USA As Represented by Secretary of the Navy

International Telephone and Telegraph Corporation

Other

Pablo C Pureza

Jasbinder Singh Sanghera

Ishwar Dayal Aggarwal

Reza Mossadegh

Leslie Brandon Shaw

Brian A Cole

Shyam S Bayya

Daniel Joseph Gibson

Frederic Hau Kung

Dilip K Nath

Robert E Miklos

Shin M Oh

Guillermo R Villalobos

Mokhtar S Maklad

Danh C Tran

Gregory Nau

Fred Kung

A method and apparatus for making a substantially void-free preform for a microstructured optical fiber using a one-step process is provided. A preform is prepared from specialty glasses using a direct extrusion method. A die for use with the direct extrusion method is also provided, and a method for drawing the preform into a HC-PBG fiber for use in transmitting infra-red wavelength light is also provided. The preform comprises an outer jacket made of solid glass, a cladding having a plurality of air holes arranged in a desired pattern within the jacket, and a core which is hollow.

Direct extrusion method for the fabrication of photonic band gap (PBG) fibers and fiber preforms

A photonic band gap fiber and method of making thereof is provided. The fiber is made of a non-silica-based glass and has a longitudinal central opening, a microstructured region having a plurality of longitudinal surrounding openings, and a jacket. The air fill fraction of the microstructured region is at least about 40%. The fiber may be made by drawing a preform into a fiber, while applying gas pressure to the microstructured region. The air fill fraction of the microstructured region is changed during the drawing.

High air fraction photonic band gap fibers

A process includes the steps of disposing a solid core glass rod at a point removed from hot temperature that can cause crystallization in the core glass rod, disposing a solid clad glass rod at a point removed from the core glass rod; softening to the flowing condition the solid clad glass rod, transferring the softened clad glass to a lower point, the softened clad glass having a central void therethrough, heating the softened clad glass above its crystallization temperature, cooling the softened clad glass to a draw temperature, transferring the solid core glass rod into the central void in the softened glad glass, softening to the flowing condition the solid core glass rod with the heat from the softened and cooled clad glass, and drawing the core/clad, glass fiber by allowing the clad and core glasses to flow in the form of a fiber.

Multi heating zone apparatus and process for making core/clad glass fibers

This invention pertains to a hollow core photonic band gap chalcogenide optical glass fiber and to a fabrication method for making the fiber. The fiber, which is 80-1000 microns in outside diameter, is characterized by a solid glass circumferential region and a structured region disposed centrally within the solid region, the structured region includes a hollow core of 1 micron to several hundreds of microns in diameter surrounded by a plurality of parallel hollow capillaries extending parallel to the core, the core being centrally and longitudinally located within the fiber. Ratio of open space to glass in the structured region is 30-99%. The fabrication method includes the steps of providing a mold, placing chalcogenide micro-tubes around the mold, stacking chalcogenide micro-canes around the stacked micro-tubes, fusing the micro-tubes and the micro-canes to form a preform, removing the mold and drawing the preform to obtain the fiber. In an alternative fabrication method, the fiber is made by extruding flowing chalcogenide glass through suitably made plate to form a preform and then drawing the preform to form the fiber.

Hollow core photonic band gap infrared fibers

This invention pertains to apparatus and process for making core/clad glass fibers. The apparatus includes a central tube or receptacle connected at the top to a pressure controller and terminating in a reduced section; a side tube or receptacle positioned at about the level of the upper portion of the central tube; an outer tube or receptacle disposed around the bottom portion of the central tube terminating in a smaller section which is concentric with and spaced directly below the section of the central tube; a side arm connecting the side tube and the outer tube; and furnaces around the side, outer, and the reduced sections of the central and the outer tubes. The process includes the steps of disposing a solid core glass rod at a point removed from hot temperature that can cause crystallization in the core glass rod, disposing a solid clad glass rod at a point removed from the core glass rod, softening to the flowing condition the solid clad glass rod, transferring the softened clad glass to a lower point, the softened clad glass having a central void therethrough, heating the softened clad glass above its crystallization temperature, cooling the softened clad glass to a draw temperature, transferring the solid core glass rod into the central void in the softened clad glass, softening to the flowing condition the solid core glass rod with the heat from the softened and cooled clad glass, and drawing the core/clad glass fiber by allowing the clad and core glasses to flow in the form of a fiber.

An apparatus and method for drawing low loss fluoride glass fibers from a preform. A stream of reactive gas is passed around the preform and fiber so as to prevent moisture and oxygen contamination of the fiber while the fiber is being drawn. The apparatus includes an insulating vessel which surrounds a heating chamber in which the fiber is drawn, and a very narrow heating zone within the chamber for preventing crystallization of the drawn fiber.

Apparatus and method for drawing glass fibers

A core/clad glass optical fiber is made by melting a core glass rod and a adding glass rod in separate crucibles which are not concentric with respect to each other and the respective core and cladding glass melts passed out of contact with each other to a glass melt contacting zone proximate a fiber drawing orifice in which the cladding glass surrounds the core glass and a core/clad glass fiber is drawn. This process enables the clad glass fiber to be drawn directly from core and cladding glass rods without the need for a preform or forming a melt from glass chards or chunks, thereby reducing the cost of producing the fiber and also producing a glass clad optical fiber of high purity and excellent concentricity. Chalcogenide glass fibers having a concentricity of 100% have been made.

Apparatus for making optical fibers from core and cladding glass rods

Chalcogenide glass fibers are coated with metals. The products have impro bending strength and resistance to UV, visible light, and moisture. The metal coating may be applied by any method, such as dip coating or sputtering. Typical metals include In, Sn, Bi, Pb, Tl, Zn, Cd and C.

Metal-coated IR-transmitting chalcogenide glass fibers

A core/clad glass optical fiber is made by melting a core glass rod and a adding glass rod in separate crucibles which are not intersecting with respect to each other and the respective core and cladding glass melts passed out of contact with each other to a glass melt contacting zone proximate a fiber drawing orifice in which the cladding glass surrounds the core glass and a core/clad glass fiber is drawn. This process enables the clad glass fiber to be drawn directly from core and cladding glass rods without the need for a preform or forming a melt from glass chards or chunks, thereby reducing the cost of producing the fiber and also producing a glass clad optical fiber of high purity and excellent concentricity. Chalcogenide glass fibers having a concentricity of 100% have been made.

Process for making optical fibers from core and cladding glass rods

Core/clad glass optical fiber preforms free of bubbles and soot at the coclad interface are fabricated by inserting a glass core rod into a cladding glass tube sized so that space remains between them, sealing the top and bottom of the tube onto the core rod to form a sealed space between them which is relatively soot free and under a vacuum and then hot isostatically pressing the sealed composite to collapse the tube onto the rod and also collapse bubbles in the glass. Soot formation is avoided or minimized by purging the space with inert gas while the bottom of the tube is collapsed onto the rod and by sealing the top under a dynamic vacuum and at the lowest possible temperature to avoid soot formation without cracking the glass. The space is vacuum outgassed before the second seal is made. Chalcogenide fiber drawn from a preform made in this fashion exhibits very low transmission losses.

Method for producing core/clad glass optical fiber preforms using hot

A fiber optic sensor for detecting at least one chemical by evanescent wave spectroscopy comprises a generator of a light signal, a mirror for introducing the light signal into a fiber, a clad optical chalcogenide glass fiber, a mirror for directing the light signal from the fiber into a detector, and a detector for detecting chemicals by the fiber. The fiber comprises a core and a clad having lower refractive index than the core enveloping and being in continuous contact with the core, at least one region on the fiber completely or partially devoid of the clad, and a polymer disposed in the region having affinity for the chemical(s). There being a different polymer in each region if there is more than one region.

Selective multi-chemical fiber optic sensor

Glass free of surface carbon deposits, such as carbon film and/or carbon occlusions, and a process for removing such carbon deposits from glass. The process is characterized by the application of a plasma to glass to remove the carbon deposits. The plasma used for this purpose contains active specie which reacts with the carbon deposits to form gaseous carbon products.

Plasma treatment of glass surfaces to remove carbon

This invention pertains to optical waveguides which includes waveguides of ll shapes and sizes, preforms, and optical fibers made from the preforms, and to a method for making waveguides devoid of a physical interface. The method includes preparation of a waveguide from a halide-containing glass, heating the waveguide to a temperature below crystallization temperature of the glass so that it is still solid, providing a gaseous reactive medium containing halide ions of higher electronegativity than halide ions in the waveguide, exposing the waveguide to said reactive medium for a sufficient duration for the halide ions of higher electronegativity in the reactive medium to replace at least a portion of the halide ions of lower electronegativity in the waveguide, and cooling the waveguide whereby a lower refractive index is formed on the side of the waveguide exposed to the reactive medium than the refractive index internally of the waveguide so that light can travel through the portion of the waveguide having the higher refractive index.

Method of forming waveguides with ion exchange of halogen ions

Hydroxyl free deposition with high efficiency and at a high deposition rate may be achieved, even with use of relatively inexpensive raw materials, by utilizing a ring-shaped plasma activated axial chemical vapor deposition obtaining 100% chemical conversion and fractional volatilization of impurities. The plasma is induced in an annular stream of a plasma-forming gaseous medium, and the reactant or reactants used in the axial chemical vapor deposition are introduced into the center of the ring-shaped plasma to be converted by the heat of the plasma flame into soot which is deposited on a bait. An annular stream of a cooling medium flows outwardly past the plasma flame and is circumferentially centered by an extension of the outer tubular element of a plasma torch in which the plasma is generated. An RF generator which induces the plasma is operated at a frequency exceeding 20 MHz to give the plasma flame the desired ring-sloped configuration.

Fabrication of optical preforms by axial chemical vapor deposition

In order to provide a high power heat source having a very clean and invariable heat flux, a ring plasma is induced in a heating zone of a plasma torch including a plurality of coaxial tubular elements and the optical fiber is drawn through a channel passing axially through the center of the plasma torch and of the ring-shaped plasma. In this manner the preform from which the fiber is drawn can be placed in close proximity to the induced plasma without exposure to non-symmetrical temperature variations. Cooling gas passes through the heating zone either in an annular stream surrounding the plasma or in an annular stream passing through the center of the plasma around the preform and the fiber being drawn, or both. The heating zone is protected from environmental disturbances by an extension of the outer tubular element of the plasma torch which surrounds the heating zone. The plasma is induced by an RF source in an undisturbed stream of a plasma-forming gaseous medium, such as argon or a mixture of argon with oxygen, which flows through the heating zone.

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Burke, VA, United States of America

Pablo C Pureza