Gte Products Corporation

Osram Sylvania Inc.

Nelson E Kopatz

Walter A Johnson

Joseph E Ritsko

Lori S Pruyne

David L Houck

Jack E Vanderpool

Philip E Stermer

Howard H Shaw

Preston B Kemp, Jr

Sanjay Sampath

Michael J Scheithauer

Leonid P Dorfman

Muktesh Paliwal

Raj P Singh

Michael R Pierce

Scott A Braymiller

A method for spheridizing silicon metal particles is described. The method involves injecting irregular silicon metal particles into a high-temperature plasma reactor to melt at least 50 weight percent of the particles. The molten droplets are solidified to form substantially spherical silicon particles having a thin SiO coating which may be removed by treating with a weak hydroxide solution.

Method of spheridizing silicon metal powders

A method of making flowable tungsten/copper composite powder by milling an aqueous slurry of a mixture of the desired weight ratio of tungsten powder and copper oxide powder and, optionally, a small amount of cobalt powder, spray-drying the slurry to form spherical, flowable agglomerates, and reducing the agglomerates in a hydrogen atmosphere.

Method of making flowable tungsten/copper composite powder

A method for making a tungsten-copper composite oxide wherein an amount of an ammonium tungstate and an amount of an oxide or hydroxide of copper are combined without milling to form a mixture. The unmilled mixture is then dehydrated and fired at a temperature and for a time sufficient to form the tungsten-copper composite oxide.

Method of making tungsten-copper composite oxides

A method of making a tungsten-copper composite oxide wherein an amount of an oxide of tungsten and an amount of an oxide of copper are combined to form a mixture, the oxide of tungsten or the oxide of copper, or both, being in a hydrated form. The mixture is then milled, dehydrated and fired at a temperature and for a time sufficient to form the tungsten-copper composite oxide, the time sufficient to form the tungsten-copper composite oxide being at least about one-half the time sufficient to form the tungsten-copper composite oxide from a mixture of tungsten trioxide, WO.sub.3, and cupric oxide, CuO, under substantially similar conditions.

A process comprising by producing maraging steel powder comprises forming an aqueous solution of iron, cobalt, nickel and molybdenum metals values in a predetermined ratio, forming a reducible solid material from the solution reducing the solid material to metallic powder particles, entraining at least a portion of the powder particle in a carrier gas which is fed into a high temperature zone to form droplets therefrom, and cooling said droplets to form essentially spherical shaped maraging steel alloy particles.

Hydrometallurgical process for producing finely divided spherical

Composite powders containing a first group of metals of iron, cobalt, nickel and molybdenum in specific ratios and one or more oxidizable metals can be formed by forming an aqueous solution containing first group of metals, forming solid material of the metals from the solution, reducing the solid material to a metallic powder, combining that powder with one or more easily oxidizable metals in an non-oxidizing atmosphere.

Hydrometallurgical process for producing irregular shaped powders with

A composition is disclosed consisting essentially of substantially spherical glass particles having a diameter of less than about 25 micrometers. A process is disclosed for producing substantially spherical particles. The process involves providing irregularly shaped glass particles having a predetermined particle size, entraining the particles in a carrier gas, feeding the entrained particles into a high temperature zone having a temperature sufficiently above the softening point of the glass to allow surface tension to subsequently spheroidize the particles and having a temperature below the vaporization temperature of the glass. The particles are maintained in the high temperature zone for a sufficient time to convert at least a portion of the particles into droplets without the formation of a substantial amount of filaments affter which the droplets are cooled to form solid spheres having essentially the same particle size as the irregularly shaped particles and a reduced surface area as compared with the irregularly shaped particles.

Process for producing spherical glass particles

A process for producing finely divided spherical iron group based metallic powders comprises forming an aqueous solution containing a source of the appropriate metal sources in a mineral acid, forming a reducible iron group based material from the solution, reducing the material to iron group based metal powder particles, subjecting the metal particles to a high temperature zone to melt a portion of the particles and to form droplets and cooling the droplets to form an essential spherical iron group based metallic powders.

Hydrometallurgical process for producing finely divided iron based

A process for forming particulate tungsten alloys from the individual metal sources comprises forming an aqueous solution containing the individual metals for producing tungsten heavy alloys, producing a solid particulate material from the solution and injecting the particle material into a high temperature zone and retaining such material in the high temperature zone for a time sufficient to at least partially melt the metals that are alloying with tungsten while maintaining the temperature of those metals below the boiling point of the lowest boiling metal in the second component. The prealloyed composite powder contains tungsten grains below about 5 micrometers as a discontinuous phase and has a continuous phase of the tungsten and a second component selected from nickel, iron, copper and mixtures thereof.

Process of making prealloyed tungsten alloy powders

A method is disclosed for producing aluminum oxide coated iron powder which comprises contacting iron powder of fine particle size with a liquid aluminum compound wherein the aluminum is hydrolyzable and adding water to the compound and the iron powder to form a slurry, removing essentially all of the liquid from the slurry to produce iron powder with a coating of hydrolyzed aluminum oxide, and firing the iron powder with the hydrolyzed aluminum oxide coating in a non-oxidizing atmosphere to produce iron powder with a coating of aluminum oxide.

Method for producing aluminum oxide coated iron powder

A method is disclosed for producing aluminum oxide coated iron-aluminum alloy powder which comprises contacting iron-aluminum alloy powder of fine particle size with a liquid aluminum compound wherein the aluminum is hydrolyzable and adding water to the compound and the iron-aluminum alloy powder to form a slurry, removing essentially all of the liquid from the slurry to produce iron-aluminum alloy powder with a coating of hydrolyzed aluminum oxide, and firing the iron-aluminum alloy powder with the hydrolyzed aluminum oxide coating in a non-oxidizing atmosphere to produce iron-aluminum alloy powder with a coating of aluminum oxide.

Method for producing aluminum oxide coated iron-aluminum alloy powder

A method is disclosed for producing aluminum oxide coated cobalt powder which comprises contacting cobalt powder of fine particle size with a liquid aluminum compound wherein the aluminum is hydrolyzable and adding water to the compound and the cobalt powder to form a slurry, removing essentially all of the liquid from the slurry to produce cobalt powder with a coating of hydrolyzed aluminum oxide, and firing the cobalt powder with the hydrolyzed aluminum oxide coating in a non-oxidizing atmosphere to produce cobalt powder with a coating of aluminum oxide.

Method for producing aluminum oxide coated cobalt powder

A process for forming particulate tungsten heavy alloys from agglomerated material containing the individual metals by using a high temperature zone is improved by retaining the material in the high temperature zone for a time sufficient to at least partially melt the metals that are alloying with tungsten while maintaining the temperature of those metals below the boiling point of the lowest boiling metal in the alloying component.

Process for producing prealloyed tungsten alloy powders

Apparatus is disclosed for reacting a powder with a gas comprising a shroud consisting of a first section having a peripheral cylindrical wall with inner surface and outer surface. Inner surface defines a cavity which serves as reaction chamber in which powder and gas react. First section is detatchably mounted at top end to exit nozzle of high temperature source. First section has powder inlet opening(s) extending through peripheral wall from outer surface to inner surface, thereby connecting the outside with reaction chamber through which powder enters the chamber. Powder inlet opening(s) are positioned sufficiently close to exit nozzle to allow powder to melt and react with gas in the molten state. Second section forms cylindrical jacket skirting lower part of first section at a point below powder inlet openings. Jacket has outer peripheral wall, inner wall one and same with peripheral wall of first section, and top and bottom ring plates forming top and bottom walls respectively of second section. Walls of second section define a plenum. Second section has outer opening(s) through outer peripheral wall of jacket connecting outside with plenum through which gas enters from outside to plenum. Second section has two or more inner openings through inner wall of second section, which connect plenum with chamber through which gas enters chamber from plenum to react with powder in chamber. Inner openings are directed downward into chamber and tangential to inner surface of shroud. Resulting reaction product exits shroud through bottom end of chamber.

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Sayre, PA, United States of America

Nelson E Kopatz