Seiko Epson Kabushiki Kaisha

Seiko Epson Corporation

Nobutaka Matsuo

Yoshitaka Itoh

Sadao Kanbe

Haruo Osafune

Masanobu Motoki

A sol-gel method of preparing doped glass articles is provided. The glass is formed by preparing a sol solution containing hydrolyzed silicon alkoxide and ultrafine particle silica. The sol solution can also include a dopant. The sol solution is gelled in a container, dried and sintered to yield the doped silica glass articles.

Method of preparing doped silica glass

A method of preparing preforms for optical fibers is provided. The method includes preparation of a first sol solution of a silicon alkoxide hydrolyzed with an acid and ultrafine particle silica, placement of the first sol solution into a container, and gelation of the first sol solution while the container is being rotated to yield a wet gel having a center hole. A second sol solution having a different composition than the first sol solution is prepared and used to fill the center hole in the wet gel. The second sol solution is then gelled to a wet gel composite and the composite is dried and sintered to yield the preform.

Method of preparing preforms for optical fibers

A method for preparing high quality silica glass articles is provided. The glass is prepared by hydrolyzing silicon alkoxide with a basic reagent to yield a first solution, hydrolyzing a silicon alkoxide with an acid reagent to yield a second solution, mixing the first solution with the second solution at a predetermined mixing rate to yield a sol solution, pouring the sol solution into a container, gelling the sol solution to a wet gel, drying the wet gel to a dry gel, and sintering the dry gel to yield a silica glass.

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Nagano, Japan

Nobutaka Matsuo