Zhejiang Huangma Technology Co., Ltd.

Zhejiang Huangma Shangyi New Material Co., Ltd.

Zhejiang Lukean Chemical Co., Ltd.

Shangyu Huangma Surface Activated Reagent Research Institute Co., Ltd.

Zhejiang Huangma Chemical New Polymer Material Co., Ltd

Minggui Song

Majishi Wang

Jun Wang

Jiang Yu

Yifan Xu

Yifeng Jin

Weisong Wang

Provided are a system and a method for preparing a polyether amine by catalytic amination of a polyether diol. The preparation method includes: filling a catalyst into the fixed bed reactor; pressurizing the internal pressure of the fixed bed reactor to 10˜13 MPa by a hydrogen gas, and raising the temperature of the fixed bed reactor to 150˜185° C.; adjusting the temperature of the multi-stage preheater so that the feeding temperature of a raw material reaches 125˜135° C.; and simultaneously feeding a polyether diol, liquid ammonia and the hydrogen gas into the multi-stage preheater, and after mixing and preheating, introducing into the fixed bed reactor from the feed inlet of the fixed bed reactor for a continuous catalytic amination reaction. The total amine value of the polyether amine finally obtained by the present invention reaches 28˜32 mgKOH/g, the color reaches 10˜20, and it is colorless transparent liquid.

System and method for preparing polyether amine by catalytic amination of polyether diol

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Shaoxing, China

Minggui Song