University of Nebraska

Nutech Ventures

Milford A Hanna

Gerald Biby

Pratik Bhandari

Viswas M Ghorpade

Yusuf Ali

Vesselin Miladinov

Rangaswamy Chinnaswamy

Robert Weber

Viswas Ghorpade

Qi Fang

A reactive extrusion process for the production of substituted polysaccharides, in particular, cellulose acetate, starch acetate, carboxymethyl cellulose, and carboxymethyl starch.

Method for the production of substituted polysaccharides via reactive extrusion

A method is provided for mulching an agricultural soil bed using a biodegradable protein mulch material. The method includes the preparation of a film forming solution of a film forming protein material. The film forming protein solution is then sprayed directly onto a surface of an agricultural soil bed. The solution dries to form a thin film of protein material on the surface of the agricultural soil bed. The protein material may comprise a plant protein, a milk protein, an animal protein, a whey protein, casein, an egg protein or gelatin. Following a harvest, the mulch material, which is biodegradable, may simply be plowed under.

Method for mulching an agricultural soil bed using a biodegradable protein material, and a mulched agricultural crop growing plot produced thereby

This process involves feeding cellulose into an extruder with an acid solution. The extruder is comprised of a screw and a barrel. The screw is rotated so as to pressurize the cellulose, and the cellulose undergoes acid hydrolysis and forms microcrystalline cellulose. The invented process can be accomplished by using pure cellulose or a lignocellulosic material as the starting material. If a lignocellulosic material is used, then a basic solution is added to it and the lignocellulosic material is fed through an extruder so as to obtain a mixture comprising lignin, hemicellulose and cellulose. The lignin and hemicellulose are extracted and the remaining cellulose is processed, as discussed previously, to form microcrystalline cellulose.

Production of microcrystalline cellulose by reactive extrusion

A foam that is the extrudate of a mixture of a biodegradable polymer, starch, talc, and a blowing agent is provided. This foam is made by extruding a mixture of the above-listed components. This foam is water-resistant and in some variations waterproof making it an effective packing material. Still further, this foam is biodegradable, and thus, it can be disposed without creating environmental waste. In addition, the foam may be extruded into sheets and then thermoformed to form various articles.

Water-resistant degradable foam and method of making the same

The present invention relates to a continuous process for preparing levulinic acid from starch in a reactive extrusion process. In a preferred embodiment, the extrusion takes place in a twin-screw extruder having a plurality of temperature zones wherein the starch slurry is preconditioned, extruded, filter pressed, reboiled, vacuum distilled, condensed, centrifuged, whereby the waste effluent from the centrifugation is reprocessed upstream to the preconditioning stage.

Method and apparatus for production of levulinic acid via reactive

To prepare a biodegradable plastic, biodegradable materials such as starches and a non-biodegradable polymer such as a polystyrene, polyurethane, polyethylene, polypropylene, or polycarbonate are treated: (1) under heat, pressure and reagents to break the polymers; and (2) by adding to them an oxidizing agent. This treatment forms and/or makes available reactive groups for bonding: (1) on the biodegradable material groups such as aldehyde or hydroxyl groups in the case of the carbohydrates and amine groups in the case of proteins and certain other compounds such as urea; and (2) on the non-biodegradable plastic groups such as aldehydes, methyl, propyl, ethyl, benzyl or hyroxyl groups. In one embodiment, plastic and starch are processed in an extruder by: (1) mixing a starch in a range of between 15 percent and 80 percent, an oxidizing agent and an agent to break up the starch and the plastics; and (2) subjecting the combination to sufficient heat and/or pressure to break the plastic into shorter chains and bond monosaccharides to monomers from the non-biodegradable polymer.

Growing community of inventors

Lincoln, NE, United States of America

Milford A Hanna