Mallinckrodt, Inc.

Mallinckrodt Medical, Inc.

Mallinckrodt Specialty Chemicals Company

Liebel-flarsheim Company LLC

Michael J Gentilcore

David H White

William Z McCarthy

Allan R Bailey

Robert E Vandas

Hung V Nguyen

Anna K Fukunaga

Derick L Kaspar

David G Mock

A process for separating soluble silica species such as monomeric silicic acid (or monosilicic acid) and low molecular weight soluble polymeric silica from impure water soluble compounds by membrane nanofiltration is provided. A process for separating soluble silica species and colloidal silica from impure water soluble compounds by reverse phase liquid chromatography is also provided.

Removal of silica from water soluble compounds by nanofiltration and reverse phase chromatography

A method to purify N,N-dimethylacetamide (DMAc) from an aqueous solution containing acetic acid as a contaminant. Two fractional distillation columns are arranged in a series. The solution containing the contaminant is provided to the first column with a temperature profile to result in acetic acid partitioning into the overhead water. The material remaining in the bottom portion of the first column is recycled to the first column and also provided into a second column, whereby DMAc free of acetic acid contamination is recovered, and remaining DMAc and acetic acid are returned to the first column for further separation. The method uses standard fractional distillation procedures and equipment, thus eliminating the need for more complex extractions and/or chromatographic separations.

Purification of N,N-dimethylacetamide

A process for the separation of amyl acetate, a high boiling point solvent from various high boiling point corrosive impurities, namely, bromoethyl acetate, in an industrial setting to allow for reuse through continuous recycling thereof.

Separation of high boiling point solvents from amyl acetate

A dust control apparatus having a cover member lowerable into an opening of a container, the cover member having a radially expandable seal for sealing the opening, the cover member having a passage therethrough adapted to receive a conduit, the cover member being operable in telescoping relation to the conduit and the passage being sufficiently larger than the conduit for the passage of air between the cover member and conduit, the cover member being movable laterally relative to the conduit to enable the cover member to be lowered into a container which is not precisely aligned therewith, a filter sleeve having a lower end attached to the cover member and an upper end attached to the conduit, the filter sleeve being adapted to prevent the escape of dust from the space between the cover member and conduit, the filter sleeve being protected by the conduit from damage caused by materials flowing through the conduit, the apparatus including an optional fume collecting annulus locatable in surrounding relation to the filter sleeve for collecting and exhausting gases and fumes collected thereby, and an optional inlet port for introducing inert gases or pressurized air to the apparatus.

Dust control apparatus

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Maryland Heights, MO, United States of America

Michael J Gentilcore