Basf Se Corporation

University of Cape Town

Nico F Fischer

Jürgen Zühlke

Hans-Martin Allmann

Michael Krämer

Frank Rosowski

Markus Schubert

Stefan Altwasser

Diana Carolina Galeano Nunez

Michael Christian Maximilian Claeys

The present invention relates to a catalyst system for oxidation of o-xylene and/or naphthalene to phthalic anhydride (PA), comprising a plurality of catalyst zones arranged in succession in the reaction tube, which have been produced using antimony trioxide comprising a noticeable proportion of senarmontite wherein some of the primary crystallites have a size of less than 200 nm. The present invention further relates to a process for gas phase oxidation, in which a gas stream comprising at least one hydrocarbon and molecular oxygen is passed through a catalyst system which comprises a plurality of catalyst zones arranged in succession in the reaction tube and which has been produced using an antimony trioxide comprising a noticeable proportion of senarmontite wherein some of the primary crystallites have a size of less than 200 nm.

Catalyst system for oxidizing o-xylol and/or naphthalene into phthalic anhydride

The present invention relates to a process for preparing phthalic anhydride by gas phase oxidation of aromatic hydrocarbons, in which a gas stream comprising at least one aromatic hydrocarbon and molecular oxygen is passed continuously over a thermostatted catalyst and the supply of the at least one aromatic hydrocarbon to the catalyst is temporarily interrupted after putting the catalyst on stream.

Process for preparing phthalic anhydride

A process for preparing carboxylic acids and/or carboxylic anhydrides by gas phase oxidation of aromatic hydrocarbons, in which a gas stream comprising at least one aromatic hydrocarbon and molecular oxygen is passed continuously over a catalyst thermostatted by a heat carrier medium, which comprises keeping the temperature of the heat carrier medium constant during the startup of the reactor for at least 24 hours, during which neither the loading of the gas stream with hydrocarbons nor the gas stream volume is increased by more than 3%.

Process for starting up a gas phase oxidation reactor

The present invention relates to a catalyst for preparing carboxylic acids and/or carboxylic anhydrides, which has a plurality of catalyst zones arranged in series and has been produced using a vanadium antimonate having a maximum content of crystalline valentinite of 5% by weight. The present invention further relates to a process for gas-phase oxidation in which a gas stream comprising at least one hydrocarbon and molecular oxygen is passed through a catalyst which has a plurality of catalyst zones arranged in series and has been produced using a vanadium antimonate having a maximum content of crystalline valentinite of 5% by weight.

Catalyst for preparing carboxylic acids and/or carboxylic anhydrides

A sample presentation device for radiation-based analytical equipment comprising a mounting base, a carrier carried by, and adjustable in position, relative to the mounting base, and an arm extending from the carrier and having at its opposite end a terminal member; Each of the carrier and terminal member has a coaxial connector for receiving two opposite end regions of a capillary tube that forms, in use, a reaction cell; A radiant heater, typically an infrared heater, is radially offset from the axis of the coaxial connectors for heating, in use, a capillary tube mounted by way of the coaxial connectors; The carrier and terminal member preferably have heaters associated therewith for heating the flow passages through them; The terminal member preferably has a passage generally coaxial with the connector for receiving a communications conductor carrying a temperature sensor at its end that is operatively located generally centrally within a capillary.

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Heidelberg, Germany

Nico F Fischer