Petrochina Company Limited

Mengjun Zhao

Xuesong Lu

Hua Tian

Caineng Zou

Shuichang Zhang

Keyu Liu

Shaobo Liu

Junjia Fan

Qingong Zhuo

Yanjie Gong

Lin Wei Jiang

Xiuli Li

Xingzhi Ma

Bin Zhang

Zhichao Yu

Qingyang Meng

Peiqiang Yang

Lili Gui

A method and an apparatus for measuring oil content of a tight reservoir based on nuclear magnetic resonance includes applying a pulse sequence to a tight reservoir rock, and after applying a first pulse and a last pulse in the pulse sequence, applying a gradient magnetic field to the tight reservoir rock, respectively, directions of the two applied gradient magnetic fields being opposite to each other, wherein the pulse sequence is composed of three 90&#xb0; pulses; acquiring a nuclear magnetic resonance signal of the tight reservoir rock; and determining oil content of the tight reservoir rock according to an intensity of the nuclear magnetic resonance signal. The method can accurately distinguish an oil phase nuclear magnetic resonance signal and a water phase nuclear magnetic resonance signal in nanopores of tight reservoir rock, thereby effectively improving the accuracy of the detection result of the oil content of the tight reservoir rock.

Method and apparatus for measuring oil content of tight reservoir based on nuclear magnetic resonance

The invention provides a method for determining oil contents in rocks. The method comprises steps of: measuring a plurality of calibration oil samples having different oil contents, and acquiring a holographic fluorescence spectral intensity corresponding to the calibration oil samples; acquiring a fit relation between the holographic fluorescence spectral intensity and the oil contents of the calibration oil, according to the oil contents of the plurality of calibration oil samples and a plurality of three-dimensional fluorescence spectral intensities corresponding thereto; adding a certain amount of the calibration oil after dilution to rocks to be measured, acquiring a sample of the rocks to be measured and performing a holographic fluorescence measurement of the rock sample to be measured; and introducing the holographic fluorescence spectral intensity of the rock sample to be measured to the fit relation, thus an oil content of the rock sample to be measured is obtained. Accordingly, oil is detectable together with an organic solvent without volatilization of the organic solvent, which not only saves time, but also address a low-detection-limit problem for oil content resulting from volatilization of oil when the organic solvent is volatilized in the conventional method.

Method for determining oil contents in rock formations

A device and method of determining thermal maturity of oil source rocks by total scanning fluorescence including testing the organic solution of the extract from a series of oil source rock samples collected at different depths by total scanning fluorescence; building a model for interpretation of the oil source rock maturity according to the variation with depth of the TSF Intensity parameter and the TSF Rparameter obtained by total scanning fluorescence, and identifying the stage of initial oil generation, the stage of major oil generation and the stage of major gas generation; and establishing the relationship between the TSF Intensity parameter and/or the TSF Rparameter with the existing characteristic parameters that quantitatively characterize the maturity of oil source rocks, thereby accomplishing the analysis and determination of the maturity of the oil source rocks.

Method for determining maturity in oil source rock by total scanning fluorescence and the device therefor

The present disclosure discloses a core holder for a micron CT observation and an experimental method thereof. The core holder for a micron CT observation comprises: a carbon fiber pipe and a base; the base comprises a fluid injection channel therein; the carbon fiber pipe is provided with a core mounting cavity and a carbon fiber plunger therein; the carbon fiber pipe is a tubular structure with one end closed and the other end open; the carbon fiber plunger can fix the core between the closed end of the carbon fiber pipe and the carbon fiber plunger; the other end of the carbon fiber pipe is in a detachable sealed connection with an outlet of the fluid injection channel of the base. The core holder for a micron CT observation reduces the distance between the core and the micron CT radiation source, and improves the resolution.

Core holder for micron CT observation and experimental method thereof

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Beijing, China

Mengjun Zhao