systems of riser conversion and solids regeneration is discussed. Heat management of the regeneration systems is restricted in substantial measure by a novel external solids heat exchange apparatus arrangement utilized to partially cool hot regenerated solids utilized in the solids regeneration systems.

Method and apparatus for cooling fluid solid particles used in a

A method and arrangement of apparatus employed is described for regenerating solid particles comprising carbonaceous deposits. At least three sequential stages of separation of flue gases from entrained solids are provided in association with an upflow catalyst regeneration operation.

Regeneration of fluid solid particles and separation of solid particles

Solids e.g. catalysts are separated from suspensions in gases e.g. products from catalytic cracking of crude oil fractions a discharging of suspensions against a surface positioned above the outlet of a riser conduit through which the suspensions are flowing and collecting the displaced gases for passage to cyclones.

Fluid particle material regeneration method and apparatus

An apparatus for upgrading residual portions of crude oils comprising metal contaminants and Conradson Carbon contributing components by the combination of thermal visbreaking with fluid inert solids and catalytic upgrading of naphtha and higher boiling components of thermal visbreaking in separate systems of riser conversion and solids regeneration includes an external solids heat exchange apparatus arrangement utilized to partially cool hot regenerated solids utilized in the solids regeneration systems.

An improved ballistic separation device results from surrounding the downstream end of a progressive flow reactor or riser reactor with a concentric conduit that is in fluid communication with a cyclone separator and optionally in fluid communication with dipleg take-offs. The device may also include a bevelled lip or projection at the axial opening of the progressive flow reactor.

Vented riser

In an apparatus for the regeneration of fluid cracking catalyst, the catalyst is cooled in a heat exchanger mounted to the lower side of the regenerator and cool catalyst is returned to the regenerator by means of a separate gas lift.

Process and apparatus for cooling during regeneration of fluid cracking

Disclosed is an insert which surrounds the vapor outlet of a modified cyclone that lessens the tendency for carbonaceous deposits to form within the cyclone when separating mixtures of particulate and conversion products from high Conradson carbon feedstocks.

Cyclone for lessening formation of carbonaceous deposits

In a process apparatus for the regeneration of fluid cracking catalyst, the catalyst is cooled in an exchanger mounted to the lower side of the regenerator and cool catalyst is returned to the regenerator by means of gas lift.

Process for cooling during regeneration of fluid cracking catalyst

The present invention is concerned with the method of regenerating the fluidizable, catalytic, particulate solids in the regenerator section of an FCC process, and RCC process or a metals removal system or 'ART' type process. It is directed to the use of a conduit means for charging fluidizing gaseous material to a vertical cylindrical vessel for cooling fluidizable particulate solids flowing through said vertical cylindrical vessel, which conduit means comprises a horizontal header means having suspended therefrom a plurality of vertical and horizontally spaced apart conduits, each conduit having near its open end a restriction orifice. The header means is located near the top of the cylindrical cooling vessel. One portion of the vertical conduits has lower ends located in the upper half of the vessel and a second portion of the vertical conduits has lower ends located in a lower half of the vessel.

Apparatus for cooling fluid solid particles in a regeneration system

The present invention is concerned with the cooling of the fluidizable particulate solids, either catalytic or inert, in the regenerator section of an FCC process, an RCC process or a metals removal systems or 'ART' type process. It is directed to the use of a conduit means for charging fluidizing gaseous material to a vertical cylindrical vessel for cooling fluidizable particulate solids flowing through said vertical cylindrical vessel, which conduits means comprises a horizontal header means having suspended therefrom a plurality of vertical and horizontally spaced apart conduits, each conduit having near its open end a restriction orifice. The header means can be located near the top of the cylindrical cooling vessel. While the example of a specific embodiment discloses one portion of the vertical conduits with lower ends located in a lower cross-sectional area of the vessel other arrangements sufficient to ensure proper fluidization are also possible.

A combination process is described for upgrading residual oils and high boiling portions thereof comprising metal contaminants and high boiling Conradson carbon forming compounds comprising a thermal visbreaking operation with fluidizable inert solids followed by a fluidized zeolite catalytic cracking operation processing demetallized products of the visbreaking operation, regenerating solid particulate of each operation under conditions to provide CO rich flue gases relied upon to generate steam used in each of the fluidized solids conversion operation and downstream product separation arrangements, separating the wet gas product stream of each operation in a common product recovery arrangement and processing the high boiling feed product of visbreaking comprising up to 100 ppm Ni+V metal contaminant over a recycled crystalline zeolite cracking catalyst distributed in a sorbent matrix material comprising a high level of Ni+V metal contaminant.

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Ashland, KY, United States of America

Paul W Walters