USA As Represented by Secretary of the Navy

Nicholas J Condon

Steven R Bowman

Shawn P O'Connor

A method of growing a single crystal material using a device that includes a conical plug. The conical plug includes a first portion defining a first conical hole about an axis, the first conical hole having a first angle, and includes a second portion contiguous with the first portion and defining a second conical hole about the axis, the second conical hole having a second angle having the same sign as the first angle and being greater than the first angle. The device includes an upper tube comprising the conical plug fused therein and a seeding well plug. The device includes a lower tube including the seeding well plug fused therein. A single crystal KPbClmaterial is grown from the oriented single crystal KPbClseed through the first conical hole and then the second conical hole and then with continuing growth in the upper tube.

Method for the bottom-seeded growth of potassium lead chloride crystals from polycrystalline seeds

The method described herein allows for melt stabilization and vapor-phase synthesis of a cesium germanium halide utilizing germanium dihalides formed in situ. This disclosure allows for the melting of cesium germanium halides without decomposition, which allows for growing crystals of these materials from the melt. This disclosure allows for a direct synthesis of these materials without the use of water or the introduction of other possible contaminants.

Melt stabilization and vapor-phase synthesis of cesium germanium halides

A method and apparatus for growing a single crystal KPbClmaterial using a device including a plug including an axis. The plug includes a first portion defining a cylindrical hole about the axis. The plug includes a second portion defining a first conical hole about the axis. The first conical hole has a first angle. The plug includes a third portion defining a second conical hole about the axis. The second conical hole has a second angle opposite in sign relative to the first angle. The plug includes a fourth portion defining a third conical hole about the axis. The third conical hole has a third angle, the third angle having a same sign as the second angle and being greater than the second angle. The device further includes an ampoule including the plug fused therein.

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Greenbelt, MD, United States of America

Nicholas J Condon