Basf Aktiengesellschaft

Paul Duffner

Gerald Neubauer

Gerhard Frank

Hans J Wilfinger

Peter Rudolf

Manfred Ohlinger

Emil Pfannebecker

Georg Pilz

Rudi-Heinz Rotzoll

Gerhard Thiel

Ernst Dietl

Molded catalyst materials contain metallic cobalt and/or nickel particles and a lubricant, the said particles being obtained by reduction of cobalt oxide and/or nickel oxide particles containing less than 0.1% by weight of alkali metal oxides and/or alkaline earth metal oxides at .ltoreq.500.degree. C., and the molded catalyst material having an indentation hardness greater than 300 kp/cm.sup.2.

Molded catalyst materials containing reduced cobalt and/or nickel

Molded iron catalysts which contain metallic iron particles, obtained from anisometric iron oxide particles by contact with hydrogen at .ltoreq.500.degree. C., and a lubricant, are prepared.

Molded iron catalyst and its preparation

Saturated primary amines are prepared by reacting a nitrile with hydrogen at elevated temperature under superatmospheric pressure in the presence of ammonia and a metallic iron catalyst which has been obtained by reducing anisometric iron oxide particles with hydrogen at not more than 500.degree. C.

Preparation of primary amines

A process for the continuous preparation of an aqueous solution of a salt of an alkanedicarboxylic acid of 6 to 12 carbon atoms and an alkanediamine of 6 to 12 carbon atoms by reacting the particular alkanedicarboxylic acid with the particular alkanediamine in an aqueous solution of the salt to be prepared. The aqueous salt solution is recycled from a first mixing zone via a transport zone and a second mixing zone into the first mixing zone, liquid alkanediamine and an aqueous solution of alkanedicarboxylic acid are introduced between the first and second mixing zones. Less than the equivalent amount of alkanediamine is introduced, the remaining amount of liquid alkanediamine is added after the second mixing zone, and aqueous salt solution is taken off the first mixing zone at the rate at which it is formed. The salt prepared is used for the manufacture of a nylon.

Continuous manufacture of an aqueous solution of a salt of an

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Ludwigshafen, Germany

Paul Duffner