Bepex Corporation

Hosokawa Bepex Corporation

Masayuki Inoue

Ilya Pikus

Greg J Kimball

A system for crystallization of polymers involving the use of a stationary housing with a rotor mounted for rotation within the housing. The rotor supports a plurality of spaced apart hollow discs and heated fluid is delivered to the interior of the discs. The polymer material to be treated is fed into the housing for heat exchange contact with the exterior surfaces of the discs. The rotation of the discs in addition serves as the propelling force for the material along the length of the housing at which point the material is discharged. The speed of rotation of the rotor is controlled to influence agitation and conveying of material in the housing to thereby control the crystallization reaction. A holdup mechanism which operates independently of the speed control is located adjacent the discharge location to contribute to the fixing of the residence time. The material inlet operation, discharge operation and residence control are such that the ratio of crystallized to uncrystallized material is maintained within desired limits, typically at about 4 to 1. The method and apparatus provides various other operating parameters and structural features which maximize the efficiency of the crystallization reaction.

System for polymer crystallization

A system for treating flowable materials wherein an elongated cylindrical housing is provided with an inlet for introducing material to the housing at one end thereof. An inner wall surface is defined by the housing and the temperature of the inner wall surface is controlled for heat exchange between the material and the surface. An outlet for the material is provided at the other end of the housing, and an agitator extends within, and at least partially along the length of, the housing for rotation within the housing. The agitator comprises a plurality of paddles extending from adjacent the axis of rotation of the agitator toward the inner wall surface, the paddles being positioned in spaced apart locations over at least a portion of the length of the inner wall surface whereby rotation of the agitator results in the moving of the material around the inner wall surface and the propelling of the material from the inlet to the outlet. A plurality of nozzles are associated with the agitator, and gas is supplied to the nozzles and directed from the nozzles into contact with the material. This action serves to spread the material over the inner wall surface for thereby maximizing the extent of contact between the material and the surface, and for otherwise maximizing the efficiency of the material treatment.

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Henn, MN, United States of America

Masayuki Inoue