R.j. Reynolds Tobacco Company

Michael E Edwards

Barry Smith Fagg

Robert Eugene Grubbs

Richard G Haberkern

William L Clapp

James D Frederickson

Concentrated tobacco extracts or essences are provided by first extracting water soluble components from tobacco. The aqueous extract then is contacted with supercritical carbon dioxide, and certain tobacco components in turn are extracted from the aqueous extract. Alternatively, the aqueous extract is subjected to a spray drying step, and the spray dried extract is contacted with supercritical carbon dioxide in order that certain tobacco components are extracted from the spray dried extract. The resulting extracted components are separated from the supercritical fluid in order to yield a tobacco essence. The essence has a homogeneous, viscous character and exhibits a tobacco aroma. The essence is useful as a flavoring agent for cigarettes and other smoking articles.

Process for providing tobacco extracts using a solvent in a

The invention is directed to a process for increasing the filling capacity of tobacco under moderate conditions of temperature and pressure. Tobacco is impregnanted with a low boiling impregnant and thereafter subjected to a pre-expansion treatment. The pre-expansion treatment includes a pre-expansion temperature which is above the atmospheric boiling point of the impregnant and which is at least ten degrees below the critical temperature of the impregnant; and a pressure which is at least five atmospheres above the boiling point pressure of the impregnant at the pre-expansion temperature. Under these conditions, the impregnant is maintained primarily in the liquid phase throughout the pre-expansion treatment. Following the pre-expansion treatment, the pressure of the treated tobacco is rapidly reduced to a pressure below the boiling point pressure of the impregnant to thereby effect tobacco expansion without the need for a separate heating step.

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Windsor, NC, United States of America

Michael E Edwards